P E T R O L E U M AS Ov TM er 1 M 00 et ho ds Certified Reference Standards 4th Edition Member AccuStandard ® Notice the Difference with AccuStandard Experience in Petrochemical Requirements • Years of Round Robin Studies with ASTM • Ampulled over 300 gallons of ASTM fuel sets including over 35 gasoline and hydrocarbon blends • Standards for over 100 ASTM Methods • 17 years of Manufacturing, Organic & Inorganic Standards • Synthesizes rare Hydrocarbons not otherwise available Involvement in the Petrochemical Industry • Participation in regular ASTM meetings • Active in D-02 and D-16 subcommittees • Provides support to several Petrochemical Instrument Manufacturers Resources • Low Sulfur Analyzers (such as XOS) for Measurements to ppb Levels • Instrumention for Analyzing Standards for ICP, ICP-MS, AA, GC/MS, GC/FID, GC/EC, GC/NPD, Karl Fischer Titrator, and others • NIST/NVLAP Accredited (Lab Code 200389-0) as a PT Provider • ISO 9001:2000 Certified (ISO 9001 for the last 10 years) • Extensive Inventory of ASTM and Related Standards New Products in this Catalog • Low Sulfur and Nitrogen Standards (see pages 6-11) • LUFT/LUST Standards (see pages 81-98) • TPH Standards (see pages 81, 92-93, 96-97) • No Haz Fee ICP & AA Standards (see pages 67-75) • Additional New ASTM Standards PRINTED ON RECYCLED PAPER © AccuStandard, Inc. 2003 Table of Contents ASTM # PIANO 81-98 Index Quote Form Order Information i-vii back back ICP & AA LUFT/LUST and TPH (New Section) ORGANOMETALLIC Wear Metals Group 10 10, 17 6-11 10 6-11, 31 38 6-11 6-11 D-3605 D-4628 D-4927 D-4951 D-5185 D-5708 D-5863 D-6443 D-6481 Trace Metals in Gas Turbine Fuel by AA Wear Metals in Lube Oil Wear Metals and Additives by WDXRF Wear Metals and Additives by ICP Wear Metals and Additives by ICP Trace Metals by ICP Trace Metals by AA Metals in Oil Lube Oils by ED-XRF INDEX Quality System is Certified to comply with the International ISO 9001:2000 Quality Standard 17 22 25, 63-64 26 28 39, 62 52 58, 64 58, 63-64 LUFT/LUST by XRF by Oxidative Microcoulometry in Petro Gas by Oxidative Microcoulometry by ED-XRF by Ultra Violet Fluorescence Compounds by Sulfur Selective Detection in Gasoline by Wavelength WD-XRF in Gasoline by ED-XRF WEAR METALS Sulfur Sulfur Sulfur Sulfur Sulfur Sulfur Sulfur Sulfur 6 62 Organometallic (Wear Metals) Analysis by AA, ICP, DCP, XRF 26, 28, 59-66 Plasma Emission Spectroscopy (ICP) 67-71 ICP (No Haz Fee) New 67-71 Atomic Absorption Spectroscopy (AA) 67, 73-75 AA (No Haz Fee) New 67, 73-75 Plasma Emission / Mass Spectroscopy (ICP/MS) 72 Trace Metals, Chlorine in Lube Oil, and Organo Tin New 66 Ion Chrom 76-79 Sulfur Standards Group D-2622 D-3120 D-3246 D-4294 D-5453 D-5623 D-6334 D-6445 Water in Petroleum V & Ni with Mn page 30 31 31 31 32 29, 32 32 32-33 34-36 37 37 38 39, 62 40 42-51 52 52 52 52 53 53 53 54 54 54 55 55 5 10, 56 56 56 57 57 57 58-65 10, 58 63, 64 58 57 SULFUR D-3120 D-3230 D-3231 D-3237 D-3246 D-3340 D-3524 D-3605 D-3606 D-3610 D-3710 D-3798 D-3831 D-4059 D-4110 D-4291 D-4294 D-4377 D-4420 D-4628 D-4629 D-4815 D-4927 D-4928 D-4929 D-4951 D-5056 D-5059 D-5134 D-5184 D-5185 D-5186 D-5188 D-5191 D-5307 Method Description MtBE Analysis by GC Petroleum Waxes by GC PNA Analysis by Multidimensional GC Sulfur by Ultra Violet Fluorescence Engine Oil Volatility by GC Vapor Pressure Standards Ethanol Analysis by GC Aromatics by GC Oxygenates by OFID Trace Metals by ICP Oxygenates by Reductive Pyrolysis Sulfur Compounds by Sulfur Selective Detection Trace Metals by ICP Nitrogen by Chemiluminescence Aromatics by GC/MS Cloud Point of Petro Products Cloud Point of Petro Products (Linear Cooling Rate) Cloud Point of Petro Products (Constant Cooling Rate) Trace Metals by AA Freezing Point Aviation Fuels (Auto Optical Method) Freezing Point Aviation Fuels Oxygenates and Aromatics by GC/FTIR PCBs by GC Solvent Red 164 Dye Concentration in Diesel Fuels Benzene in Spark Ignition Fuels Oxygenates (O-PONA) in Engine Fuels by GC Total Olefins in Spark Ignition Engine Fuels by GC Water in Liquid Petro Products Sulfur in Gasoline by Wavelength WD-XRF Boiling Range Distribution of Petroleum Vapor Pressure Aromatic Hydrocarbon by HPLC Engine Oil by GC Sulfur by ECD Metals in Oil Sulfur in Gasoline by ED-XRF Lube Oils by ED-XRF 58, Olefin Content of Gasoline by SFC Aromatic Hydrocarbon by HPLC ASTM D-2887 ASTM # D-5441 D-5442 D-5443 D-5453 D-5480 D-5482 D-5501 D-5580 D-5599 D-5600 D-5622 D-5623 D-5708 D-5762 D-5769 D-5771 D-5772 D-5773 D-5863 D-5901 D-5972 D-5986 D-6160 D-6258 D-6277 D-6293 D-6296 D-6304 D-6334 D-6352 D-6378 D-6379 D-6417 D-6428 D-6443 D-6445 D-6481 D-6550 D-6591 (IP 391) E-1064 ISO/CD QC D-56 D-86 D-92 D-93 D-445 D-611 D-1015 D-1319 D-1744 D-2386 D-2500 D-2622 D-2789 Method Description page Cross Reference Tables (ASTM,IP,ISO,DIN,JIS,AFNOR) II Analytical Capabilities III On-Line Ordering IV Quality Control 1-2 Flash Point Standards 3 Synthetic Distillation Standard 3 Flash Point Standards (COC) 3 Flash Point Standards (PMCC) 3 Viscosity Calibration Standard 3 Aniline Point Standard 4 Freezing Point Standards 4 Olefin Analysis by FIA 4 Water in Liquid Petroleum Products 5 Freezing Point Calibration Standards 5 Cloud Point Calibration Standards 5 Sulfur by XRF 10 Hydrocarbon Analysis in Gasoline by GC/MS 11 PIANO, PONA, PNA by GC 12-13 Proposed Method for Detailed Hydrocarbon Analysis 14 Detailed Hydrocarbon Analysis PONA VI 14 Boiling Range by GC 14 Simulated Distillation (SIM DIS) by GC 15 Sulfur by Oxidative Microcoulometry 16 Salts in Crude Oil 16 Phosphorus in Gasoline 16 Lead in Gasoline by AA 16 Sulfur in Petroleum Gas by Oxidative Microcoulometry 17 Li & Na in Lubricating Greases by Flame Photometer 17 Diesel Fuel Analysis by GC 17 Trace Metal in Gas Turbine Fuels by AA 17 Aromatics in Gasoline by GC 18 Total Co Analysis by Potentiometric Titration 18 Boiling Range by GC 20 p-Xylene Analysis by GC 20 Manganese in Gasoline by AA 20 PCB Analysis by GC 21 Ion Chrom 76 Ethylene Glycol by GC 21 Sulfur by ED-XRF 7-11, 21 Water in Liquid Petroleum Products 5, 21 Aromatics in Gasoline by GC 22 Wear Metals in Lube Oil 22 Nitrogen by Chemiluminescence 23 Oxygenates in Gasoline by GC 24 Wear Metals and Additives by WD-XRF 25,63 Water in Liquid Petroleum Products 6, 25 Chlorine in Crude Oil by Microcoulometry 25 Wear Metals and Additives by ICP 26 Trace Metals in Petroleum Coke by AA 26 Lead in Gasoline by X-Ray Spectroscopy 27 Petroleum Naphthas through n-Nonane by GC 27 Al and Si by ICP-AES & AA 28 Wear Metals and Additives by ICP 28 Aromatics by SFC 28 Vapor - Liquid Ratio Temperature 29 Vapor Pressure Standards 29 Boiling Range Distribution of Crude Petroleum by GC 29 QUOTE FORM Cross Reference Table Sorted by ASTM Method Use the AccuStandard Cross Reference Tables to Match various International Methods for known Petrochemical analysis. MEMBER Fully Accredited For over 17 years AccuStandard has been the Leader in the Chemical Standards Industry in both Organic and Inorganic products. AccuStandard is ISO 9001:2000 registered and a NIST/NVLAP accredited Proficiency Testing provider (NVLAP Code 200389-0). ISO 9001:2000 Certificate Number: 31692 ANALYSIS ASTM IP ISO DIN JIS AFNOR PAGE Tag Flash Point D-56 Distillation D-86 123 3405 51411 K 2580 M07-003 3 51751 K 2254 M07-002 3 COC Flash Point D-92 36 2592 51376 K 2265 T60-118 3 PMCC Flash Point D-93 34 2719 51758 K 2265 M07-019 3 Kinematic Viscosity D-445 71-1 3104 51562 K 2283 T60-100 3 Aniline Point D-611 2 2977 51775 M07-021 4 Hydrocarbon Types by FID D-1319 156 3837 51791 M07-024 4 Water (Karl Fischer) D-1744 T60-154 5 Freezing Point D-2386 16 3013 51421 K 2276 M07-048 5 Cloud Point D-2500 219 3015 51597 K 2269 T60-105 5 Sulfur by XRF D-2622 51400T6 K 2541 Boiling Range By GC D-2887 3924 14 Sulfur by Oxidative Microcoulometry D-3120 16591 16 Lead by AAS D-3237 428 Sulfur by Oxidative Microcoulometry D-3246 373 Metals by AA D-3605 413 Benzene by GC D-3606 425 Sulfur by ED-XRF D-4294 336 8754 Water (Karl Fischer) D-4377 356 10336 Metals by AA D-4628 308 Nitrogen by Chemiluminescence Detection D-4629 379 Metals by WD-XRF D-4927 407 Water (Karl Fischer) D-4928 386 Lead in Gas By X-Ray D-5059 228 Vapor Pressure D-5191 394 Oxygenates D-5599 408 34-36 Cloud Point D-5771 444 52 Cloud Point D-5772 445 52 Cloud Point D-5773 446 52 Freezing Point D-5901 434 53 Auto-Freeze Point D-5972 435 53 Hydrocarbons Automatic D-6379 436 57 Hydrocarbons Automatic NEW D-6591 391 57 Metals K 2536 6296 10 16 M07-052 8691 51790T3 10 17 18 M07-053 21 5 51391T1 22 M07-058 51391T2 23 25, 63 10337 5, 25 27 M07-079 14597 29, 32 62 This is a partial list of Standards available for ASTM Methods Tables Generated from (a) R.A. Nadkarni, “Guide to ASTM Test Methods for the Analysis of Petroleum Products and Lubricants”, Manual 44 (200), ASTM West Conshohocken, PA (b) Annual Book of ASTM Standards 2000, Volumes 05.01 to 05.05 II Member AccuStandard is an active member in ASTM and strives to keep abreast of ASTM method revisions. If our listed formulation does not meet the most recent method revision, please contact Technical Support, ext. 117 for an updated product. Analytical Capabilities Analytical Instruments Inorganic (ICP) PE Optima 3000 Spectro FMD-07 Organics GCs: (6) HP 5890 Series II, FID, NPD, ECD all with auto injectors GC/MS: (3) HP 5971A HP 5971A with OI Analytical Purge & Trap PE Q-Mass 910 HPLC: Varian 5000 with Applied Bioscience Fluorescence detector and HP auto injector Sulfur (low level) XOS (XRF) with monochromatic wavelength disperser Antek 9000 Series (UVF) Miscellaneous Ion Chromatograph, Waters 600E with Conductivity detector 431, Alltech 335 Ion Suppressor Automatic Polarimeter, Zuzi W22 Karl Fischer Titrator Lab Resources Milligram to Kilogram Scale Glassware Equipment to work under N2/Ar Flash and Liquid Solid Phase Chrom. (mg to 2 kg) Preparative TLC Buchi Rotary Evaporator Vacuum Drying Oven Parr Pressure Reactor (high pressure reaction, hydrogenation) Distillation Equipment - High Vacuum Distillation, Molecular Distillation (Kugelrohr), Spinning Band Columns, Packed and Vigreaux columns Melting Point Apparatus pH meter Viscometer Centrifuge III On-Line Ordering There is an easier way to get Chemical Reference Standards ® e-Standards from AccuStandard.com 5 Ways to Search “e-Standards” is the Fastest, Most Comprehensive Search Engine available and contains over 30,000 products. Search by: Catalog Number Single or Multiple Components, Method (EPA, ASTM, etc.) Chemical Category (Organic, Inorganic, Petroleum, etc.) Other Companys’ Part Number Log on to www.accustandard.com and see how easy it is. Easy Ordering 24/7 Find It Fast...simply search for a product, select it for purchase & click - it's that easy! Discounts may apply to online orders, see details on website. On-Line Custom Services AccuStandard specializes in synthesizing chemicals of high purity to be used as reference standards, and offers custom synthesis capability for milligram to kilogram batches. If you can't find the specific standard you need, we can prepare Custom Formulations and Custom Packaging for both Organic and Inorganic needs. See our Website for more info. Over 30,000 Standards just a click away Custom Formulations AccuStandard offers over 30,000 different standards, and if you can't find the specific standard you need, we will prepare a custom formulation. Our custom organic and inorganic standards are a fast, economical way to address your unique requirements. To make an inquiry for Custom Quotes visit our website. You can also Email your requirements to [email protected] or Fax us at 203-786-5287. Please include the following information: List of analytes and concentrations, Solvent or matrix, Quantity required (milliliters), Packaging unit size (milliliters per ampule, bottle, or vial). Quality Control Options 1. Gravimetric/Volumetric Certification: Each standard is measured gravimetrically and then QC’ed instrumentally (where available). Every component in the standard is guaranteed to be within ±0.5% of the requested value unless otherwise stated. The solutions are made up to volume using class A glassware. A certificate comes with each standard and documents the gravimetric values used. 2. Quantitative Validation: Full QA/QC method includes extended GC analysis using both internal and calibration standards plus statistical analysis. A data package is provided containing analytical and gravimetric data (Organic customs only). Also available: OEM Standards - Privately labeled standards manufactured and tested to your specifications. IV Quality Control Standards Real World Gasoline D-02.03 D-02.04 QC AccuPetroCheck and AccuPetroTest Real World Gasoline QC Standards AccuPetroCheck Consensus Value QC Standards Conventional Gasoline QC Standard CARB Low Sulfur RFG QC Standard ASTM-FUEL-QCS-01-PAK $ 60 / 5 x 15 mL ASTM-FUEL-QCS-02-PAK $ 60 / 5 x 15 mL Parameter Total Aromatics Total Olefins Total Saturates Sulfur Sulfur Sulfur Sulfur Benzene Toluene Total Aromatics Benzene Total Olefins Value 24.5 5.3 58.3 0.0057 0.0078 55.76 59.31 0.80 4.92 23.42 0.78 5.3 Parameter Total Aromatics Total Olefins Total Saturates Sulfur Sulfur Sulfur Sulfur Benzene Toluene Total Aromatics Benzene Total Olefins Method D-1319 D-1319 D-1319 D-2622 D-4294 D-5453 D-6344 D-5769 D-5769 D-5769 D-6277 D-6550 Conc. Vol.% Vol.% Vol.% Wt.% Wt.% µg/g µg/g Vol.% Vol.% Vol.% Vol.% Vol.% Method D-1319 D-1319 D-1319 D-2622 D-4294 D-5453 D-6344 D-5769 D-5769 D-5769 D-6277 D-6550 Value 34.6 12.4 62.8 0.0338 0.0368 317.36 338.78 0.55 5.53 32.51 0.52 12.4 Conc. Vol.% Vol.% Vol.% Wt.% Wt.% µg/g µg/g Vol.% Vol.% Vol.% Vol.% Vol.% AccuPetroTest Sulfur in Diesel Fuel QC Standard SBPT-SDF $ 25 / 2 x 15 mL Parameter Sulfur Approx. Range 20 - 11000 µg/g See ASTM Methods D-2622, D-3120, D-3246-92, D-4294, D-5453 for Sulfur Calibration Standards Sulfur in White Mineral Oil QC Standard SBPT-SWMO $ 25 / 2 x 15 mL Parameter Sulfur Approx. Range 20 - 11000 µg/g See ASTM Methods D-2622, D-3120, D-3246-92, D-4294, D-5453 for Sulfur Calibration Standards AccuPetroTest Gasoline Low Sulfur QC Sample Olefin QC Sample SBPT-LSGAS SBPT-OLEFINSFC Parameter Sulfur $ 25 / 2 x 15 mL Method D-5453 Approx. Range 0 - 50 µg/g Parameter Total Olefins Method D-6550 AccuPetroTest Gasoline SBPT-COMP $ 50 / 2 x 15 mL Method D-1319 D-1319 D-1319 D-2622 D-4294 D-5453 D-6344 D-5769 D-5769 D-5769 D-6277 D-6550 Sulfur Single Blind AccuPetroTest Alternative Matrices Standards AccuStandard has manufactured a number of Diesel and White Mineral Oil QC products containing a gravimetrically prepared amount of Sulfur. Use of these alternative matrix materials can provide further evaluation of the QA/QC process in the laboratory. Two samples will be sent for the test parameter and a separate sealed envelope containing the gravimetrically prepared sulfur values is also provided. The second sample is for repeatability testing or for use as a future QA/QC reference. $ 25 / 2 x 15 mL Approx. Range 1 - 40 Vol.% Technical Note Comprehensive Single Blind Gasoline QC Sample Parameter Total Aromatics Total Olefins Total Saturates Sulfur Sulfur Sulfur Sulfur Benzene Toluene Total Aromatics Benzene Total Olefins AccuPetroCheck QC Standards Two of the fuels are available as AccuPetroCheck Consensus Value QC Standards. The AccuPetroCheck CARB and Conventional gasoline reference materials have all parameters listed on the certificate with the Consensus Values and the regression equations for reproducability. Use of these Reference Materials improve the quality of laboratory results. The Consensus Values listed reflect initial statistical treatment of the data at the time the catalog was published. The actual certificate provided with the AccuPetroCheck QC standard will have the accepted Consensus Value based on statistical treatment of the data. Approx. Range 8 - 60 1 - 40 30 - 80 0.0001 - 0.0930 0.0016 - 0.0930 0.5 -500 1.0 - 1000 0.1 - 2.0 1.0 - 15 8 - 60 0.1 - 2.0 1 - 40 Conc. Vol.% Vol.% Vol.% Wt.% Wt.% µg/g µg/g Vol.% Vol.% Vol.% Vol.% Vol.% This comprehensive single blind gasoline QC sample tests for more parameters from a single sample. The actual gasoline sample will have consensus values listed on the datasheet that fall within the range listed for each parameter. Quality Control Standards continue on next page Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 1 QC In cooperation with ASTM D-02 subcommittee 3 and 4, AccuStandard ampulled 21 Real World gasoline reference fuels. Consensus Values have been determined for these reference fuels by various ASTM Round Robins to provide Petrochemical Laboratories with a source of well characterized gasoline standards for use in QA/QC applications and as Single Blind test samples over an extended period of time. As new ASTM D-02.03 and D-02.04 Test methods are promulgated they require mandatory Quality Control testing of real world samples. AccuStandard’s PetroTest & PetroCheck standards are being successfully used to achieve these new Quality Control requirements. Quality Control Standards ASTM Round Robin & PT Samples QC QC AccuPetroTest Gasoline QC Olefins QC Sample SBPT-OLEFIN Sulfur QC Sample $ 25 / 2 x 15 mL Parameter Total Aromatics Total Olefins Total Saturates Method D-1319 D-1319 D-1319 Approx. Range 8-60 Vol.% 1 - 40 Vol.% 30-80 Vol. % See ASTM Method D-1319 for Sulfur Calibration Standards Aromatics QC Sample SBPT-AROM Method D-5769 Parameter Sulfur Sulfur Sulfur Sulfur $ 25 / 2 x 15 mL Method D-2622 D-4294 D-5453 D-6344 Approx. Range 0.0001 - 0.0930 Wt.% 0.0016 - 0.0930 Wt.% 4.0 - 500 µg/g 1.0 - 1000 µg/g See ASTM Methods D-2622, D-3120, D-3246-92, D-4294, D-5453 for Sulfur Calibration Standards Benzene/Toluene QC Sample $ 25 / 2 x 15 mL Parameter Total Aromatics SBPT-SGAS Approx. Range 8 - 60 Vol.% See ASTM Methods, D-3606, D-5580-95, D-5769-95 for Benzene Calibration Standards SBPT-BENZ Parameter Benzene Toluene $ 25 / 2 x 15 mL Method D-5769 D-5769 AccuPetroTest Single Blind Standards Petrochemical laboratories looking to test the performance of the laboratory for a specific parameter can order the Single Blind AccuPetroTest sample for the parameter of interest. Two real world gasoline samples will be sent for the test parameter requested and a separate sealed envelope containing the determined Consensus Value is also provided. The second sample is for repeatability testing or as a future QA/QC reference. Approx. Range 0.1 - 2.0 Vol.% 1.0 - 15 Vol.% See ASTM Methods, D-3606, D-5580-95, D-5769-95 for Benzene Calibration Standards Conducting a Petrochemical Round Robin for a new ASTM method? Select AccuStandard to prepare the necessary samples for the Round Robin study AccuStandard has packaged for ASTM committee D-02 various select groups of gasoline fuels and hydrocarbon products for use in various Round Robin studies. Large Sample Offering AccuStandard was selected by ASTM committee D-02 to fill, seal and package an initial set of 21 different types of Round Robin Gasolines. Each gasoline was selected due to its unique properties. These unique properties will be determined by various ASTM methods under evaluation through ASTM subcommittees. AccuStandard has expanded this offering with additional materials blended for other ASTM Round Robins. Flexibility Use the original 21 gasoline samples to conduct a Round Robin and we can label the samples appropriately to protect the integrity of the Round Robin. In addition, we can easily add additional samples to your specific Round Robin study to expand the scope of the method for different matrices, concentrations or instrument types. NEW Petro PT Samples Oxygenate PT Sample With MtBE contamination problems in drinking water, numerous states are now requiring certification for Oxygenate monitoring. Join AccuStandard’s next study for Oxygenate analysis. Our timely PT schedule easily allows your lab to be proactive in new regulatory requirements. The analytes in the standard and the PT sample have been drawn from the California list of known prevalent oxygenates in gasoline. These new Oxygenate PT samples and standards allow your Lab to: • Eliminate standard preparation • Easily combine with other AccuStandard Volatile standards • Expand testing capabilities • Generate new testing revenue WS-PT Oxygenates * * * OPE-OXY-001-AS OPE-OXY-001-AT OPE-OXY-001-AV Sample conc. after prep 5.0-50 µg/L Contains 4 analytes listed below ETBE Diisopropylether $ 47 / 2 mL $ 47 / 2 mL $ 47 / 2 mL Suggested Calibration Standard Oxygenate Gasoline Additive Standard MtBE ETBE Isopropyl ether 2 NEW (2000 µg/mL) (2000 µg/mL) (2000 µg/mL) * * * IPE-OILG-001-AS IPE-OILG-001-AT IPE-OILG-001-AV Sample conc. after prep Contains 2 analytes listed below Analyte List Total Oil & Grease † TPH Sample range 5-100 mg/L 5-100 mg/L $ 32 / 5 mL $ 32 / 5 mL $ 32 / 5 mL * Designed for NELAC/CA † Indicates that theses analytes are included in the NVLAP Scope of Accreditation, Lab Code 200389-0 Technical Note This PT sample can be used by gravimetric oil and grease methods. In addition, it can also be used for TPH analysis by gravimetric methods including the EPA method 1664. The sample contains real world material commonly found at petroleum containment sites. Suggested Calibration Standard MTBE TAME OGAD-001 OGAD-001-PAK At stated conc. in MeOH WP-PT Oil, Grease & TPH $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 5 comps. TAME t-Butanol (2000 µg/mL) (10000 µg/mL) Oil and Grease WC-OILG-10X-1 1000 µg/mL Total Oil and Grease in n-Propanol $ 45 / 100 mL Contains 500 µg/mL vegetable oil and 500 µg/mL of petroleum oil. Shake well before use. SUFFIX KEY "AS" = Formal PT Study "AT" = Pre-Test "AV" = Values Included Lab Code 200389-0 Quality System is Certified to comply with the International ISO 9001 Quality Standard Physical Properties Method 56, 92, 93 86 445 Member QC ASTM D-56, D-92, D-93 Flash Point Standards Verified by consensus analysis using ASTM Method # referenced ASTM # PMCC D93 PMCC D93 COC D92 COC D92 Nominal Flash Point 65°C 93°C 200°C 230°C Price / Unit $ 110 110 110 110 / / / / 250 250 250 250 ASTM Cat. No. ASTM-P-132-01 ASTM-P-132-02 ASTM-P-132-03 ASTM-P-132-04 Originally designed for ASTM D-56-98a, D-92-98a, D-93-99b mL mL mL mL Certified Flash Point Standards The reference material is a stable, pure hydrocarbon with a method specific flash point determined by an inter-laboratory study using the ASTM Method # referenced. Cat. No. ASTM # ASTM-P-133-01 ASTM-P-133-02 ASTM-P-133-03 ASTM-P-133-04 PMCC D93 PMCC D93 COC D92 TCC D56 ASTM D-86 Nominal Flash Point 65°C 134°C 138°C 67°C Price / Unit $ 175 130 130 175 / / / / 250 250 250 250 mL mL mL mL Synthetic Distillation Standard The automatic distillation apparatus duplicates the distillation conditions of the manual method. The increased reliance on electronic control requires an independent standard to verify that the apparatus is performing correctly. This synthetic blend of hydrocarbons boil in the temperature range specified in ASTM D-86 distillation groups 1 and 2, and a fuel oil that meets the group 4 criteria. The group 1 and 2 standards cover the boiling range 129 - 368 °F (54 - 187 °C) and are verified by consensus analysis with twelve refinery laboratories. The group 4 standard covers the range from 410 670 °F (210 - 355 °C). Products are packaged in convenient sizes to meet your laboratory sample analysis demands. Cat. No. Group Description ASTM-P-126-01 ASTM-P-126-SET 1, 2 1, 2 Synthetic Distillation Standard Synthetic Distillation Standard ASTM-P-127-01 ASTM-P-127-02 4 4 Distillation Standard Distillation Standard ASTM D-92 & ASTM D-93 Price / Unit $ 160 / 500 mL 290 / 2 x 500 mL Originally designed for ASTM D-86-99a 160 / 250 mL 290 / 500 mL Flash & Fire Points by Cleveland Open Cup (COC) & Flash Point by Pensky Martin Closed Cup (PMCC) See Method D-56 on this page for the comprehensive line of flash point standards ASTM D-445 Viscosity Calibration Standards Cat. No. Viscosity @ 40 °C ASTM-P-128-01 ASTM-P-128-02 ASTM-P-128-03 ASTM-P-128-04 ASTM-P-128-05 ASTM-P-128-06 4 7 19 61 180 520 Cst Cst Cst Cst Cst Cst Price / Unit $ 60 60 60 60 60 60 / / / / / / 500 500 500 500 500 500 mL mL mL mL mL mL Originally designed for ASTM D-445-97 Standards of Interest Technical Note Oils are tested in accordance with ASTM D-445 Also see Cloud Point Standards used for ASTM Method D-2500 on page 5 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 3 Method Physical Properties 611 1015 1319 Member ASTM ASTM D-611 (Reapproved 1998) Technical Note Aniline Point Standards The accuracy of automated aniline point apparatus can be verified using a range of standards whose aniline points are determined using ASTM D-611 (Method A) and ASTM D-611 (Method E). Standards are packaged in 20 mL ampules in an inert atmosphere. Cat. No. Nominal Aniline Point D-611-SET D-611-01 D-611-02 D-611-03 D-611-04 D-611-05 Set include 5 Standards listed below Aniline Point Verification Set Method 611(A) 0°C 30°C 55°C 68°C 94°C Cat. No. Nominal Aniline Point D-611E-SET Set include 3 Standards listed below Aniline Point Verification Set Method 611(E) 43°C 62°C 77°C $ 90 / 3 x 20 mL ASTM-P-134-PAK Pure Aniline $ 30 / 5 x 15 mL ASTM D-1015 Freezing Points of High Purity Hydrocarbons D-611E-01 D-611E-02 D-611E-03 Price / Unit $ 90 / 5 x 20 mL 20 20 20 20 20 For routine purposes pure Aniline is packaged in ampules under dry nitrogen. This minimizes the risk of oxidation. Originally designed for D-611-82 mL mL mL mL mL Price / Unit 20 mL 20 mL 20 mL Cat. No. Price / Unit See Method D-2386 page 5 for AccuStandard’s new line of Freezing Point Standards Technical Note ASTM D-1319 Calibration Standards by Fluorescent Indicator Adsorption FIA Originally designed for D-1319-99 Olefin FIA Calibration Curve FIA-CAL-SET $ 300 / Set of 7 x 1 mL Std. 1 Target Vol. % Total Olefins Total Paraffins Total Aromatics Total Oxygenate 2.0 57.0 23.0 18.0 Std. 2 Vol. % Std. 3 Vol. % Std. 4 Vol. % Std. 5 Vol. % Std. 6 Vol. % Std. 7 Vol. % 4.0 55.0 24.0 17.0 5.0 52.0 25.0 18.0 6.0 51.0 26.0 17.0 8.0 45.0 29.0 18.0 10.0 45.0 28.0 17.0 12.0 40.0 30.0 18.0 FIA Paraffin Standard FIA Olefin Standard FIA-PAR FIA-PAR-5ML FIA-OLE FIA-OLE-5ML n-Pentane n-Hexane Cyclohexane n-Heptane Vol. % 8 9 15 14 $ 30 / 1 x 1 mL SAVE 33% $ 100 / 1 x 5 mL 8 comps. Vol. % 2,3-Dimethylpentane 14 Isooctane 16 n-Octane 14 n-Decane 7 mix ratio Benzene 4 Toluene 32 Ethylbenzene 8 p-Xylene 8 o-Xylene 8 4 $ 40 / 1 x 1 mL SAVE 40% $ 120 / 1 x 5 mL 3 comps. 1-Pentene 2,3-Dimethyl-2-butene Vol. % 33.3 33.3 1-Heptene Vol. % 33.3 Standards of Interest For the mandatory real world QC samples stipulated in the Method, see page 1-2 FIA Aromatic Standard FIA-ARO FIA-ARO-5ML D-1319 Meets es EPA Guidelin for RFG Analysis $ 30 / 1 x 1 mL SAVE 33% $ 100 / 1 x 5 mL 10 comps. mix ratio m-Xylene 16 1,2,4-Trimethylbenzene 8 1,3,5-Trimethylbenzene 8 1,2,4,5-Tetramethylbenzene 4 Naphthalene 4 The following set of standards have been prepared for the determination of Aromatics, Olefins, Oxygenates and Saturates in petroleum fractions by Fluorescent Indicator Adsorption (FIA) IP designation 156/95. The final certificate for the FIA calibration curve lists not only the volume percents for the hydrocarbon types, but also the individual volume percents for each analyte in the functional group. To further assist the Petrochemist, the weight fraction for each hydrocarbon type and individual analyte is listed on the final certificate. By providing the individual weights the Petrochemical chemist can use the FIA standards for other types of instrumentation measuring these Petroleum fractions. Quality System is Certified to comply with the International ISO 9001 Quality Standard Physical Properties Method Member 17446304 2386 2500 ASTM D-1744, E-1064, D-4377 Water in Liquid Petroleum Products by D-4928, D-6304 Karl Fischer Cat. No. Description KF-0.6X-5ML-VAP Water content 60 µg/g $ 65 / 10 x 5 mL KF-1X-2ML-VAP KF-1X-5ML-VAP KF-1X-20ML-PAK Water content 100 µg/g Water content 100 µg/g Water content 100 µg/g 40 / 10 x 2 mL 45 / 10 x 5 mL 50 / 5 x 20 mL KF-10X-2ML-VAP KF-10X-5ML-VAP KF-10X-20ML-PAK Water content 1000 µg/g Water content 1000 µg/g Water content 1000 µg/g 40 / 10 x 2 mL 45 / 10 x 5 mL 50 / 5 x 20 mL KF-50X-2ML-VAP KF-50X-5ML-VAP KF-50X-20ML-PAK Water content 5000 µg/g Water content 5000 µg/g Water content 5000 µg/g 40 / 10 x 2 mL 45 / 10 x 5 mL 50 / 5 x 20 mL ASTM D-2386 Cat. No. ASTM D-2500 Cat. No. - 50 °C - 45 °C Price / Unit $ 110 / 250 mL 110 / 250 mL Originally designed for D-2386-97 Technical Note Verified by consensus analysis by ASTM Method D-2386 Cloud Point Calibration Standards Cloud Point, Approx. Value ASTM-P-131-01 ASTM-P-131-02 ASTM-P-131-03 ASTM-P-131-04 ASTM-P-131-05 Value Added Paks (Cat. No.’s ending in -VAP) provide multiple single units packaged together for both greater stability and cost savings. Freezing Point Calibration Standards Nominal Freezing Point ASTM-P-129-01 ASTM-P-129-02 Price / Unit Technical Note Many ASTM Petrochemical methods and specifications reference using QA/QC standards for water content measurements. AccuStandard has formulated a comprehensive range of water standards packaged in convenient sizes to meet the various referenced methods. + 5 °C - 2 °C - 10 °C - 15 °C - 20 °C Technical Note Price / Unit $ 110 110 110 110 110 / / / / / 250 250 250 250 250 mL mL mL mL mL Originally designed for D-2500-00 Verified by consensus analysis by ASTM Method D-2500 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 5 ASTM Standards are available for coulometric Karl Fischer titrations and are packaged in 2 mL, 5 mL, and 20 mL ampules in sets of 5 and 10. The following concentrations are available: ASTM Methods for Sulfur Analysis Sulfur Standards SULFUR ASTM D-2622-98, D-3120-96, D-3246-96, D-4294-98, D-5453-00, D-6334-98, D-6445-99 & Proposed ASTM Sulfur Methods AccuStandard offers the Petroleum Industry the most complete line of calibration standards designed for today’s Proposed & Promulgated test methods for Sulfur analysis. These calibration standards are designed specifically for the analysis of Sulfur in a wide variety of matrices such as #2 diesel fuel, white mineral oil, kerosene, gasoline, crude oil & residual oil. Traceability, Quality and Certification All Sulfur standards are manufactured from the highest quality raw materials, including well characterized starting materials & the lowest sulfur matrices available from the Petrochemical market. All standards are manufactured on a weight/weight basis using balances that are calibrated and verified daily against reference mass standards directly traceable to NIST under test No. 822/254480. The concentration of these working level Sulfur standards have established traceability links to NIST SRM’s where available. Convenient Packaging Since applicable concentration ranges will vary based on the instrumentation used & the nature of the sample the standards can be ordered as complete sets, individual bottles, or Ready-to-Aspirate AccuShots. AccuShots... Packaged to improve analytical standard integrity AccuStandard is the first standard manufacturer to provide sulfur standards in convenient and Ready-to-Aspirate AccuShot 20 mL sealed ampules. Each 20 mL AccuShot provides the necessary material for calibration curve development or daily QA/QC. By purchasing AccuShots the analytical chemist can open a fresh shot for each analysis which eliminates opening and pipetting repeatedly from a stock bottle. This minimizes contamination and evaporation. These ship with no haz fee for additional savings. ASTM D-5453 Test to Low ppb Sulfur Contact us for a copy of the Southwest Research Institute D-5453 Fitness for Use Report Low Sulfur Standards on following pages 6 Quality System is Certified to comply with the International ISO 9001 Quality Standard Analytical Capabilities MWD XRF Sulfur Analyzer in Diesel and Gasoline Fuels Limits of Detection < 1 ppm Fast and easy sample preparation. SULFUR Typical measurement time: 300 sec. Dynamic range: 0-1000 ppm in one calibration. No sample conversion or reagents required. Exceptional signal-to-background provides high sensitivity for low-level sulfur fuels X-Ray Optical Systems, Inc. 15 Tech Valley Drive East Greenbush, NY 12061 Tel. 518-880-1500 website: www.xos.com SULFUR ANALYSIS IN XOS SINDIE Analyzer X-Ray optics enable detection capability well beyond traditional XRF techniques. The same Monochromatic WD XRF technology of the SINDIE bench-top sulfur analyzer is available in an on-line sulfur analyzer. ULTRA LOW SULFUR FUELS Repeatability: 1 ppm 10 ppm 100 ppm 500 ppm 0.5 1.7 5.3 11.7 ppm ppm ppm ppm Monochromatic WDXRF Technology 7 Sulfur Sulfur Standards in Mineral Oil Diesel Fuel ASTM Methods Sulfur Standards for ASTM D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 & Proposed ASTM Sulfur Methods ASTM ASTM Methods Sulfur in Mineral Oil Sulfur in Heavy Weight Mineral Oil (75 cSt) SULFUR Concentration µg/g Blank 100 200 300 400 500 750 1,000 1,500 2,000 3,000 4,000 5,000 7,000 10,000 15,000 20,000 30,000 40,000 50,000 60,000 Wt. % 0.000 0.010 0.020 0.030 0.040 0.050 0.075 0.10 0.15 0.20 0.30 0.40 0.50 0.70 1.00 1.50 2.00 3.00 4.00 5.00 6.00 Set of above Cat. No.’s Sulfur in White Mineral Oil Ready-to-Use Sulfur AccuShots Cat. No. SWMO-BL-4 SWMO-1X-4 SWMO-2X-4 SWMO-3X-4 SWMO-4X-4 SWMO-5X-4 SWMO-7.5X-4 SWMO-10X-4 SWMO-15X-4 -------------------SWMO-30X-4 -------------------SWMO-50X-4 SWMO-70X-4 SWMO-100X-4 SWMO-150X-4 SWMO-200X-4 SWMO-300X-4 SWMO-400X-4 SWMO-500X-4 SWMO-600X-4 Cat. No. SWMO-BL-SHOT SWMO-1X-SHOT SWMO-2X-SHOT SWMO-3X-SHOT SWMO-4X-SHOT SWMO-5X-SHOT SWMO-7.5X-SHOT SWMO-10X-SHOT SWMO-15X-SHOT -------------------------SWMO-30X-SHOT -------------------------SWMO-50X-SHOT SWMO-70X-SHOT SWMO-100X-SHOT SWMO-150X-SHOT SWMO-200X-SHOT SWMO-300X-SHOT SWMO-400X-SHOT SWMO-500X-SHOT SWMO-600X-SHOT µg/g Blank 100 200 300 400 500 750 1,000 1,500 2,000 3,000 4,000 5,000 7,000 10,000 15,000 20,000 30,000 40,000 50,000 60,000 SWMO-CAL-SET-4 19 x 4 oz. $ 850 Each AccuShot product contains 5 x 20 mL ampules at the stated conc. for $ 60 Set of above Cat. No.’s Individual Sulfur 1 -10 units 10 +units Standards 4 oz Bottle $ 55 ea $ 50 ea ASTM Methods Sulfur in #2 Diesel Fuel Concentration µg/g Blank 100 200 300 400 500 750 1,000 1,500 2,000 3,000 4,000 5,000 7,000 10,000 15,000 20,000 30,000 40,000 50,000 60,000 Wt. % 0.000 0.010 0.020 0.030 0.040 0.050 0.075 0.10 0.15 0.20 0.30 0.40 0.50 0.70 1.00 1.50 2.00 3.00 4.00 5.00 6.00 Set of above Cat. No.’s Sulfur in #2 Diesel Fuel Ready-to-Use Sulfur AccuShots Cat. No. SDF-BL-4 SDF-1X-4 SDF-2X-4 SDF-3X-4 SDF-4X-4 SDF-5X-4 SDF-7.5X-4 SDF-10X-4 SDF-15X-4 ------------SDF-30X-4 ------------SDF-50X-4 SDF-70X-4 SDF-100X-4 SDF-150X-4 SDF-200X-4 SDF-300X-4 SDF-400X-4 SDF-500X-4 SDF-600X-4 Cat. No. SDF-BL-SHOT SDF-1X-SHOT SDF-2X-SHOT SDF-3X-SHOT SDF-4X-SHOT SDF-5X-SHOT SDF-7.5X-SHOT SDF-10X-SHOT SDF-15X-SHOT ------------SDF-30X-SHOT ------------SDF-50X-SHOT SDF-70X-SHOT SDF-100X-SHOT SDF-150X-SHOT SDF-200X-SHOT SDF-300X-SHOT SDF-400X-SHOT SDF-500X-SHOT SDF-600X-SHOT SDF-CAL-SET-4 19 x 4 oz. $ 850 Each AccuShot product contains 5 x 20 mL ampules at the stated conc. for $ 60 Individual Sulfur 1 -10 units 10 +units Standards 4 oz Bottle $ 55 ea $ 50 ea Technical Note Sulfur conc. calculated from % sulfur in di-n-butyl sulfide 8 Sulfur in Light Weight Mineral Oil (20 cSt) Concentration Wt. % 0.000 0.010 0.020 0.030 0.040 0.050 0.075 0.10 0.15 0.20 0.30 0.40 0.50 0.70 1.00 1.50 2.00 3.00 4.00 5.00 6.00 Sulfur in White Mineral Oil Ready-to-Use Sulfur AccuShots Cat. No. SWMO-LT-BL-4 SWMO-LT-1X-4 SWMO-LT-2X-4 SWMO-LT-3X-4 SWMO-LT-4X-4 SWMO-LT-5X-4 SWMO-LT-7.5X-4 SWMO-LT-10X-4 SWMO-LT-15X-4 -------------------SWMO-LT-30X-4 -------------------SWMO-LT-50X-4 SWMO-LT-70X-4 SWMO-LT-100X-4 SWMO-LT-150X-4 SWMO-LT-200X-4 SWMO-LT-300X-4 SWMO-LT-400X-4 SWMO-LT-500X-4 SWMO-LT-600X-4 Cat. No. SWMO-LT-BL-SHOT SWMO-LT-1X-SHOT SWMO-LT-2X-SHOT SWMO-LT-3X-SHOT SWMO-LT-4X-SHOT SWMO-LT-5X-SHOT SWMO-LT-7.5X-SHOT SWMO-LT-10X-SHOT SWMO-LT-15X-SHOT -------------------------SWMO-LT-30X-SHOT -------------------------SWMO-LT-50X-SHOT SWMO-LT-70X-SHOT SWMO-LT-100X-SHOT SWMO-LT-150X-SHOT SWMO-LT-200X-SHOT SWMO-LT-300X-SHOT SWMO-LT-400X-SHOT SWMO-LT-500X-SHOT SWMO-LT-600X-SHOT SWMO-LT-CAL-SET-4 19 x 4 oz. $ 850 Each AccuShot product contains 5 x 20 mL ampules at the stated conc. for $ 60 Individual Sulfur 1 -10 units 10 +units Standards 4 oz Bottle $ 55 ea $ 50 ea Ready-to-Use AccuShots... Packaged to improve analytical standard integrity AccuStandard is the first standard manufacturer to provide sulfur standards in convenient and Ready-toAspirate AccuShot 20 mL sealed ampules. Each 20 mL AccuShot provides the necessary material for calibration curve development or daily QA/QC. By purchasing AccuShots the analytical chemist can open a fresh shot for each analysis which eliminates opening and pipetting repeatadly from a stock bottle. This minimizes contamination and evaporation. These ship with no haz fee for additional savings. Cross Reference Table ASTM IP ISO DIN JIS AFNOR sorted by ASTM Method see beginning of Catalog Quality System is Certified to comply with the International ISO 9001 Quality Standard Sulfur Standards Method ASTM SulfurMethods for in Kerosene Sulfur ASTM Methods Sulfur Standards for ASTM D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 & Proposed ASTM Sulfur Methods ASTM Methods Sulfur in Kerosene Ready-to-Use Sulfur AccuShots µg/g Blank 100 200 300 400 500 750 1,000 1,500 2,000 3,000 4,000 5,000 7,000 10,000 15,000 20,000 30,000 40,000 50,000 60,000 Cat. No. SK-BL-4 SK-1X-4 --------------SK-3X-4 --------------SK-5X-4 SK-7.5X-4 SK-10X-4 --------------SK-20X-4 SK-30X-4 SK-40X-4 SK-50X-4 --------------SK-100X-4 --------------SK-200X-4 --------------------------------------------------------- Cat. No. SK-BL-SHOT SK-1X-SHOT SK-CAL-SET-4 12 x 4 oz. $ 500 Each AccuShot product contains 5 x 20 mL ampules at the stated conc. for $ 60 Wt. % 0.000 0.010 0.020 0.030 0.040 0.050 0.075 0.10 0.15 0.20 0.30 0.40 0.50 0.70 1.00 1.50 2.00 3.00 4.00 5.00 6.00 Set of above Cat. No.’s Individual Sulfur 1 -10 units 10 +units Standards 4 oz Bottle $ 55 ea $ 50 ea SK-3X-SHOT SK-5X-SHOT SK-7.5X-SHOT SK-10X-SHOT SK-20X-SHOT SK-30X-SHOT SK-40X-SHOT SK-50X-SHOT SK-100X-SHOT SK-200X-SHOT Concentration Sulfur in Heavy Distillate Kerosene µg/g Blank 100 200 300 400 500 750 1,000 1,500 2,000 3,000 4,000 5,000 7,000 10,000 15,000 20,000 30,000 40,000 50,000 60,000 Cat. No. SK-HD-BL-4 SK-HD-1X-4 SK-HD-2X-4 SK-HD-3X-4 SK-HD-4X-4 SK-HD-5X-4 SK-HD-7.5X-4 SK-HD-10X-4 SK-HD-15X-4 SK-HD-20X-4 SK-HD-30X-4 SK-HD-40X-4 SK-HD-50X-4 SK-HD-70X-4 SK-HD-100X-4 SK-HD-150X-4 SK-HD-200X-4 SK-HD-300X-4 SK-HD-400X-4 SK-HD-500X-4 SK-HD-600X-4 Wt. % 0.000 0.010 0.020 0.030 0.040 0.050 0.075 0.10 0.15 0.20 0.30 0.40 0.50 0.70 1.00 1.50 2.00 3.00 4.00 5.00 6.00 Set of above Cat. No.’s Technical Note Sulfur concentration calculated from % sulfur in di-n-butyl sulfide. Standards of Interest For the mandatory real world QC samples stipulated in the Method, see pages 1- 2. SK-HD-CAL-SET-4 21 x 4 oz. $ 950 Individual Sulfur 1 -10 units 10 +units Standards 4 oz Bottle $ 55 ea $ 50 ea Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 9 SULFUR Concentration Sulfur in Light Distillate Kerosene Sulfur in Heavy Distillate Kerosene ASTM Sulfur in Light Distillate Kerosene ASTM Sulfur Standards 26226445 ASTM Methods ASTM D-2622, D-4294 Sulfur Calibration Standards SULFUR ASTM Sulfur Calibration Standards in Isooctane for Gasoline & Reformulated Gasoline Analysis Standards can be mixed for quantity discounts 1 to 4 units 5 to 10 units more than 10 units Cat. No. STP-BL-4 STP-1X-4 STP-2X-4 STP-3X-4 STP-5X-4 STP-10X-4 STP-20X-4 STP-30X-4 STP-40X-4 STP-60X-4 STP-100X-4 STP-200X-4 STP-300X-4 STP-CAL-SET In Isooctane $ 60 each per Sulfur Standard $ 55 each per Sulfur Standard $ 50 each per Sulfur Standard Sulfur Conc. Blank 10 µg/g 20 µg/g 30 µg/g 50 µg/g 100 µg/g 200 µg/g 300 µg/g 400 µg/g 600 µg/g 1000 µg/g 2000 µg/g 3000 µg/g Low Level Sulfur Calibration Standards Low Level Sulfur Calibration Standards for use on XRF Energy Dispersive or Wavelength Instruments Originally designed for D-2622-98 D-4294-98 Sulfur Wt. % 0.0 0.001 0.002 0.003 0.005 0.010 0.020 0.030 0.040 0.060 0.10 0.20 0.30 ASTM D-2622, D-6334, D-6445 Unit 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. $ 650 / set of 13 x 4 oz. Set contains the above 13 individual bottles Standards can be mixed for quantity discounts 1 to 4 units 5 to 10 units more than 10 units Cat. No. D-2622-LL-BL-4 D-2622-LL-5X-4 D-2622-LL-10X-4 D-2622-LL-30X-4 D-2622-LL-50X-4 D-2622-LL-75X-4 D-2622-LL-100X-4 D-2622-LL-300X-4 D-2622-LL-500X-4 D-2622-LL-1000X-4 $ 60 each per Sulfur Standard $ 55 each per Sulfur Standard $ 50 each per Sulfur Standard Sulfur Conc. Blank 5 µg/g 10 µg/g 30 µg/g 50 µg/g 75 µg/g 100 µg/g 300 µg/g 500 µg/g 1000 µg/g Sulfur Wt. % 0.0 0.0005 0.0010 0.0030 0.0050 0.0075 0.010 0.030 0.050 0.100 Originally designed for D-2622-98 D-6334-98 D-6445-99 Unit 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. 4 oz. D-2622-LL-CAL-SET $ 450 / 10 x 4 oz. In Isooctane : Toluene (3:1) Set contains the above 10 individual bottles Technical Note Technical Note A well characterized di-n-butyl sulfide starting mat’l is used with a low sulfur Isooctane matrix for RFG/gasoline sulfur standards. Well characterized Thiophene & 2-Methyl thiophene are used in a low sulfur Isooctane/Toluene matrix for this calibration set. ASTM D-2622, D-6334, D-6445 ASTM D-3120, D-3246 Sulfur Calibration Set Mid Level Sulfur Calibration Standards Sulfur Calibration Set D-3120-92-CAL-SET In Isooctane Cat. No. D-3120-92-BL D-3120-92-1X D-3120-92-3X D-3120-92-10X D-3120-92-30X D-3120-92-50X D-3120-92-75X D-3120-92-100X $ 75 / set of 8 x 1 mL Sulfur Conc. Blank 1 µg/g 3 µg/g 10 µg/g 30 µg/g 50 µg/g 75 µg/g 100 µg/g Sulfur Wt. % ——— 0.0001 0.0003 0.0010 0.0030 0.0050 0.0075 0.010 Originally designed for D-3120-96 D-3246-96 Technical Note Well characterized di-n-butyl sulfide is used in a low sulfur Isooctane matrix for this calibration set. New Requested Additions for use on XRF Energy Dispersive or Wavelength Instruments Standards can be mixed for quantity discounts 1 to 4 units 5 to 10 units more than 10 units Cat. No. D-2622-LL-200X-4 D-2622-LL-400X-4 D-2622-LL-600X-4 D-2622-LL-700X-4 D-2622-LL-800X-4 D-2622-LL-900X-4 D-2622-LL-1100X-4 D-2622-LL-1200X-4 $ 60 each per Sulfur Standard $ 55 each per Sulfur Standard $ 50 each per Sulfur Standard Sulfur Conc. 200 µg/g 400 µg/g 600 µg/g 700 µg/g 800 µg/g 900 µg/g 1100 µg/g 1200 µg/g Sulfur Wt. % 0.020 0.040 0.060 0.070 0.080 0.090 0.110 0.120 Originally designed for D-2622-98 D-6334-98 D-6445-99 Unit 4 oz 4 oz 4 oz 4 oz 4 oz 4 oz 4 oz 4 oz Technical Note Standards of Interest For the mandatory real world QC samples stipulated in many ASTM Sulfur Methods, see page 1-2 Member 10 Well characterized Thiophene & 2-Methyl thiophene are used in a low sulfur Isooctane/Toluene matrix for this calibration set. AccuStandard is an active member in ASTM and strives to keep abreast of ASTM method revisions. If our listed formulation does not meet the most recent method revision, please contact Technical Support, ext. 117 for an updated product. Quality System is Certified to comply with the International ISO 9001 Quality Standard Sulfur Standards ASTM 2789 ASTM Methods Sulfur Standards for ASTM D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 & Proposed ASTM Sulfur Methods ASTM Methods Sulfur Calibration Standards Sulfur in Crude Oil Standards Sulfur in Residual Oil Standards Concentration Concentration Sulfur in Crude Oil Wt. % 0.10 0.25 0.50 1.00 2.00 3.00 4.00 5.00 µg/g 3,500 7,000 10,000 15,000 20,000 30,000 40,000 Wt. % 0.35 0.70 1.00 1.50 2.00 3.00 4.00 Set of above Cat. No.’s SCO-CAL-SET-4 8 x 4 oz. $ 500 Individual Sulfur 1 -10 units 10 +units Standards 4 oz Bottle $ 75 ea $ 65 ea Cat. No. SRO-35X-4 SRO-70X-4 SRO-100X-4 SRO-150X-4 SRO-200X-4 SRO-300X-4 SRO-400X-4 SULFUR Set of above Cat. No.’s Cat. No. SCO-10X-4 SCO-25X-4 SCO-50X-4 SCO-100X-4 SCO-200X-4 SCO-300X-4 SCO-400X-4 SCO-500X-4 AccuStandard's Technical Service Dept. can provide Ready-to-Inject working level calibration standards to meet unique laboratory applications. Call or fax us your standard requirements. SRO-CAL-SET-4 7 x 4 oz. $ 450 Individual Sulfur 1 -10 units 10 +units Standards 4 oz Bottle $ 75 ea $ 65 ea ASTM Methods Sulfur Standards Total Sulfur in Aromatic Compounds by Hydrogenolysis & Rateometric Colorimetry Trace Quantities of Sulfur in Liquid Aromatic Hydrocarbons by Oxidative Microcoulometry ASTM-P-0010-PAK 1000 µg/mL in Toluene ASTM-P-0020-PAK 1000 µg/mL in Xylenes $ 75 / 5 x 1 mL Sulfur (as Thiophene) $ 75 / 5 x 1 mL Sulfur (as Dibenzothiophene) ASTM-SSTD-A/B-SET $ 100 / 10 x 2 mL The set contains the following 10 standards in isooctane Cat. No. Description ASTM-SSTDA-BL ASTM-SSTDA-01 ASTM-SSTDA-02 ASTM-SSTDA-03 ASTM-SSTDA-04 Sulfur Sulfur Sulfur Sulfur Sulfur Blank @ 0.5 @ 1.0 @ 2.5 @ 5.0 Unit ASTM-SSTDB-BL ASTM-SSTDB-04 ASTM-SSTDB-05 ASTM-SSTDB-06 ASTM-SSTDB-07 Sulfur Sulfur Sulfur Sulfur Sulfur Blank @ 5.0 µg/g in Isooctane @ 10.0 µg/g in Isooctane @ 25.0 µg/g in Isooctane @ 50.0 µg/g in Isooctane µg/g µg/g µg/g µg/g in in in in Isooctane Isooctane Isooctane Isooctane 2 2 2 2 2 mL mL mL mL mL 2 2 2 2 2 mL mL mL mL mL Technical Note ASTM D-2789 Hydrocarbon Types in Low Olefinic Gas by MS Composition Test Mix D-2789-CTM D-2789-CTM-PAK 2-Methylpentane 2,4-Dimethylpentane n-Octane Methylcyclopentane Methylcyclohexane $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 9 comps. (Vol. %) 7.2 9.4 16.6 7.1 10 cis-1,2-Dimethylcyclohexane Benzene Toluene p-Xylene Originally designed for D-2789-95 ASTM µg/g 1,000 2,500 5,000 10,000 20,000 30,000 40,000 50,000 Sulfur in Crude Oil Technical Note Both the actual volume % ratio and the final weight fractions for each analyte will be listed on the certificate. (Vol. %) 15.5 7.7 10 16.5 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 11 PIANO PIANO, PONA, PNA PIANO PONA PNA AccuStandard has introduced the PIANO line of quantitative and qualitative Petrochemical Standards for class type analysis of petrochemical samples or product streams. PIANO analysis involves the determination of the percentage of the following five fractions Paraffins, Isoparaffins, Aromatics, Naphthenes, and Olefins. PONA analysis involves analyzing the naphtha sample for Paraffins, Olefins, Naphthenes, and Aromatics. If the Isoparaffins and Olefins are not present, the analysis is just for PNA. The PIANO line of standards is used to determine quantitative and qualitative retention times and indices as well as to monitor response factors within the hydrocarbon blend. These complex mixes are prepared from materials of the highest available purity, accurate to four decimal places, and include a detailed data sheet on the formulation composition. The typical range for the analytes in each formulation has been provided for each catalog item. The exact composition on a weight % basis for each analyte has been provided on the certificate, and a disk deliverable spreadsheet is available on request. Mini Inert Valves Seal The PIANO standards are supplied in convenient to use crimp top vials with Viton septa that resist mineral oil, aliphatic, aromatics hydrocarbons, and higher temperatures. Mini inert valve seals are available for an additional $ 25 vial. To order, add “-MIV” to any of the PIANO catalog numbers on this page. PIANO, PONA, PNA Analysis PIANO Mixture High Aromatic PIAN Blend ASTM-P-0030 ASTM-P-0037 PIONA $ 250 / 100 µL 135 comps. The PIANO formulation contains the n-Paraffins, Isoparaffins,Aromatics, Naphthenes, and Olefins from the five Cat. No.’s: ASTM-P-0031, ASTM-P-0032, ASTM-P-0033, ASTM-P-0034, ASTM-P-0035 Approximate weight percentages for the total: n-Paraffins 18.5%, Isoparaffins 17.9%, Aromatics 23.6%, Naphthenes 20.9%, Olefins 19.0%. The actual certificate will list the weight % for all analytes in the formulation. $ 120 / 100 µL 110 comps. High Aromatic blend contains the PIAN components blended to resemble a reformate. The actual certificate will have the exact weight % for each analyte accurate to four decimal places. Analyte list is drawn from Cat. No.’s: ASTM-P-0031, ASTM-P-0032, ASTM-P-0033, ASTM-P-0034 Standards of Interest Low Aromatic PIAN Blend ASTM-P-0036 $ 120 / 100 µL 110 comps. Low Aromatic blend contains the PIAN components blended to resemble a light naphtha. The actual certificate will have the exact weight % for each analyte accurate to four decimal places. Analyte list is drawn from Cat. No.’s: ASTM-P-0031, ASTM-P-0032, ASTM-P-0033, ASTM-P-0034 For individual PIANO descriptions see next page AccuStandard, Your Standards and Technical Information Source! 12 Total Petroleum Hydrocarbon Pattern Recognition Standards Analytical Standards and Reference Material for all 209 PCB Congeners BOOK-TPH S-3571 $ 35 $ 25 Quality System is Certified to comply with the International ISO 9001 Quality Standard PIANO, PONA, PNA PIANO PIANO PONA PNA PIANO, PONA, PNA Analysis PIANO Mix Set ASTM-PIANO-SET $ 700 / 6 x 100 µL Set includes the following Cat. No.: ASTM-P-0030, ASTM-P-0031, ASTM-P-0032, ASTM-P-0033, ASTM-P-0034, ASTM-P-0035 Special Packaging Mini inert valve seals are available for an additional $ 25 / vial. To order, add “-MIV” to any of the PIANO cat.# on this page. PIANO n-Paraffins Mix PIANO Isoparaffins Mix ASTM-P-0031 $ 80 / 100 µL 11 paraffins listed below at varying Wt. % typically in the range from 7.0 to 11.0 Wt. %. The actual certificate will have the exact Wt. % for each analyte. Typ. Wt. % n-Pentane 9.4375 n-Hexane 9.5661 n-Heptanea 9.8048 n-Octane 9.5518 n-Nonane 9.0482 n-Decane 9.2517 n-Undecane 9.3172 n-Dodecane 9.1855 n-Tridecane 8.9332 n-Tetradecane 8.7989 n-Pentadecane 7.1057 ASTM-P-0032 $ 120 / 100 µL 35 Isoparaffins listed below at varying Wt. % typically in the range from 0.5 to 6.0 Wt. %. The actual certificate will have the exact Wt. % for each analyte. Typ. Wt. % Isopentane 2.1928 2,3-Dimethylbutane 0.4466 2-Methylpentane 3.2815 3-Methylpentane 5.3865 2,2-Dimethylpentane 1.7747 2,4-Dimethylpentane 3.6993 2,2,3-Trimethylbutane 3.9291 3,3-Dimethylpentane 1.1848 2-Methylhexane 2.2384 2,3-Dimethylpentane 1.7883 3-Methylhexane 1.6708 3-Ethylpentane 0.5080 PIANO Aromatics Mix PIANO Naphthenes Mix PIANO Olefins Mix ASTM-P-0033 $ 120 / 100 µL 38 Aromatics listed below at varying Wt. % typically in the range from 0.2 to 7.0 Wt. %. The actual certificate will have the exact Wt. % for each analyte. ASTM-P-0034 $ 120 / 100 µL 30 Napthenes listed below at varying Wt. % typically in the range from 0.5 to 8.0 Wt. %. The actual certificate will have the exact Wt. % for each analyte. Typ. Wt. % Cyclopentane 4.9143 Methylcyclopentane 3.2829 Cyclohexane 5.3268 1,1-Dimethylcyclopentane 3.4612 cis-1,3-Dimethylcyclopentane 0.5963 trans-1,2-Dimethylcyclopentane 1.4715 trans-1,3-Dimethylcyclopentane 2.7531 Methylcyclohexane 5.6091 Ethylcyclopentane 3.5534 ctc-1,2,3-Trimethylcyclopentane 1.5859 cct-1,2,4-Trimethylcyclopentane 3.7208 ctc-1,2,4-Trimethylcyclopentane 1.6467 trans-1,4-Dimethylcyclohexane 3.6499 1-Ethyl-1-methylcyclopentane 1.0554 trans-1,2-Dimethylcyclohexane 1.6537 ccc-1,2,3-Trimethylcyclopentane 0.7971 Isopropylcyclopentane 3.5042 cis-1,2-Dimethylcyclohexane 3.7159 n-Propylcyclopentane 3.6438 ccc-1,3,5-Trimethylcyclohexane 3.5263 1,1,4-Trimethylcyclohexane 3.6791 ctt-1,2,4-Trimethylcyclohexane 3.6107 ctc-1,2,4-Trimethylcyclohexane 3.5069 1,1,2-Trimethylcyclohexane 3.3354 Isobutylcyclopentane 3.7123 Isopropylcyclohexane 5.7233 n-Butylcyclopentane 3.6944 Isobutylcyclohexane 5.6729 t-1-Methyl-2-propylcyclohexane 3.8434 t-1-Methyl-2-(4MP)cyclopentane 3.7534 ASTM-P-0035 $ 120 / 100 µL 25 Olefins listed below at varying Wt. % typically in the range from 1.2 to 9.0 Wt. %. The actual certificate will have the exact Wt. % for each analyte. PIANO Mixture Typ. Wt. % 2,3-Dimethylheptane 1.4870 3,4-Dimethylheptane 3.7450 2-Methyloctane 3.7576 3-Methyloctane 5.6020 3,3-Diethylpentane 1.5755 2,2-Dimethyloctane 3.4135 3,3-Dimethyloctane 3.2582 2,3-Dimethyloctane 3.8842 3-Ethyloctane 3.7482 2-Methylnonane 3.7144 3-Methylnonane 5.7687 3-Methyl-1-butene 1-Pentene 2-Methyl-1-butene 2-Methyl-1,3-butadiene trans-2-Pentene cis-2-Pentene 4-Methylpentene-1 1-Hexene trans-2-Hexene 2-Methylpentene-2 cis-2-Hexene 1-Heptene trans-3-Heptene cis-3-Heptene trans-2-Heptene cis-2-Heptene 1-Octene trans-2-Octene cis-2-Octene 1-Nonene trans-3-Nonene cis-3-Nonene trans-2-Nonene cis-2-Nonene 1-Decene PIONA Typ. Wt. % Benzene 7.1437 Toluene 4.5738 EthylBenzene 6.7670 m-Xylene 2.2259 p-Xylene 4.4815 o-Xylene 2.2519 Isopropylbenzene 2.2248 n-Propylbenzene 4.4979 1-Methyl-3-ethylbenzene 2.2243 1-Methyl-4-ethylbenzene 2.2206 1,3,5-Trimethylbenzene 1.1076 1-Methyl-2-ethylbenzene 2.2611 1,2,4-Trimethylbenzene 2.2535 tert-Butylbenzene 4.5310 Isobutylbenzene 4.4216 sec-Butylbenzene 2.2368 1-Methyl-3-isopropylbenzene 1.1066 1-Methyl-4-isopropylbenzene 1.0668 1-Methyl-2-isopropylbenzene 1.1241 1-Methyl-3-n-propylbenzene 2.1135 1-Methyl-4-n-propylbenzene 2.2336 n-Butylbenzene 2.2087 1,2-Diethylbenzene 1.0947 1-Methyl-2-n-propylbenzene 2.2641 1,4-Dimethyl-2-ethylbenzene 2.2803 1,3-Dimethyl-5-ethylbenzene 2.2858 1,2-Dimethyl-4-ethylbenzene 2.2558 1,3-Dimethyl-2-ethylbenzene 1.1416 1,2-Dimethyl-3-ethylbenzene 2.1864 1,2,4,5-Tetramethylbenzene 0.2360 2-Methylbutylbenzene 1.1453 trans-1-Butyl-2-methylbenzene 0.7641 n-Pentylbenzene 4.4828 t-1-Butyl,3,5-dimethylbenzene 2.1641 t-1-butyl-ethylbenzene 2.2322 1,3,5-Triethylbenzene 4.5671 1,2,4-Triethylbenzene 1.1087 n-Hexylbenzene 4.5029 Typ. Wt. % 2,2-Dimethylhexane 1.3061 2,5-Dimethyl hexane 3.6975 2,2,3-Trimethylpentane 1.7371 2,4-Dimethylhexane 1.6252 2,3-Dimethylhexane 1.6212 2-Methylheptane 4.4073 4-Methylheptane 3.2015 3-Methylheptane 5.5186 3-Ethylhexane 0.6999 3,3-Dimethylheptane 1.7011 2,5-Dimethylheptane 5.6731 3,5-Dimethylheptane 0.7565 Typ. Wt. % 1.9396 4.1355 1.4440 2.3889 1.8034 1.9792 3.4372 7.0484 1.7302 3.3901 3.8765 7.6134 3.3469 5.8657 3.7217 5.7679 7.6901 1.9432 3.9502 7.6425 1.9972 4.0042 1.9848 2.7952 8.2053 Production Note AccuStandard may add and/or subtract PIANO Analytes and vary the weight % for each Analyte. The certificate will reflect the exact Analyte composition. ASTM-P-0030 $ 250 / 100 µL (135 comps.) The PIANO formulation contains the n-Paraffins, Isoparaffins,Aromatics, Naphthenes, and Olefins from the Five Cat. No.’s: ASTM-P-0031, ASTM-P-0032, ASTM-P-0033, ASTM-P-0034, ASTM-P-0035 Approximate weight %’s for the total: n-Paraffins 18.5%, Isoparaffins 17.9%, Aromatics 23.6%, Naphthenes 20.9%, Olefins 19.0%. The certificate lists the weight % for all analytes in the formulation. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 13 Method Detailed Hydrocarbon Analysis 2887 DHA Member ASTM Detailed Hydrocarbon Analysis DHA - PONA-VI (PONA 6) is a qualitative mixture of various gasoline and refinery materials prepared to provide nearly every component that may be encountered in feedstock and finished gasolines. Some oxygenates have been added to allow this blend to be used for DHA method setup. This blend contains approximately 450 components (peaks). Proposed ASTM Method for Detailed Hydrocarbon Analysis (DHA) Determination of Individual Components and Groups of Components in Spark Ignition Engine fuels by High Efficiency Open Tubular Column Gas Chromatography (Detailed Hydrocarbon Analysis) Detailed Hydrocarbon Analysis (includes oxygenates) ASTM-P-0038 $ 120 / 100 µL 30 Analytes listed below at varying targeted weight %. The actual certificate will has the exact Wt. % for each analyte. Ethanol Pentane 2-Methyl-2-propanol 2-Methylbutene 2,3-Dimethylbutane Methyl-t-butyl ether Hexane Methylcyclopentene Benzene Cyclohexane 3-Ethylpentane t-1,2-Dimethylcyclopentane Heptane 2,2,3-Trimethylpentane 2,3,3-Trimethylpentane Toluene p-Xylene Ethylbenzene Octane 2,3-Dimethylheptane Nonane 5-Methylnonane 1-Ethyl-2-methylbenzene Decane Undecane 1,2,3,5-Tetramethylbenzene Naphthalene Dodecane 1-Methylnaphthalene Tridecane ASTM-P-0139 $ 120 / 100 µL ASTM D-2887 Boiling Range Distribution of Petroleum Fractions by GC Calibration Mix DRH-002N DRH-002N-10X Wt. % n-Hexane 6 n-Heptane 6 n-Octane 8 n-Nonane 8 n-Decane 12 n-Undecane 12 n-Dodecane 12 n-Tetradecane 12 n-Hexadecane 10 $ 10 / 100 mg $ 40 / 1 gm 17 comps. Wt. n-Octadecane n-Eicosane n-Tetracosane n-Octacosane n-Dotriacontane n-Hexatriacontane n-Tetracontane n-Tetratetracontane % 5 2 2 1 1 1 1 1 n-Hexadecane $ 10 / 1 x 1 mL 2 comps. n-Octadecane Heptadecane Octadecane Phytane (2,6,10,14-Tetramethylhexadecane) Pristane (2,6,10,14-Tetramethylpentadecane) DRH-008S-R2 $ 65 / 1 x 1 mL DRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL 500 µg/mL each in Chloroform 35 comps. D-2887-REFOIL NEW Calibration Solution * µg/mL 600 600 800 800 1200 1200 1200 1200 1000 ASTM D-2887 Reference Gas Oil Sample Lot #2 Nonadecane Phytane Eicosane Heneicosane Docosane Tricosane Tetracosane Pentacosane Hexacosane Heptacosane Octacosane Nonacosane $ 35 / 1 x 1 mL Technical Note Triacontane n-Hentriacontane Dotriacontane Tritriacontane Tetratriacontane Pentatriacontane Hexatriacontane Heptatriacontane Octatriacontane Nonatriacontane Tetracontane This sample is a petroleum fraction having a boiling range from 250°F to 850°F, evaluated in round robin studies by the ASTM D-02 committee. Use of this sample and the supplied ASTM boiling range consensus values helps to evaluate system performance AccuStandard offers a hydrocarbon window defining standard with the C8 to C40 odd and even Alkanes. As an added benefit, AccuStandard included pristane and phytane in the formulation. Use of this one standard measuring the C17/ pristane and C18/ phytane ratio can be used to estimate degradation of fuel oil. If you prefer, AccuStandard has also developed a fuel oil degradation mixture containing just the four required analytes to determine the C17/pristane and C8/ phytane ratio Catalog Numbers DRH-005S-10X. DRH-005S-10X $ 20 / 1 x 1 mL 2.0 mg/mL each in CH2Cl2 : CS2 (1:1) 4 comps. n-Hexane n-Heptane n-Octane n-Nonane n-Decane n-Undecane n-Dodecane n-Tetradecane n-Hexadecane Hydrocarbon Window Defining Standard* Technical Note Fuel Oil Degradation/Retention Time Mix for Quantification of C17/Pristane & C18/Phytane ratios DRH-002S-R1 DRH-002S-R1-PAK At stated conc. in Chloroform Originally designed for D-2887-99 Octane Nonane Decane Undecane Dodecane Tridecane Tetradecane Pentadecane Hexadecane Heptadecane Octadecane Pristane Column Test Mixture ASTM-D2887 1% v/v in n-Octane Complete Hydrocarbon Analysis $ 50 / 1 x 1 mL SAVE 20% $ 200 / 5 x 1 mL 17 comps. n-Octadecane n-Eicosane n-Tetracosane n-Octacosane n-Dotriacontane n-Hexatriacontane n-Tetracontane n-Tetratetracontane µg/mL 500 200 200 100 100 100 100 100 NEW Calibration Solution * DRH-002S-R2 DRH-002S-R2-PAK 1 % Wt./Wt. each in Chloroform n-Tetratetracontane n-Tetracontane n-Hexatriacontane n-Dotriacontane n-Octacosane n-Tetracosane n-Eicosane $ 50 / 1 x 1 gm SAVE 20% $ 200 / 5 x 1 gm 20 comps. n-Octadecane n-Hexadecane n-Tetradecane n-Dodecane n-Undecane n-Decane n-Nonane n-Octane n-Heptane n-Hexane n-Pentane n-Pentadecane n-Heptadecane * Can be shipped by Air and Sea 14 Quality System is Certified to comply with the International ISO 9001 Quality Standard Petrochemical Standards Method SIM DIS Member SIM DIS Standards Simulated Distillation Stock SIM DIS Paraffin Solution ASTM-P-0050 $ 85 / 1 x 5 mL 14 comps. Wt. % n-Pentane 6.66 n-Hexane 6.66 n-Heptane 6.66 n-Octane 6.66 n-Nonane 6.66 n-Decane 6.66 n-Undecane 6.66 Wt. % n-Dodecane 13.33 n-Tetradecane 6.66 n-Pentadecane 6.66 n-Hexadecane 6.66 n-Heptadecane 6.66 n-Octadecane 6.66 n-Eicosane 6.66 $ 20 / 2 grams n-Pentane n-Hexane n-Heptane n-Octane n-Nonane n-Decane n-Undecane n-Dodecane Wt. % 0.0333 0.0333 0.0333 0.0333 0.0333 0.0333 0.0333 0.0666 n-Tetradecane n-Pentadecane n-Hexadecane n-Heptadecane n-Octadecane n-Eicosane Polywax 500 ASTM-P-0137N-2G $ 20 / 2 grams AccuStandard designed the following formulations for a Proposed ASTM Method under development for Motor Oil Volatility analysis & SIM DIS applications. Polywax 1000® Polywax 655® ASTM-P-0053N-2G Wt. % 0.0333 0.0333 0.0333 0.0333 0.0333 0.0333 0.5 Standards of Interest See ASTM Methods D-3710, D-5307, D-5442, D-6352 for additional calibration standards for hydrocarbon analysis. Technical Note Polywax 850 Polywax 500 Polywax 655 ASTM-P-0052 $ 40 / 1 x 1 mL ASTM-P-0052-PAK SAVE 20% $ 160 / 5 x 1 mL At stated conc. in Carbon disulfide 15 comps. Polywax 850® Polywax 500® ASTM-P-0051N-2G Working Level SIM DIS Paraffin Solution with Polywax 500 $ 20 / 2 grams ASTM-P-0138N-2G $ 20 / 2 grams Polywax 1000 For our complete line of Organic Standards, request a copy of our Organic Catalog For our complete line of Inorganic Standards, request a copy of our Inorganics Catalog Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 15 ASTM Simulated Distillation (SIM DIS) and Proposed Motor Oil Volatility Method AccuStandard has developed an extensive line of SIM DIS standards for normal and high temperature analytical requirements when generating boiling point versus retention time calibration curves. Since normal paraffins above Alkane C60 are not readily available, Polywax 500, Polywax 655, Polywax 850 and Polywax 1000 standards have been incorporated to perform SIM DIS analysis of heavy petroleum fractions with boiling points up to 1350 °F. If you require additional analytes added to the formulations for extended SIM DIS work, use our custom quotation request form located in the back of the catalog. Method ASTM Standards 3120 3230 3231 3237 , Member ASTM D-3120 & D-3246 Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulometry Originally designed for D-3120-96 D-3246-96 ASTM Sulfur Calibration Set D-3120-92-CAL-SET In Isooctane Cat. No. D-3120-BL D-3120-92-1X D-3120-92-3X D-3120-92-10X D-3120-92-30X D-3120-92-50X D-3120-92-75X D-3120-92-100X $ 75 / set of 8 x 1 mL Sulfur Conc. Sulfur Wt.% Blank 1 µg/g 3 µg/g 10 µg/g 30 µg/g 50 µg/g 75 µg/g 100 µg/g Blank 0.0001 0.0003 0.0010 0.0030 0.0050 0.0075 0.010 Standards of Interests Technical Note Well characterized di-n-butyl sulfide is used in a low sulfur Isooctane matrix for this calibration set. See page 1 for AccuStandard’s comprehensive line of Certified Sulfur calibration standards, AccuPetroCheck, and AccuPetroTest quality control products. ASTM D-3230 Salts in Crude Oil Mixed Salt Solution D-3230-89-1 $ 75 / 100 mL D-3230-89-5 $ 150 / 500 mL At stated conc. in Alcohol Solution (1-butanol : MeOH) (ratio 63:37) tr. H2O 3 comps. Calcium chloride Magnesium chloride 10 µg/mL 20 µg/mL Sodium chloride ASTM D-3231 Phosphorus in Gasoline Element Matrix Originally designed for D-3230-99 70 µg/mL Originally designed for D-3231-99 Quantity Conc. Cat. No. Price Phosphorus H2O 100 mL 1000 µg/mL ICP-41W-1 $ 34 Phosphorus H2O 500 mL 1000 µg/mL ICP-41W-5 $ 67 1 D-323 Meets es id u elin EPA G FG for R is Analys ASTM D-3237 Lead in Gasoline by AA Spectroscopy Lead Standard Calibration Curve D-3237-CAL-SET Set includes the following Catalog Numbers: Cat. No. D-3237-01 D-3237-02 D-3237-03 D-3237-04 $ 210 / 4 x 100 mL Originally designed for D-3237-97 Description Blank 1% Aliquot 336/MIBK 0.02 g Pb / gal ( 5.3 mg Pb/ L) in 1% Aliquat 336 / MIBK 0.05 g Pb / gal ( 13.2 mg Pb/ L) in 1% Aliquat 336 / MIBK 0.10 g Pb / gal ( 26.4 mg Pb/ L) in 1% Aliquat 336 / MIBK $ $ $ $ Price / Unit 20 / 100 mL 80 / 100 mL 80 / 100 mL 80 / 100 mL 7 D-323 Meets es uidelin EPA G FG for R is Analys Ready-to-Inject Petrochemical Standards and Calibration Curves Reduce Costs Ready-to-Inject Increase Time Spent for Sample Analysis Are Validated Against Independent Lots Include Internal Standards or Surrogates Working Level Standards & Continuing Calibration Check (CCC) Follow ASTM Method Guidelines Allow Direct Transfer to Autosampler Vials 16 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method Member 3246 3340 3524 3605 ASTM D-3246 Sulfur in Petroleum Gas by Oxidative Microcoulometry See pages 6 - 11 for AccuStandards comprehensive line of certified sulfur calibration standards ASTM ASTM D-3340 Lithium & Na in Lubricating Greases by Flame Photometer AccuStandard AccuTrace brand AA standards are produced under our rigorous ISO 9001 quality system to exacting specifications. Each standard is prepared from high purity starting materials; deionized water and high purity acids. Every standard is instrumentally assayed to verify 1000 ppm concentration of specified element; Actual Lot Analysis is provided on the label and a Certificate of Analysis is included for ease of record keeping and availability at audits. Originally designed for D-3340-98 Element Unit Matrix Cat. No. Price Technical Note 1,000 µg/mL 100 mL 500 mL AA30H-1 AA30H-5 $ 12 30 Sodium * HCl 100 mL 500 mL AA54H-1 AA54H-5 13 33 ASTM D-3524 (Reapproved 1999) Diesel Fuel Diluent in Used Diesel Engine Oils by GC D-3524 Calibration Curve D-3524-CAL-SET-5ML D-3524-CAL-SET-10ML Test to Low ppb Originally designed for D-3524-90 $ 150 / set of 6 x 5 mL $ 250 / set of 6 x 10 mL Sulfur Analyte Standard 1 Target Wt. % Standard 2 Target Wt. % Standard 3 Target Wt. % Standard 4 Target Wt. % Standard 5 Target Wt. % Standard 6 Target Wt. % # 2 Diesel 30 W Motor oil 10 90 7.5 92.5 5 95 2.5 97.5 1 99 0 100 Internal Standard Solution Mid Level Daily QC Solution D-3524-IS-10ML $ 25 / 1 x 10 mL D-3524-IS-10ML-PAK SAVE 20% $ 100 / 5 x 10 mL At stated conc. in n-Heptane 2 comps. Wt. / Wt. % n-Decane 1.0 n-Octadecane 0.2 D-3524-QC-10ML # 2 Diesel 30 W Motor oil WEAR METALS Lithium * HCl * For your convenience these elements are also available in HNO3. To order HNO3 change the H to N at the end of the Cat. No. See Pages 6-11 $ 30 / 1 x 10 mL 2 comps. Wt. / Wt. % 5.0 95 Column Resolution Mix D-3524-CR $ 10 / 1 x 1 mL D-3524-CR-PAK SAVE 20% $ 40 / 5 x 1 mL At stated conc. in n-Heptane 2 comps. Wt. / Wt. % n-Hexadecane 1.0 n-Octadecane 1.0 ASTM D-3605 (Reapproved 1995) Trace Metals in Gas Turbine Fuels by AA & Flame Emission Spectroscopy D-3605-91 Trace Metals Standard D-3605-91-1 $ 165 / 1 x 100 mL At stated conc. in 1,2,3,4-Tetrahydronaphthalene 4 comps. Na (Sodium) Pb (Lead) (250 µg/mL) (250 µg/mL) Ca (Calcium) V (Vanadium) Originally designed for D-3605-91 Standards of Interests See Table of Contents for the Wear Metals Group pages (250 µg/mL) (250 µg/mL) Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 17 Method ASTM Standards 3606 3610 , Member Originally designed for D-3606-99 ASTM D-3606 Benzene & Toluene in Finished Motor & Aviation Gasoline by GC Aromatics Quantitative Calibration Standard (without Internal Standards) ASTM D-3606-SET-25ML Benzene Toluene Isooctane $ 800 / set of 7 x 25 mL Analyte Calibr. range Std. 1 Target Vol. % Std. 2 Vol. % Std. 3 Vol. % Std. 4 Vol. % Std. 5 Vol. % Std. 6 Vol. % Std. 7 Vol. % 0.06 - 5.0 0.5 - 20 5.00 20.00 75.00 2.50 15.00 82.50 1.25 10.00 88.75 0.67 5.00 94.33 0.33 2.50 97.17 0.12 1.00 98.88 0.06 0.50 99.44 6 D-360 Meets es uidelin EPA G FG for R is Analys Aromatics Quantitative Calibration Standard (with Internal Standard: MEK) D-3606/IS-SET D-3606/IS-SET-2ML D-3606/IS-SET-2ML-PAK $ 115 / set of 7 x 1 mL $ 190 / set of 7 x 2 mL $ 760 / 5 x (7 x 2) mL Analyte Calibr. range Benzene 0.06 - 5.0 Toluene 0.5 - 20 Isooctane Methyl ethyl ketone (Internal Std.) Std. 1 Target Vol. % Std. 2 Vol. % Std. 3 Vol. % Std. 4 Vol. % Std. 5 Vol. % Std. 6 Vol. % Std. 7 Vol. % 4.8 19.2 72.0 4.0 2.4 14.4 79.2 4.0 1.2 9.6 85.2 4.0 0.6432 4.8000 90.5568 4.0 0.3168 2.4000 93.2832 4.0 0.1152 0.9600 94.9248 4.0 0.0576 0.4800 95.4624 4.0 Gasoline Refinery Quality Control Standards Daily Quality Control Standard (with Internal Standard: MEK) Daily Quality Control Standard (without Internal Standard) D-3606-QC/IS-10ML D-3606-QC/IS-10ML-PAK Each at stated quantities D-3606-QC-25ML D-3606-QC-25ML-PAK Each at stated quantities Compound Benzene Toluene Isooctane Methyl ethyl ketone (ISTD) $ 75 / 1 x 10 mL $ 300 / 5 x 10 mL 4 comps. Target Vol. % 0.6432 4.8000 90.5568 4.0 Compound Benzene Toluene Isooctane $ 125 / 1 x 25 mL $ 600 / 5 x 25 mL 3 comps. Target Vol. % 0.67 5.00 94.33 100 100 Technical Note Aromatics Quantitative Calibration Standard (w/ Internal Standard: sec Butanol) D-3606/IS2-SET D-3606/IS2-SET-PAK $ 115 / set of 7 x 1 mL $ 500 / 5 x (7 x 1) mL Analyte Calibr. range Benzene 0.06 - 5.0 Toluene 0.5 - 20 Isooctane sec Butanol (Internal Standard) Std. 1 Target Vol. % Std. 2 Vol. % Std. 3 Vol. % Std. 4 Vol. % Std. 5 Vol. % Std. 6 Vol. % Std. 7 Vol. % 4.8 19.2 72.0 4.0 2.4 14.4 79.2 4.0 1.2 9.6 85.2 4.0 0.6432 4.8000 90.5568 4.0 0.3168 2.4000 93.2832 4.0 0.1152 0.9600 94.9248 4.0 0.0576 0.4800 95.4624 4.0 Gasoline Refinery Quality Control Standards Daily Quality Control Standard Daily Quality Control Standard (without Internal Standard) (with Internal Standard: sec Butanol) D-3606-QC-IS2-25ML D-3606-QC-IS2-25ML-PAK Each at stated quantities Compound Benzene Toluene Isooctane sec-Butanol (ISTD) $ 125 / 1 x 25 mL $ 600 / 5 x 25 mL 4 comps. Target Vol. % 0.6432 4.8000 90.5568 4.0 100 D-3606-QC-25ML D-3606-QC-25ML-PAK Each at stated quantities Compound Benzene Toluene Isooctane Due to changes in the possible use of other oxygenates like ethanol added to gasoline, AccuStandard formulated a new calibration curve using sec-butanol as an Internal Standard. The use of this new ISTD minimizes coelution caused by the oxygenate(s) and pre column - standard column configuration in the GC system. $ 125 / 1 x 25 mL $ 600 / 5 x 25 mL 3 comps. Target Vol. % 0.67 5.00 94.33 100 ASTM D-3610 Total Cobalt in Alumina-Base Cobalt-Molybdenum Catalyst by Potentiometric Titration Cobalt Oxide Standard D-3610-93-1 $ 50 / 1 x 100 mL Originally designed for D-3610-88 (Re-Approved 1993) Cobalt oxide @ 1500 µg/mL in Water 18 Quality System is Certified to comply with the International ISO 9001 Quality Standard On-Line Ordering There is an easier way to get Chemical Reference Standards ® e-Standards from AccuStandard.com ASTM 5 Ways to Search “e-Standards” is the Fastest, Most Comprehensive Search Engine available and contains over 30,000 products. Search by: Catalog Number Single or Multiple Components, Method (EPA, ASTM, etc.) Chemical Category (Organic, Inorganic, Petroleum, etc.) Other Companies’ Part Number Log on to www.accustandard.com and see how easy it is. Easy Ordering 24/7 Find It Fast...simply search for a product, select it for purchase & click - it's that easy! Discounts may apply to online orders, see details on website. On-Line Custom Services AccuStandard specializes in synthesizing chemicals of high purity to be used as reference standards, and offers custom synthesis capability for milligram to kilogram batches. If you can't find the specific standard you need, we can prepare Custom Formulations and Custom Packaging for both Organic and Inorganic needs. See our Website for more info. Over 30,000 Standards just a click away Cross Reference Table ASTM IP ISO DIN JIS AFNOR sorted by ASTM Method see beginning of Catalog Test to Low ppb Sulfur See Pages 6-11 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 19 Method ASTM Standards 3710 3798 3831 , Member ASTM ASTM D-3710 (Reapproved 1999) Boiling Range Distribution of Gasoline & Gasoline Fractions by GC This SIM DIS (Simulated Distillation or GCD) Method is used to determine the boiling range distribution of gasoline and gasoline components. ASTM Method D-3710 is used for petroleum products and fractions with a final boiling point of 500°F (260°C) or lower. By having an insight into the composition of the gasoline blend, essential data for the calculation of vapor pressure and a prediction of the D-86 distillation curve can be made. Qualitative Calibration Standard Quantitative Calibration Standard D-3710-QUAL D-3710-QUAL-PAK ASTM-D3710 ASTM-D3710-PAK $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 19 comps. Approx. Wt./ Wt. % n-Butane 4.5 n-Butylbenzene 3.2 n-Decane 3.2 2,4-Dimethylpentane 5.4 n-Dodecane 3.2 n-Heptane 9.7 n-Hexane 5.4 2-Methylbutane 9.7 2-Methylpentane 5.4 2-Methylpropane 1.5 Approx. Wt./ Wt. % n-Octane 5.4 n-Pentadecane 2.2 n-Pentane 7.6 n-Propane 1.5 n-Propylbenzene 4.3 n-Tetradecane 2.2 Toluene 10.8 n-Tridecane 2.2 p-Xylene 13 $ 25 / 1 x 1 mL SAVE 36% $ 80 / 5 x 1 mL 16 comps. Vol./Vol. % n-Butylbenzene 3.5 n-Decane 3.5 2,4-Dimethylpentane 5.8 n-Dodecane 3.5 n-Heptane 10.5 n-Hexane 5.8 2-Methylbutane 10.5 2-Methylpentane 5.8 Vol./Vol. % n-Octane n-Pentadecane n-Pentane n-Propylbenzene n-Tetradecane Toluene n-Tridecane p-Xylene Originally designed for D-3710-95 Standards of Interests See page 3 for AccuStandard’s new D-86 QA/QC Standards. 5.8 2.3 8.1 4.7 2.3 11.6 2.3 14.0 NEW ASTM D-2887-99 Boiling Range Distribution of Petroleum Fractions by GC Calibration Solution * DRH-002S-R1 DRH-002S-R1-PAK At stated conc. in Chloroform µg/mL µg/mL 1200 n-Hexane 600 n-Undecane 1200 n-Heptane 600 n-Dodecane 1200 n-Octane 800 n-Tetradecane 1000 n-Nonane 800 n-Hexadecane n-Decane 1200 n-Octadecane n-Eicosane n-Tetracosane n-Octacosane µg/mL 500 200 200 100 $ 50 / 1 x 1 mL SAVE 20% $ 200 / 5 x 1 mL 17 comps. µg/mL n-Dotriacontane 100 n-Hexatriacontane 100 n-Tetracontane 100 n-Tetratetracontane100 * Can be shipped by Air and Sea ASTM D-3798 Analysis of p-Xylene by GC Technical Note AccuStandard’s R & D team has developed a special highly purified p-Xylene designed for ASTM Method D-3798 specifications. The incorporation of this p-Xylene into the formulation allows the analytical chemist to qualitatively and quantitatively measure the impurities in the p-Xylene feedstock streams. p-Xylene Impurity Standard with ISTD p-Xylene Impurity Standard without ISTD D-3798-IS $ 30 / 1 x 1 mL D-3798-IS-PAK SAVE 33% $ 100 / 5 x 1 mL At stated conc. by weight 11 comps. D-3798-10ML $ 65 / 1 x 10 mL D-3798-10ML-PAK SAVE 20% $ 260 / 5 x 10 mL At stated conc. by weight 10 comps. Wt./Wt. % n-Pentane 0.15 n-Octane 0.15 Benzene 0.15 Toluene 0.15 Ethylbenzene 0.15 p-Xylene 98.65 m-Xylene 0.15 Wt./Wt. % 0.15 0.15 0.15 o-Xylene Cumene Propylbenzene Total Analytes 100 plus n-Undecane* (ISTD) 0.500 grams n-Pentane n-Octane Benzene Toluene Ethylbenzene Wt./Wt. % 0.15 0.15 0.15 0.15 0.15 p-Xylene m-Xylene o-Xylene Cumene Propylbenzene Wt./Wt. % 98.65 0.15 0.15 0.15 0.15 Bulk Packaged p-Xylene without Internal Standard Other suggested internal standards can be used in conjunction with the bulk packaged D-3789 1 x 10 mL ampule to meet your company’s application. If you prefer to eliminate making standards, contact AccuStandard’s Technical Department with your unique formulation for a custom quotation. The custom quotation request form is located in the back of this catalog. ASTM D-3831 Manganese in Gasoline by AA Spectroscopy Manganese Stock Solution D-3831 $ 65 / 1 x 100 mL Originally designed for D-3831-98 Manganese @ 1.0 g Mn / gal (264.2 mg Mn / L) in Methyl isobutyl ketone 20 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method Member 4059 4291 4294 4377 Originally designed for D-4059-96 ASTM D-4059 Polychlorinated Biphenyls in Insulating Liquids by GC Aroclors in PCB-Free Transformer Oil (At 2 concentrations in Transcrest W130) Conc. (ppm w/w) Cat. No. 1 x 1 mL Price 5 x 1 mL Price PAK Cat. No. Aroclor 1016 Aroclor 1016 50 500 C-216-ST-1 C-216-ST-2 $ 25 30 C-216-ST-1-PAK C-216-ST-2-PAK $ 90 120 Aroclor 1221 Aroclor 1221 50 500 C-221-ST-1 C-221-ST-2 25 30 C-221-ST-1-PAK C-221-ST-2-PAK 90 120 Aroclor 1232 Aroclor 1232 50 500 C-232-ST-1 C-232-ST-2 25 30 C-232-ST-1-PAK C-232-ST-2-PAK 90 120 Aroclor 1242 Aroclor 1242 50 500 C-242-ST-1 C-242-ST-2 25 30 C-242-ST-1-PAK C-242-ST-2-PAK 90 120 Aroclor 1248 Aroclor 1248 50 500 C-248-ST-1 C-248-ST-2 25 30 C-248-ST-1-PAK C-248-ST-2-PAK 90 120 Aroclor 1254 Aroclor 1254 50 500 C-254-ST-1 C-254-ST-2 25 30 C-254-ST-1-PAK C-254-ST-2-PAK 90 120 Aroclor 1260 Aroclor 1260 50 500 C-260-ST-1 C-260-ST-2 25 30 C-260-ST-1-PAK C-260-ST-2-PAK 90 120 Aroclor 1262 Aroclor 1262 50 500 C-262-ST-1 C-262-ST-2 25 30 C-262-ST-1-PAK C-262-ST-2-PAK 90 120 Aroclor 1268 Aroclor 1268 50 500 C-268-ST-1 C-268-ST-2 25 30 C-268-ST-1-PAK C-268-ST-2-PAK 90 120 Additional Aroclors and PCB Congener Standards available in our Organic Catalog Neat Individual Aroclors Z-008 Aroclor # Cat. No. Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor C-216N C-221N C-232N C-242N C-248N C-254N C-260N C-262N C-268N 1016 1221 1232 1242 1248 1254 1260 1262 1268 Kit of above 9 Aroclors Price / Unit $ 25 25 25 25 25 25 25 25 25 / / / / / / / / / 100 100 10 100 10 100 100 100 10 Z-008 mg mg mg mg mg mg mg mg mg (Kit) 100 100 10 100 10 100 10 10 10 mg mg mg mg mg mg mg mg mg Aroclor-free transformer oil also available as: T-W130 $ 5 / 1 x 1 mL $ 125 / 9 vials ASTM D-4291 (Reapproved 1998) Trace Ethylene Glycol in Used Engine Oil Ethylene Glycol Stock Standard D-4291-93 D-4291-93-PAK $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL Originally designed for D-4291-93 Ethylene glycol @ 2000 µg/mL in water ASTM D-4294 Sulfur in Petroleum Products by ED-XRF Spectroscopy See page 8-11 for AccuStandard’s comprehensive line of Certified Sulfur Calibration Standards designed for matrix specific applications as described in Method D-4294 in section 9.0 (Calibration & Standardization). 4 D-429 Meets es id u elin EPA G FG for R is Analys ASTM D-4377 Water in Crude oils by Potentiometric Karl Fischer Titration See page 5 for AccuStandard’s comprehensive line of Certified Karl Fischer Water Standards. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 21 ASTM Aroclor # Method ASTM Standards 4420 4628 , Member ASTM D-4420 Aromatics in Finished Gasolines by GC Originally designed for D-4420-94 Aromatics in Gasoline by GC/TC ASTM D-4420-CAL-SET $ 105 / set of 7 x 1 mL Analyte Std. 1 Target Vol. % Std. 2 Target Vol. % Std. 3 Target Vol. % Std. 4 Target Vol. % Std. 5 Target Vol. % Std. 6 Target Vol. % Std. 7 Target Vol. % Benzene Toluene Total Xylenes (C8 aromatics) n-Butylbenzene (C9 + aromatics) Isooctane 0.05 0.5 5 30.00 64.45 0.10 1.00 10.00 25.00 63.90 0.25 2.50 15.00 20.00 62.25 0.75 5.00 20.00 10.00 64.25 1.25 10.00 25.00 5.00 58.75 2.50 15.00 1.00 15.00 66.50 5.00 25.00 3.00 2.50 64.50 Aromatics in Gasoline by GC/TX WEAR METALS D-4420-94 D-4420-94-PAK $ 20 / 1 x 1 mL $ 80 / 5 x 1 mL 5 comps. Benzene Toluene Total Xylenes (C8 aromatics) Vol. % 3.00 10.00 15.00 Vol. % 15.00 57.00 n-Butylbenzene(C9 + aromatics) Isooctane ASTM D-4628 Barium, Calcium, Magnesium & Zinc in Unused Lubricating Oil Lubricating Oil, Elements (Nominal Value) Wt.% listed below ASTM-P-0113-SET $ 2850 / 17 x 100 mL Cat. No. ASTM-P-0113-01 ASTM-P-0113-02 ASTM-P-0113-03 ASTM-P-0113-04 ASTM-P-0113-05 ASTM-P-0113-06 ASTM-P-0113-07 ASTM-P-0113-08 ASTM-P-0113-09 ASTM-P-0113-10 ASTM-P-0113-11 ASTM-P-0113-12 ASTM-P-0113-13 ASTM-P-0113-14 ASTM-P-0113-15 ASTM-P-0113-16 ASTM-P-0113-17 Originally designed for D-4628-97 Ba (Wt.%) Ca (Wt.%) Mg (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.025 0.000 0.100 0.175 0.150 0.000 0.100 0.200 0.050 0.075 0.010 0.000 0.175 0.005 0.000 0.005 0.000 0.600 0.500 0.400 0.260 0.005 0.400 0.300 0.200 0.060 0.060 0.050 0.025 0.005 0.170 0.100 0.010 0.000 0.100 0.150 0.350 0.225 0.450 0.500 0.325 0.250 0.100 0.400 0.300 0.200 0.375 0.175 0.425 0.275 0.000 0.005 0.200 0.150 0.250 0.005 0.025 0.060 0.100 0.080 0.050 0.120 0.150 0.200 0.250 0.100 0.010 0.000 0.175 0.050 0.300 0.150 0.450 0.350 0.250 0.450 0.300 0.200 0.100 0.200 0.400 0.550 0.200 0.600 0.000 0.060 0.080 0.180 0.120 0.070 0.100 0.120 0.100 0.130 0.050 0.075 0.130 0.150 0.110 0.200 0.250 0.000 Standards of Interests See Table of Contents for the Wear Metals Group pages. Ready-to-Inject Petrochemical Standards and Calibration Curves Reduce Costs Increase Time Spent for Sample Analysis Are Validated Against Independent Lots Include Internal Standards or Surrogates Follow ASTM Method Guidelines Allow Direct Transfer to Autosampler Vials Cross Reference Table ASTM IP ISO DIN JIS AFNOR sorted by ASTM Method see beginning of Catalog 22 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 4629 Member ASTM D-4629 Trace Nitrogen in Liquid Petroleum Hydrocarbons by Syringe/Inlet Oxidative Combustion and Chemiluminescence Detection. IP Designation 379/88 Originally designed for D-4629-96 Technical Note Nitrogen Calibration Set-Low Boiling Solvents D-4629-91-LB-CAL-SET $ 75 / set of 7 x 1 mL Set includes the following Cat. No.s Cat. No. Description D-4629-91-LB-0.3X D-4629-91-LB-1X D-4629-91-LB-10X D-4629-91-LB-25X D-4629-91-LB-50X D-4629-91-LB-75X D-4629-91-LB-100X Nitrogen Nitrogen Nitrogen Nitrogen Nitrogen Nitrogen Nitrogen @ @ @ @ @ @ @ ASTM Method D-4629 is used to determine trace total nitrogen naturally found in liquid hydrocarbons boiling from 50 to 400°C with viscosities between 0.2 and 10 cSt. This method monitors feed stocks for nitrogen to prevent the poisoning of some process catalysts when trace nitrogenous materials are present. Nitrogen introduced using Pyridine Price / Unit 0.3 1 10 25 50 75 100 µg/mL in µg/mL in µg/mL in µg/mL in µg/mL in µg/mL in µg/mL in Isooctane Isooctane Isooctane Isooctane Isooctane Isooctane Isooctane $ $ $ $ $ $ $ 20 20 20 20 20 20 20 / / / / / / / 1 1 1 1 1 1 1 x x x x x x x 1 1 1 1 1 1 1 mL mL mL mL mL mL mL Stock Nitrogen Solution for Low Boiling Solvents D-4629-91-LB-CON D-4629-91-LB-CON-PAK $ 20 / 1 x 1 mL $ 80 / 5 x 1 mL Nitrogen @ 1000 µg/mL in Isooctane (Pyridine @ 5.65 mg/mL in Isooctane) Technical Note Nitrogen Calibration Set-High Boiling Solvents D-4629-91-HB-CAL-SET $ 75 / set of 7 x 1 mL Set includes the following Cat. No.s Cat. No. Description D-4629-91-HB-0.3X D-4629-91-HB-1X D-4629-91-HB-10X D-4629-91-HB-25X D-4629-91-HB-50X D-4629-91-HB-75X D-4629-91-HB-100X Nitrogen Nitrogen Nitrogen Nitrogen Nitrogen Nitrogen Nitrogen @ @ @ @ @ @ @ Nitrogen introduced using Carbazole Price / Unit 0.3 1 10 25 50 75 100 µg/mL in Toluene µg/mL in Toluene µg/mL in Toluene µg/mL in Toluene µg/mL in Toluene µg/mL in Toluene µg/mL in Toluene $ $ $ $ $ $ $ 20 20 20 20 20 20 20 / / / / / / / 1 1 1 1 1 1 1 x x x x x x x 1 1 1 1 1 1 1 mL mL mL mL mL mL mL Stock Nitrogen Solution for High Boiling Solvents D-4629-91-HB-CON D-4629-91-HB-CON-PAK $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL Nitrogen @ 1000 µg/mL in Toluene : Acetone (9:1) (Carbazole @ 11.95 mg/mL in Toluene : Acetone (9:1) ) Low level Nitrogen Calibration Set ASTM-P-0070-SET Set includes the following Cat. No.s Technical Note $ 75 / 6 x 1 mL Cat. No. Description ASTM-P-0070-BL ASTM-P-0070-1X ASTM-P-0070-2X ASTM-P-0070-4X ASTM-P-0070-10X ASTM-P-0070-20X Isooctane Blank Nitrogen @ 0.5 Nitrogen @ 1.0 Nitrogen @ 2.0 Nitrogen @ 5.0 Nitrogen @ 10.0 Unit µg/g µg/g µg/g µg/g µg/g Low level Nitrogen & Sulfur Calibration Set ASTM-P-0071-SET Nitrogen introduced using Aniline in in in in in 1 1 1 1 1 1 Isooctane Isooctane Isooctane Isooctane Isooctane x x x x x x 1 1 1 1 1 1 mL mL mL mL mL mL Technical Note $ 50 / 4 x 1 mL Set includes the following Cat. No.s The Nitrogen is introduced using Aniline and the Sulfur is introduced using di-n-Butyl sulfide Cat. No. Description ASTM-P-0071-BL ASTM-P-0071-01 ASTM-P-0071-02 ASTM-P-0071-03 Benzene Blank Nitrogen @ 0.25 µg/g & Sulfur @ 0.25 µg/g in Benzene Nitrogen @ 0.50 µg/g & Sulfur @ 0.50 µg/g in Benzene Nitrogen @ 1.00 µg/g & Sulfur @ 1.00 µg/g in Benzene Unit 1 1 1 1 x x x x 1 1 1 1 mL mL mL mL Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 23 Method ASTM Standards 4815 , Member ASTM D-4815 Originally designed for D-4815-99 MtBE, EtBE, TAME, DIPE, Tertiary-amyl Alcohol and C1 to C4 Alcohols in Gasoline by GC ASTM Oxygenate Quantitative Calibration Mixtures (without Internal Standard) D-4815-SET-10ML $ 300 / set of 5 x 10 mL of 5 component mix Std. 1 Wt. % Analyte Ethanol t-Butanol Methyl t-butyl ether (MtBE) t-Pentanol Isooctane/xylene (65:35) Std. 2 Wt. % 3.00 0.10 20.0 1.25 75.65 Std. 3 Wt. % 0.10 3.00 15.00 5.00 76.90 6.00 6.00 10.00 2.50 75.50 Std. 4 Wt. % 9.00 8.00 5.00 3.75 74.25 Std. 5 Wt. % 12.00 12.00 0.10 0.10 75.80 Oxygenate Quantitative Calibration Mixtures (with Internal Standard) D-4815/IS-SET of 6 component mix D-4815/IS-SET-PAK Analyte $ 125 / set of 5 x 1 mL $ 500 / set of 5 x (5 x 1 mL) Calibration Range Std. 1 Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % Ethanol 0.1 - 11.40 t-Butanol 0.1 - 11.40 Methyl t-butyl ether (MtBE) 0.1 - 19.0 t-Pentanol 0.1 - 4.79 1,2-Dimethoxyethane (DME) (Internal Std.) Isooctane/xylene (65:35) 2.85 0.10 19.00 1.19 5.00 71.87 0.10 2.85 14.25 4.75 5.00 73.06 5.70 5.70 9.50 2.38 5.00 71.73 8.55 7.60 4.75 3.56 5.00 70.54 11.40 11.40 0.10 0.10 5.00 72.0 Total Oxgenates & Internal Standard 28.14 26.95 28.28 29.46 28.00 Quantitative Peak ID and Retention Time Mixture D-4815-RT D-4815-RT-PAK $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL Compound Wt. % Methylcyclopentane 4.00 Methanol 7.30 Ethanol 7.30 Isopropanol 7.30 tert-Butanol 7.30 n-Propanol 7.30 Methyl tert-butyl ether (MtBE) 4.00 sec-Butanol 7.30 Diisopropyl ether (DIPE) 4.00 Isobutanol 7.30 Ethyl tert-butyl ether (EtBE) 4.00 tert-Pentanol 7.30 1,2-Dimethoxyethane (ISTD) 6.00 n-Butanol 7.30 Benzene 5.00 tert-Amyl methyl ether 7.30 100 16 comp. core mix 5 D-481 Meets es uidelin EPA G FG for R is Analys Technical Note Additional Oxygenate calibration, check standards, and independent reference standards can be found in ASTM method D-5599 (pages 34-36) or D-5622-94 (page 37) The required QA/QC procedures in EPA methods stipulate a calibration check standard be used once per analytical batch or per 10 sample set. AccuStandard has bulk packaged our check standards to meet this increased usage. Valve Timing Mixture D-4815-VT D-4815-VT-PAK $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 5 comps. Compound Wt. % Methylcyclopentane 10.00 Diisopropyl ether (DIPE) 10.00 Ethyl tert-butyl ether (EtBE) 10.00 Methyl tert-butyl ether (MtBE) 10.00 n-Hexane 60.00 Oxygenate Internal Standard Mixture M-GRO-IS-5ML M-GRO-IS-5ML-PAK $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL 1,2-Dimethoxyethane (ISTD) (neat) Test to Low ppb Oxygenate Free Refinery Gasoline Blank M-GRO-BLNK-10ML $ 10 / 1 x 10 mL M-GRO-BLNK-10ML-PAKSAVE 20% $ 40 / 5 x 10 mL Sulfur See Pages 6-11 RFA Gasoline (neat) Custom Formulations AccuStandard offers over 30,000 different standards, and if you can't find the specific standard you need, we will prepare a custom formulation. Our custom organic and inorganic standards are a fast, economical way to address your unique requirements. To make an inquiry for Custom Quotes visit our website. You can also Email your requirements to [email protected] or Fax us at 203-786-5287. Please include the following information: List of analytes and concentrations, Solvent or matrix, Quantity required (milliliters), Packaging unit size (milliliters per ampule, bottle, or vial). Quality Control Options 1. Gravimetric/Volumetric Certification: Each standard is measured gravimetrically and then QC’ed instrumentally (where available). Every component in the standard is guaranteed to be within ±0.5% of the requested value unless otherwise stated. The solutions are made up to volume using class A glassware. A certificate comes with each standard and documents the gravimetric values used. 2. Quantitative Validation: Full QA/QC method includes extended GC analysis using both internal and calibration standards plus statistical analysis. A data package is provided containing analytical and gravimetric data (Organic customs only). Also available: OEM Standards - Privately labeled standards manufactured and tested to your specifications. 24 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 4927 4928 4929 Member ASTM D-4927 Elemental Analysis of Lubricant and Additive Components Barium, Calcium,Phosphorus, Sulfur, and Zinc by WD-XRF Spectroscopy Cat. No. Ca (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.100 0.175 0.000 0.025 0.150 0.000 0.200 0.000 0.100 0.050 0.075 0.010 0.005 0.000 0.000 0.005 0.000 0.600 0.500 0.400 0.260 0.005 0.400 0.300 0.200 0.060 0.060 0.050 0.025 0.005 0.170 0.100 0.010 0.000 0.005 0.200 0.150 0.250 0.005 0.025 0.060 0.100 0.080 0.050 0.120 0.150 0.200 0.250 0.100 0.010 0.000 0.175 0.050 0.300 0.150 0.450 0.350 0.250 0.450 0.300 0.200 0.100 0.200 0.400 0.550 0.200 0.600 0.000 0.060 0.080 0.180 0.120 0.070 0.100 0.120 0.100 0.130 0.050 0.075 0.130 0.150 0.110 0.200 0.250 0.000 Standards of Interests See Table of Contents for the Wear Metals Group pages WEAR METALS ASTM-P-0110-01 ASTM-P-0110-02 ASTM-P-0110-03 ASTM-P-0110-04 ASTM-P-0110-05 ASTM-P-0110-06 ASTM-P-0110-07 ASTM-P-0110-08 ASTM-P-0110-09 ASTM-P-0110-10 ASTM-P-0110-11 ASTM-P-0110-12 ASTM-P-0110-13 ASTM-P-0110-14 ASTM-P-0110-15 ASTM-P-0110-16 ASTM-P-0110-17 Ba (Wt.%) Originally designed for D-4927-96 ASTM D-4928 Water in Crude Oils by Potentiometric Karl Fischer Titration See page 5 for AccuStandard’s new line of Karl Fischer Water Standards. ASTM D-4929 Organic Chloride Content in Crude Oil - Test Method B Combustion and Microcoulometry Originally designed for D-4929-99 Standards of Interests Working Level Chlorine Standard Stock Chlorine Standard D-4929-94 D-4929-94-PAK D-4929-94-100X $ 15 / 1 x 5 mL D-4929-94-100X-PAK SAVE 20% $ 60 / 5 x 5 mL $ 10 / 1 x 5 mL SAVE 20% $ 40 / 5 x 5 mL Chlorine @ 10 µg/mL in Isooctane ASTM Lubricating Oil, Elements (Nominal Value) Wt.% listed below ASTM-P-0110-SET $ 2300 / 17 x 100 mL See page 66 for additional proposed and promulgated Chlorine in Lube Oil standards Chlorine @ 1000 µg/mL in Isooctane Custom Ampulling for Bulk Quantity Requirements Automated ampule filling & sealing 0.2 mL up to 20 mL Quantities from 500 to over 500,000 ampules Homogeneity testing Amber ampules for added product stability Private labeling and packaging We can reduce your costs using the Cozzoli Auto Filling/ Sealing Machine to package just the right size product for your application. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 25 Method ASTM Standards 4951 5056 , Member ASTM ASTM D-4951 20 Wear Metal Multi-Element Standard containing no metallic sulfonates Conc. (µg/g) Cat. No. Price 10 30 50 100 300 500 900 WM-20-NMS-1X-1 WM-20-NMS-3X-1 WM-20-NMS-5X-1 WM-20-NMS-10X-1 WM-20-NMS-30X-1 WM-20-NMS-50X-1 WM-20-NMS-90X-1 $ 150 150 150 170 230 350 500 Standards of Interests Each Wear Metal Standard contains the below list of 20 elements in hydrocarbon oil at the stated concentration Al (Aluminum) B (Boron) Ba (Barium) Ca (Calcium) Cd (Cadmium) Cr (Chromium) Cu (Copper) Fe (Iron) Mg (Magnesium) Mn (Manganese) WM-20-NMS-SET-1 $ 1450 set of above 7 x 100 mL WEAR METALS Originally designed for D-4951-96 Additive Elements in Lubricating Oils by Inductively Coupled Plasma Atomic Emission Spectrometry Mo (Molybdenum) Na (Sodium) Ni (Nickel) P (Phosphorus) Pb (Lead) Si (Silicon) Sn (Tin) Ti (Titanium) V (Vanadium) Zn (Zinc) Technical Notes This calibration curve has been formulated with starting materials containing no metal sulfonates. This way a sulfur calibration curve can easily be developed using a high concentration sulfur standard. Recommended Internal Standard (IS) Element Sulfur free Organometallic (IS) @ 1000 µg/g Price Cat. No. 50 mL Sulfur free Organometallic (IS) @ 5000 µg/g Price Cat. No. 50 mL Cobalt WM-NMS-14 WM-NMS-14-5X $ 75 $ 110 Originally designed for D-5056-96 ASTM D-5056 Trace Metals in Petroleum Coke by Atomic Absorption Element @ 1000 µg/mL Matrix See Table of Contents for the Wear Metals Group pages. Element @ 1000 µg/mL Matrix Cat. No. Price 100 mL AA52W-1 $ 13 500 mL AA52W-5 33 100 mL AA54N-1 13 HNO3 500 mL AA54N-5 33 12 Vanadium 100 mL AA67N-1 13 30 HNO3 500 mL AA67N-5 33 Unit Cat. No. Price * Aluminum 100 mL AA01N-1 $ 13 Silicon HNO3 500 mL AA01N-5 33 H2O tr. NaOH * Calcium 100 mL AA09N-1 12 * Sodium HNO3 500 mL AA09N-5 30 * Iron 100 mL AA27N-1 HNO3 500 mL AA27N-5 Nickel 100 mL AA37N-1 12 HNO3 500 mL AA37N-5 30 Unit * For your convenience these elements are available in HCl. To order, change the N to H at the end of the catalog numbers. Cross Reference Table ASTM IP ISO DIN JIS AFNOR sorted by ASTM Method see beginning of Catalog 26 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5059 5134 Member Originally designed for D-5059-98 ASTM D-5059 Lead in Gasoline by X-Ray Spectroscopy IP Designation 228/79 Technical Notes Part A - Lead in Gasoline Standards Internal Standard D-5059-A-CAL-SET $ 450 / set of 7 x 4 oz The Set contains the following 7 solutions in isooctane D-5059-IS-4 $ 80 / 1 x 4 oz bottle D-5059-IS-10ML-PAK $ 60 / 5 x 10 mL amps Cat. No. Lead Concentration g Pb/US gal g Pb/ UK gal mg Pb/mL Bismuth @ 0.793 mg/mL (3.00 g/US gal) (3.60 g/UK gal) in Mineral oil D-5059-A-01 D-5059-A-02 D-5059-A-03 D-5059-A-04 D-5059-A-05 D-5059-A-06 D-5059-A-07 0.0000 0.1000 1.0000 2.0000 3.0000 4.0000 5.0000 0.000 0.026 0.264 0.528 0.793 1.057 1.321 0.000 0.120 1.200 2.400 3.600 4.800 6.000 Price / Unit $ 10 80 80 80 80 80 80 / / / / / / / 4 4 4 4 4 4 4 oz oz oz oz oz oz oz 9 D-505 Meets es uidelin EPA G FG for R is Analys ASTM AccuStandard has formulated the following standards to measure the lead content in gasoline for both high and low concentrations using bismuth as an internal standard. For long term stability and ease of use AccuStandard provides the internal standard in two convenient packaging sizes. The bulk 4 oz. bottles are designed for laboratories analyzing many samples while the 10 mL ampules are for laboratories that have limited requests for the test method. Should you require bulk quantities of the internal standard conveniently packaged in single-use ampules, contact AccuStandard’s technical department for a quotation. Bulk volumes of 250 mL or more can be sealed into ampules (your choice up to 20 mL size). Use of our ampulling services can provide substantial saving for the Laboratory. Technical Notes All D-5059 Certificates have the concentrations for the Standard listed in three convenient Lead Concentration units. Part C - Lead in Gasoline Standards D-5059-C-CAL-SET $ 450 / set of 7 x 4 oz The Set contains the following 7 solutions in isooctane Cat. No. D-5059-C-01 D-5059-C-02 D-5059-C-03 D-5059-C-04 D-5059-C-05 D-5059-C-06 D-5059-C-07 Lead Concentration g Pb/US gal g Pb/ UK gal µg Pb/mL 0.0000 0.0010 0.0050 0.0100 0.0500 0.1000 0.3000 0.000 0.264 1.321 2.642 13.209 26.417 79.252 0.000 0.001 0.006 0.012 0.060 0.120 0.360 Price / Unit $ 10 80 80 80 80 80 80 / / / / / / / 4 4 4 4 4 4 4 oz oz oz oz oz oz oz ASTM D-5134 Petroleum Naphthas through n-Nonane by Capillary GC Originally designed for D-5134-98 Qualitative Reference Petroleum Set D-5134-92-SET $ 75 / 3 x 1 mL Cat. No. Description Unit D-5134-92-ALK Qualitative Reference Alkylate Standard neat fraction approx. 30 components identified 1 x 1 mL $ 30 D-5134-92-NAP Qualitative Reference Naphtha Standard neat fraction approx. 70 components identified 1 x 1 mL 30 D-5134-92-REF Qualitative Reference Reformate Standard neat fraction approx. 100 components identified 1 x 1 mL 30 Column Evaluation Mix Linearity Check Mix D-5134-92-CEM D-5134-92-LCM 10% w/w each component Wt. / Wt. % Toluene 0.5 n-Heptane 1.0 2,3,3-Trimethylpentane 1.0 2-Methylheptane 1.0 $ 35 / 1 x 1 mL 7 comps. Wt. / Wt. % 4-Methylheptane 1.0 n-Octane 1.0 2-Methylpentane 94.5 Benzene 2,4-Dimethylheptane 2,4-Dimethylhexane n-Heptane n-Hexane Price Standards of Interests See page 14 for additional Detailed Hydrocarbon Analysis (DHA) blends. $ / 1 x 1 mL 10 comps. 2-Methylheptane 2-Methylhexane n-Nonane n-Octane Toluene Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 27 Method ASTM Standards 5184 5185 5186 , Member ASTM D-5184 ASTM (Reapproved 1995) Aluminum and Silicon in Fuel Oils by Ashing, Fusion, ICP-AES Spectrometry & AA Spectrometry Aluminum Standard Solution Tartaric Acid / Hydrochloric Acid Solution D-5184-91-TA-5 D-5184-91-AL-1 D-5184-91-AL-5 $ 20 / 1 x 500 mL Silicon Standard Solution $ 34 / 1 x 100 mL $ 67 / 1 x 500 mL WEAR METALS Silicon @ 1000 µg/mL in trace NaOH ASTM D-5185 Technical Note Contact the our Technical department for Ready-toAspirate working level calibration curves designed for your laboratories' specific calibration ranges. Additive Elements, Wear Metals, & Contaminants in Used Lubricating Oils by ICP-AES 21 Wear Metal Multi-Element Standard Containing No Metallic Sulfonates Conc. (µg/g) 10 30 50 100 300 500 $ 34 / 1 x 100 mL $ 67 / 1 x 500 mL Al @ 1000 µg/mL in 5 % HCl Tartaric acid @ 0.5% w/v in 4% HCl D-5184-91-SI-1 D-5184-91-SI-5 Originally designed for D-5184-91 Cat. No. Price WM-21-NMS-1X-1 WM-21-NMS-3X-1 WM-21-NMS-5X-1 WM-21-NMS-10X-1 WM-21-NMS-30X-1 WM-21-NMS-50X-1 Each Wear Metal Standard contains the below list of 21 elements in hydrocarbon oil at the stated concentration Ag (Silver) Al (Aluminum) B (Boron) Ba (Barium) Ca (Calcium) Cd (Cadmium) Cr (Chromium) Cu (Copper) Fe (Iron) Mg (Magnesium) Mn (Manganese) $ 160 160 160 180 240 350 WM-21-NMS-SET-1 $ 1050 set of above 6 x 100 mL Mo (Molybdenum) Na (Sodium) Ni (Nickel) P (Phosphorus) Pb (Lead) Si (Silicon) Sn (Tin) Ti (Titanium) V (Vanadium) Zn (Zinc) Recommended Internal Standard (IS) Element Sulfur free Organometallic (IS) @ 1000 µg/g Price Cat. No. 50 mL Sulfur free Organometallic (IS) @ 5000 µg/g Price Cat. No. 50 mL Cobalt WM-NMS-14 WM-NMS-14-5X ASTM D-5186 $ 75 $ 110 Aromatic Content & Polynuclear Aromatic Content of Diesel Fuels & Aviation Turbine Fuels by SFC Performance Solution Detector Linearity Check Solution Set D-5186-96-PM D-5186-96-PM-PAK D-5186-96-DLC-SET $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 4 comps. Wt. / Wt. % Wt. / Wt. % n-Hexadecane 75 Tetralin 3.0 Naphthalene 2.0 Toluene 20 Originally designed for D-5185-97 Standards of Interests See Table of Contents for the Wear Metals Group pages Technical Notes This calibration curve has been formulated with starting materials containing no metal sulfonates. So a sulfur calibration curve can easily be developed using a high concentration sulfur standard. Originally designed for D-5186-99 $ 30 / 2 x 1 mL Set includes the below two Cat. No.'s D-5186-96-DLC-25X 25% w/w #2 Diesel Fuel in n-Hexadecane D-5186-96-DLC-50X 50% w/w #2 Diesel Fuel in n-Hexadecane ISO 9001:2000 Certificate Number: 31692 28 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method Member 5188 5191 & 5482 5307 ASTM D-5188 Vapor - Liquid Ratio Temperature Standards Performance Check Samples for daily monitoring of instrument performance V/L Temp ASTM-P-125-01-VAP ASTM-P-125-02-VAP 36.1˚C (96.9˚F) 68.0˚C (155.7˚F) Price / Set $ 45 / 5 x 20 mL 45 / 5 x 20 mL Originally designed for D-5188-99 Originally designed for D-5191-99 & D-5482-99 ASTM D-5191 & D-5482 Vapor Pressure Standards Vapor Pressure Quality Control Samples Cat. No. Vapor Pressure ASTM-P-124-01-VAP ASTM-P-124-02-VAP ASTM-P-124-03-VAP ASTM-P-124-04-VAP ASTM-P-124-05-VAP ASTM-P-124-06-VAP 68.3kPa (9.91 psi) 68.0kPa (9.86 psi) 51.1kPa (7.41 psi) 46.7kPa (6.77 psi) 22.5kPa (3.26 psi) 7.1kPa (1.03 psi) Technical Note Price / Set $ 65 75 70 115 50 50 / / / / / / 10 10 10 10 10 10 x x x x x x 10 10 10 10 10 10 mL mL mL mL mL mL ASTM Cat. No. Value Added Paks (Cat. No.’s ending in -VAP) provide multiple single units packaged together for both greater stability and cost savings. Consists of pure solvents with known vapor pressure ASTM D-5307-97 Boiling Range Distribution of Crude Petroleum by GC Quantitative Paraffins Standard Qualitative Paraffins Standard D-5307-QUANT D-5307-QUANT-PAK Equal Wt. % D-5307-QUAL $ 40 / 1 x 1 mL D-5307-QUAL-PAK SAVE 20% $ 160 / 5 x 1 mL At stated approx. Wt. % 7 comps. n-Decane n-Undecane n-Dodecane n-Tridecane n-Tetradecane n-Pentadecane n-Hexadecane n-Heptadecane $ 60 / 1 x 2 mL SAVE 20% $ 240 / 5 x 2 mL 16 comps. n-Octadecane n-Eicosane n-Tetracosane n-Octacosane n-Dotriacontane n-Hexatriacontane n-Tetracontane n-Tetratetracontane Propane Butane n-Pentane n-Hexane Wt./Wt. % 10 15 15 15 n-Heptane n-Octane n-Nonane Wt./Wt. % 15 15 15 Column Resolution Mixture Internal Standard D-5307-CR D-5307-CR-PAK At stated approx. Wt. % D-5307-IS-10ML $ 30 / 1 x 10 mL D-5307-IS-10ML-PAK SAVE 20% $ 120 / 5 x 10 mL 4 comps. Wt./Wt. % n-Hexadecane 1.0 n-Octadecane 1.0 $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL 3 comps. n-Octane Wt./Wt. % 98.0 Wt./Wt. % n-Tetradecane 25 n-Pentadecane 25 Member Wt./Wt. % n-Hexadecane 25 n-Heptadecane 25 AccuStandard is an active member in ASTM and strives to keep abreast of ASTM method revisions. If our listed formulation does not meet the most recent method revision, please contact Technical Support, ext. 117 for an updated product. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 29 Method ASTM Standards 5441 Member Originally designed for D-5441-98 ASTM ASTM D-5441 Analysis of Methyl tert-butyl ether (MtBE) by GC The ASTM Committee D-02 on Petroleum Products and Lubricants has issued the Standard Method D-5441-98 for the determination of the purity of methyl tert-butyl ether (MtBE) by Gas Chromatography. This method provides a procedure to measure impurities in MtBE such as C4 to C12 olefins, methyl, isopropyl and tert-butyl alcohols, methyl sec-butyl & methyl tert-amyl ethers, acetone, and methyl ethyl ketones. The presence of these impurities in MtBE can have a direct effect upon the value of the MtBE as a gasoline additive. AccuStandard has formulated the following reference standards to meet the method specifications. Different packaging sizes are available to meet various sample testing capacities . MtBE Contaminant Standard Low Concentration MtBE Contaminant Standard High Concentration D-5441 D-5441-PAK D-5441-10X D-5441-10X-PAK $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL D-5441-5ML $ 100 / 1 x 5 mL D-5441-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL Each comp. at 0.1% Wt./Wt. in MtBE 12 comps. tert-Amyl methyl ether tert-Butanol tert-Butyl ethyl ether 4,4-Dimethyl-2-neopentyl-1-pentene Methanol 2-Methylbutane 2-Methyl-2-butene 2,2',4,6,6'-Pentamethyl-3-heptene Pentane cis-2-Pentene trans-2-Pentene 2,4,4-Trimethyl-1-pentene Qualitative Standard D-5441-QUAL 0.1% Wt./Wt. in n-Dodecane Methanol Isobutylene n-Butane trans-2-butene cis-2-butene 3-Methyl-1-butene Acetone Isopentane 2-Propanol 1-Pentene 2-Methyl-1-butene n-Pentane trans-2-Pentene t-Butanol cis-2-Pentene 2-Methyl-2-butene Cyclopentene $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL D-5441-10X-5ML $ 100 / 1 x 5 mL D-5441-10X-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL Each comp.at 1% Wt./Wt. in MtBE 12 comps. tert-Amyl methyl ether tert-Butanol tert-Butyl ethyl ether 4,4-Dimethyl-2-neopentyl-1-pentene Methanol 2-Methylbutane 2-Methyl-2-butene 2,2',4,6,6'-Pentamethyl-3-heptene Pentane cis-2-Pentene trans-2-Pentene 2,4,4-Trimethyl-1-pentene Quantitative Standard $ 145 / 1 x 1 mL 33 comps. MtBE 2,3-Dimethyl-1-butene 4-Methyl-cis-2-pentene 2-Methylpentane Methylethyl ketone 3-Methylpentane sec-Butyl methyl ether ETBE TAME 3,5-Dimethyl-1-hexene 2,4,4-Trimethyl-1-pentene 2,4,4-Trimethyl-2-pentene 3,4,4-Trimethyl-trans-2-pentene 2,3,4-Trimethyl-2-pentene 4,4-Dimethyl-2-neopentyl-1-pentene 2,2’,4,6,6’-Pentamethyl-3-heptene D-5441-QUANT 0.1% Wt./Wt. in n-Dodecane $ 130 / 1 x 1 mL 29 comps. For our complete line of Organic Standards and Inorganic Standards, request a copy of the Catalog(s). Methanol 2-Methylpentane 3-Methyl-1-butene Methyl ethyl ketone Acetone 3-Methylpentane Isopentane sec-Butyl methyl ether 2-Propanol Ethyl tert-butyl ether 1-Pentene TAME 2-Methyl-1-butene 3,5-Dimethyl-1-hexene n-Pentane 2,4,4-Trimethyl-1-pentene trans-2-Pentene 2,4,4-Trimethyl-2-pentene t-Butanol 3,4,4-Trimethyl-trans-2-pentene cis-2-Pentene 2,3,4-Trimethyl-2-pentene 2-Methyl-2-butene 4,4-Dimethyl-2-neopentyl-1-pentene Cyclopentene 2,2’,4,6,6’-Pentamethyl-3-heptene MtBE 2,3-Dimethyl-1-butene 4-Methyl-cis-2-pentene MtBE Resolution Test Mixture D-5441-RES D-5441-RES-PAK $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL D-5441-RES-5ML $ 60 / 1 x 5 mL D-5441-RES-5ML-PAK SAVE 20% $ 240 / 5 x 5 mL Each comp. at 1% Wt./Wt. in MtBE 3 comps. trans-2-Pentene tert-Butanol 30 cis-Pentene Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5442 5443 5453 Member Originally designed for D-5442-93 ASTM D-5442 (Reapproved 1998) Analysis of Petroleum Waxes by GC Wt./Wt. % n-Dodecane 0.02 n-Tetradecane 0.03 n-Hexadecane 0.04 n-Octadecane 0.05 n-Eicosane 0.06 n-Docosane 0.08 $ 95 / 5 x 1 mL 16 comps. Wt./Wt. % n-Tetracosane 0.10 n-Hexacosane 0.12 n-Octacosane 0.12 n-Triacontane 0.10 n-Dotriacontane 0.08 Retention Time Standard Mix 1 D-5442-RT1 Equal parts by weight n-Hexadecane (c16) n-Octadecane (c18) n-Eicosane (c20) n-Docosane(c22) n-Tetracosane (c24) n-Hexacosane (c26) Wt./Wt. % n-Hexatriacontane 0.06 n-Tetracontane 0.05 n-Tetratetracontane 0.04 n-Pentacontane 0.03 n-Hexacontane 0.02 NEW n-Eicosane n-Tetracontane Wt./Wt. % 0.05 0.05 $ 55 / 500 mg 16 comps. n-Dodecane (c12) n-Tetradecane (c14) n-Hexadecane (c16) n-Octadecane (c18) n-Eicosane (c20) n-Docosane (c22) n-Tetracosane (c24) n-Hexacosane (c26) n-Octacosane (c28) n-Triacontane (c30) n-Dotriacontane (c32) n-Hexatriacontane (c36) n-Tetracontane (c40) n-Tetratetracontane (c44) See ASTM Methods D-3710, D-5307, D-6352 for additional calibration standards for hydrocarbon analysis or page 15 for new proposed methods. NEW Retention Time Standard Mix 2 D-5442-RT2 Equal parts by weight $ 50 / 500 mg 12 comps. ASTM D-5443 D-5442-CR-PAK $ 40 / 5 x 1 mL At stated Wt. % in Cyclohexane 2 comps. n-Octacosane (c28) n-Triacontane (c30) n-Dotriacontane (c32) n-Hexatriacontane (c36) n-Tetracontane (c40) n-Tetratetracontane (c44) n-Pentacontane (c50) n-Hexacontane (c60) Paraffin, Naphthene, and Aromatic Hydrocarbon Type Analysis in Originally designed for D-5443-93 (Reapproved 1998) Petroleum Distillates through 200°C by Multi-dimensional GC Hydrocarbon Test Mixture D-5443-93-HTM At stated Wt. % Wt./Wt. % 1cis,2-Dimethylcyclohexane 5.00 Isooctane 5.00 n-Octane 5.00 1cis,2 cis,4-Trimethylcyclohexane 4.25 n-Nonane 4.50 n-Decane 4.25 n-Undecane 3.50 n-Dodecane 3.25 Benzene 2.25 Toluene 2.25 Wt./Wt. % Cyclopentane 1.00 n-Pentane 1.00 Cyclohexane 2.00 2,3-Dimethylbutane 2.00 n-Hexane 2.00 n-Hexene 1.50 Methylcyclohexane 4.25 4-Methyl-1-hexene 1.50 n-Heptane 3.50 ASTM D-5453 $ 100 / 1 x 1 mL 28 comps. Wt./Wt. % trans-Decahydronaphthelene 4.25 n-Tetradecane 4.50 Ethylbenzene 4.50 o-Xylene 4.25 n-Propylbenzene 5.00 1,2,4-Trimethylbenzene 4.50 1,2,3-Trimethylbenzene 5.00 1,2,4,5-Tetramethylbenzene 5.00 Pentamethylbenzene 5.00 Originally designed for D-5453-00 Total Sulfur in Light Hydrocarbons, Motor Fuels and Oils by Ultraviolet Fluorescence Standards of Interests See pages 6-11 for a comprehensive line of Certified Sulfur Calibration Standards, Petrocheck, & Petrotest quality control products, pages 1-2. 3 D-545 Meets es uidelin EPA G FG for R is Analys Low Level Sulfur Set D-5453-LL-SET $ 90 / 5 x 2 mL The set contains the following 5 standards in Isooctane Cat. No. Description D-5453-LL-BL D-5453-LL-01 D-5453-LL-02 D-5453-LL-03 D-5453-LL-04 Sulfur Sulfur Sulfur Sulfur Sulfur Blank @ 0.5 @ 2.5 @ 5.0 @ 10.0 Unit ng/µL ng/µL ng/µL ng/µL 2 2 2 2 2 mL mL mL mL mL Technical Note Real World Sulfur in Various Gasoline & Fuels QC Samples SBPT-LSGAS $ 25 / 2 x 15 mL Parameter Method Approx .Range Sulfur D-5453-00 0 - 50 µg/g Mid Level Sulfur Set High Level Sulfur Set D-5453-ML-SET $ 90 / 6 x 2 mL The set contains the following 5 standards in Isooctane D-5453-HL-SET $ 90 / 5 x 2 mL The set contains the following 5 standards in Isooctane Cat. No. Description D-5453-ML-BL D-5453-ML-01 D-5453-ML-02 D-5453-ML-03 D-5453-ML-04 D-5453-ML-05 Sulfur Sulfur Sulfur Sulfur Sulfur Sulfur Blank @ 5.0 @ 25 @ 50 @ 100 @ 200 Unit ng/µL ng/µL ng/µL ng/µL ng/µL 2 2 2 2 2 2 mL mL mL mL mL mL Cat. No. Description Unit D-5453-HL-BL D-5453-HL-01 D-5453-HL-02 D-5453-HL-03 D-5453-HL-04 Sulfur Sulfur Sulfur Sulfur Sulfur ng/µL ng/µL ng/µL ng/µL Blank @ 100 @ 250 @ 500 @ 1000 2 2 2 2 2 mL mL mL mL mL Due to the wide variety of recommended solvents and starting materials mentioned in the preparation of the sulfur standards, please review the current product offering listed for certified sulfur standards. Should AccuStandard’s current sulfur standard line be missing the necessary standards for your application, please use our custom quotation request form to indicate your required formulation. For ppb Sulfur measurements, see page 6-11. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 31 ASTM D-5442-PAK At stated Wt. % in Cyclohexane Standards of Interests Column Resolution Standard Quantitative Wax Standard Method ASTM Standards 5480 5482 5501 5580 Member Originally designed for D-5480-95 ASTM ASTM D-5480 Engine Oil Volatility by GC Stock Column Resolution Standard Internal Standard Solution D-5480-CR-PAK Each comp. at 10 µg/mL in CS2 $ 40 / 5 x 1 mL 5 comps. D-5480-CR-100X-PAK Each comp. at 1000 µg/mL in CS2 $ 50 / 5 x 1 mL 5 comps. D-5480-IS-5ML $ 30 / 1 x 5 mL D-5480-IS-5ML-PAK SAVE 20% $ 120 / 5 x 5 mL Each comp. at equal weights 3 comps. n-Decane n-Dodecane n-Hexadecane n-Decane n-Undecane n-Octadecane n-Tetracosane n-Dodecane Tetracosane (Solution A) D-5480-C40-5ML D-5480-C40-5ML-PAK 500 µg/mL in CS2 $ 15 / 1 x 5 mL SAVE 20% $ 60 / 5 x 5 mL Standards of Interest Alternative n-Paraffin standards are available on page 15 for further method development work or more Detailed Hydrocarbon Analysis (DHA). n-Tetracosane Originally designed for D-5482-99 & D-5191-99 ASTM D-5482 & D-5191 Vapor Pressure Standards Vapor Pressure Quality Control Samples Cat. No. Vapor Pressure ASTM-P-124-01 ASTM-P-124-02 ASTM-P-124-03 ASTM-P-124-04 ASTM-P-124-05 ASTM-P-124-06 68.3kPa (9.91 psi) 68.0kPa (9.86 psi) 51.1kPa (7.41 psi) 46.7kPa (6.77 psi) 22.5kPa (3.26 psi) 7.1kPa (1.03 psi) Technical Note Price / Set of 10 $ 65 75 70 125 50 50 / / / / / / 10 10 10 10 10 10 x x x x x x 10 10 10 10 10 10 Consists of pure solvents with known vapor pressure. mL mL mL mL mL mL Technical Note ASTM D-5501 Ethanol Content of Denatured Fuel Ethanol by GC Originally designed for D-5501-94 Denatured Fuel Ethanol Calibration Set D-5501-94-SET $ 75 / set of 7 x 1 mL Cat. No. Comp.1 Wt./ Wt.% Comp.2 Wt./ Wt.% Comp.3 Wt./ Wt.% D-5501-94-01 D-5501-94-02 D-5501-94-03 D-5501-94-04 D-5501-94-05 D-5501-94-06 D-5501-94-07 Ethanol Ethanol Ethanol Ethanol Ethanol Ethanol Ethanol Methanol Methanol Methanol Methanol Methanol Methanol Methanol Heptane Heptane Heptane Heptane Heptane Heptane Heptane ASTM D-5580 92 93 94 95 96 97 98 0.6 0.5 0.4 0.3 0.2 0.1 0.05 Unit 7.4 6.5 5.6 4.7 3.8 2.9 1.95 1 1 1 1 1 1 1 x x x x x x x 1 1 1 1 1 1 1 mL mL mL mL mL mL mL Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene, C9 and Heavier Aromatics, & Total Aromatics in Finished Gasoline by GC Additional Oxygenate calibration, check standards, and independent reference standards can be found in ASTM method D-4815 (page 24) or D-5622-94 (page 37). The required QA/QC procedures in EPA methods stipulate a calibration check standard be used once per analytical batch or per 10 sample set. AccuStandard has bulk packaged check standards to meet this increased usage. Originally designed for D-5580-00 Aromatics Quantitative Calibration Mixes (without Internal Standard) D-5580-95-CAL-SET-10ML Analyte Benzene Toluene Ethylbenzene o-Xylene 1,2,4-Trimethylbenzene Isooctane $ 300 / set of 5 x 10 mL of 6 component mix Analyte Calibration range Std. 1 Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % 0.10 1.00 0.50 0.50 0.50 0.10 15.00 0.50 1.00 1.00 82.40 0.50 10.00 1.00 2.50 10.00 76.00 1.00 5.00 2.50 10.00 0.50 81.00 2.00 2.50 5.00 5.00 5.00 80.50 5.00 1.00 10.00 0.50 2.50 81.00 - 5.00 15.00 10.00 10.00 10.00 Aromatics Quantitative Calibration Mixes (with Internal Standard) D-5580-95-CAL-IS-SET Analyte Benzene Toluene Ethylbenzene o-Xylene 1,2,4-Trimethylbenzene 2-Hexanone (Internal Std.) Isooctane 32 $ 100 / set of 5 x 1 mL of 7 component mix Analyte Calibration range Std. 1 Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % 0.09 0.90 0.45 0.45 0.45 0.09 13.50 0.45 0.90 0.90 10.00 74.16 0.45 9.00 0.90 2.25 9.00 10.00 68.40 0.90 4.50 2.25 9.00 0.45 10.00 72.90 1.80 2.25 4.50 4.50 4.50 10.00 72.45 4.50 0.90 9.00 0.45 2.25 10.00 72.90 - 4.50 13.50 9.00 9.00 9.00 Quality System is Certified comply with the International 9001 Quality Standard ASTM to D-5580-00 Continued on the ISO Next Page ASTM Standards Method 5580 Member Originally designed for D-5580-00 ASTM D-5580-00 Benzene, Toluene, Ethylbenzene, m/p-Xylene, o-Xylene, C9 & Continued Heavier Aromatics, and Total Aromatics in Finished Gasoline by GC Valve Timing Calibration Mix (without Internal Standard) M-GRA-VT/IS-AS M-GRA-VT/IS-AS-PAK Each at stated conc. M-GRA-VT-AS-10ML $ 100 / 1 x 10 mL M-GRA-VT-AS-10ML-PAK SAVE 20% $ 400 / 5 x 10 mL Each at stated conc. 5 comps. Wt./Wt. % Benzene 5.0 Toluene 5.0 Ethylbenzene 10.0 o-Xylene 10.0 Isooctane 70.0 $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 6 comps. Wt./Wt. % Benzene 4.5 Toluene 4.5 Ethylbenzene 9.0 o-Xylene 9.0 2-Hexanone (Internal Std.) 10.0 Isooctane 63.0 Technical Note Selectivity Check Standard Internal Standard M-GRA-IS-AS-5ML $ 10 / 1 x 5 mL M-GRA-IS-AS-5ML-PAK SAVE 20% $ 40 / 5 x 5 mL M-GRA-SCS-AS M-GRA-SCS-AS-PAK Each at stated conc. Wt./Wt. % 1.5 98.5 n-Dodecane Isooctane 2-Hexanone (Neat) $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL 2 comps. Daily Quality Control Standard without Internal Standard Daily Quality Control Standard without Internal Standard D-5580-QC-R1 D-5580-QC-R1-PAK D-5580-QC D-5580-QC-PAK Wt./Wt. % n-Hexane 12 n-Heptane 20 n-Octane 15 n-Decane 10 n-Dodecane 1 Isooctane 20 Benzene 1 $ 125 / 1 x 10 mL SAVE 20% $ 500 / 5 x 10 mL 14 comps. Wt./Wt. Toluene Ethylbenzene p-Xylene o-Xylene 1,2,4-Trimethylbenzene 1,2,4,5-Tetramethylbenzene Naphthalene % 9 2 3 2 3 1 1 Wt./Wt. % n-Hexane 12 n-Heptane 20 n-Octane 15 n-Decane 10 n-Triadecane 1 Isooctane 20 Benzene 1 $ 125 / 1 x 10 mL $ 500 / 5 x 10 mL 14 comps. Wt./Wt. Toluene Ethylbenzene p-Xylene o-Xylene 1,2,4-Trimethylbenzene 1,2,4,5-Tetramethylbenzene Naphthalene % 9 2 3 2 3 1 1 ASTM D-5580 Gasoline Refinery Quality Control Standard AccuStandard was requested by the Petrochemical Industry to manufacture the following QA/QC standards for ASTM Method D-5580. The configuration of your instrument valve time switching and the pre-column incorporated determines which QA/QC standard provides optimum performance when analyzing gasolines samples by Method D-5580. Use of the D-5580 standards in conjunction with the real world gasoline AccuPetroTest & AccuPetroCheck Consensus Value Reference Material (see pages 1-2) can provide added assurance that the analytical results being generated by the laboratory are reproducible and the analytical system is performing to method specifications. Exclusive Aromatic Chemical Reference Material Benefits from AccuStandard Every analyte in each solution is individually weighed Actual weights and weight percents are available with all ASTM/EPA solutions Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 33 ASTM Valve Timing Calibration Mix (with Internal Standard) Method ASTM Standards 5599 ASTM Member Originally designed for D-5599-95 ASTM D-5599 Oxygenates in Gas by GC & O-FID ASTM Oxygenates Calibration Curve with Internal Standard M-GRO-CAL/IS-SET M-GRO-CAL/IS-SET-PAK Analyte Calibration range $ 250 / set of 8 x 1 mL $ 1,000 / 5 x (8 x 1) mL of 15 Comp. Mix Technical Note Every analyte in each solution is individually weighed Actual weights and weight percents are provided with all ASTM/EPA Solutions Std. 1 Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % Std. 6 Wt. % Std. 7 Wt. % Std. 8 Wt. % --12 2 0.5 2 5 1 --2 --0.3 1 --- 0.1 --1 0.1 --17 --0.5 0.5 3.5 1 --3.5 2.5 3 --1 0.7 --0.5 0.3 --18 --0.3 1 ----0.1 --0.2 --0.1 0.1 1 7.5 0.5 --18 5 8 0.3 2 1 1 --2 0.1 --0.1 0.5 7.5 0.5 5 --0.3 --2.5 2.5 1 0.3 1 2 0.1 12 1 1 0.5 --0.4 10 0.7 ----12 --2 --- --------------------------- 1,2- Dimethoxyethane (ISTD) RFA Gasoline 4 70.2 4 68.8 4 68.7 4 68.5 4 68.5 4 68.8 4 68.4 --100 Total oxygenates & ISTD 29.8 31.2 31.3 31.5 31.5 31.2 31.6 0 Methanol Ethanol Isopropanol t-Butanol Propanol MtBE sec-Butanol Diisopropyl ether iso-Butanol EtBE t-Pentanol Butanol TAME 0.1 - 5.0 1.0 - 12.0 0.1 - 2.0 0.1 - 2.0 0.2 - 2.0 1.0 - 17.0 0.1 - 2.5 0.1 - 2.0 0.1 - 2.0 1.0 - 18.0 0.1 - 2.0 0.1 - 2.0 1.0 - 18.0 Oxygenates Calibration Curve without Internal Standard M-GRO-CAL-SET $ 850 / set of 8 x 10 mL of 14 Comp. Mix Analyte Calibration range Std. 1 Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % Std. 6 Wt. % Std. 7 Wt. % Std. 8 Wt. % --12 2 0.5 2 5 1 --2 --0.3 1 --- 0.1 --1 0.1 --17 --0.5 0.5 3.5 1 --3.5 2.5 3 --1 0.7 --0.5 0.3 --18 --0.3 1 ----0.1 --0.2 --0.1 0.1 1 7.5 0.5 --18 5 8 0.3 2 1 1 --2 0.1 --0.1 0.5 7.5 0.5 5 --0.3 --2.5 2.5 1 0.3 1 2 0.1 12 1 1 0.5 --0.4 10 0.7 ----12 --2 --- --------------------------- RFA Gasoline 74.2 64.8 64.7 64.5 64.5 64.8 64.4 100 Total oxygenates 25.8 27.2 27.3 27.5 27.5 27.2 27.6 0 Methanol Ethanol Isopropanol t-Butanol Propanol MtBE sec-Butanol Diisopropyl ether iso-Butanol EtBE t-Pentanol Butanol TAME 0.1 - 5.0 1.0 - 12.0 0.1 - 2.0 0.1 - 2.0 0.2 - 2.0 1.0 - 17.0 0.1 - 2.5 0.1 - 2.0 0.1 - 2.0 1.0 - 18.0 0.1 - 2.0 0.1 - 2.0 1.0 - 18.0 Oxygenate Calibration Curves ISTD-Free and Larger Packaging Size. AccuStandard has received requests from the Petroleum Industry to formulate our D-5599 Oxygenate product without internal standard (ISTD) and package it in a larger volume. We have met those requests by introducing the M-GRO-CAL-SET calibration curve. This curve is manufactured without incorporating an internal standard and is packaged in Ready-to-Use 10 mL sample volume. The certified oxygenate calibration curve can be used in combination with other aromatic standards for combined oxygenate/aromatic analysis, to change the amount of internal standard added, or to incorporate alternative internal standard analytes. 9 D-559 Meets es uidelin EPA G FG for R is Analys Technical Note AccuStandard’s M-GRO oxygenate calibration curve has been successfully used by Petroleum Refineries and supporting laboratories for both ASTM Method D-5599 and ASTM Method D-4815. In addition, AccuStandard’s certified oxygenate chemical reference materials provide the following features and benefits for superior performance and value. Benefits from AccuStandard’s Oxygenates 34 Features: Benefits: Analytes checked for chemical purity & water content The use & validation of the highest purity neats enhance the integrity of the standard. Analyzed by Independent Laboratories Independent product validation of certified values. Certified method specific calibration standards Increased confidence in analytical results. Elimination of standards preparation Time is utilized quantifying samples. Internal Standards incorporated Ready-to-Inject Standards. Weights and weight percents provided Ease of use in performing back calculations. All necessary solutions included Provides single source for sample analysis. Variations in Packaging size Meet laboratory sample volumes. Economical Time is spent on analysis rather than preparing stds. 7 stds. used to generate 5 point curve Generate a 5 point curve in 30% less time than competitors' 10 standard set. Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5599 Member ASTM D-5599 Originally designed for D-5599-95 Oxygenates in Gasoline by GC & O-FID Continued Daily Quality Control Standard (without Internal Standard) Revised Daily Quality Control Standard (without Internal Standard) M-GRO-QC-10ML $ 100 / 1 x 10 mL M-GRO-QC-10ML-PAK SAVE 20% $ 400 / 5 x 10 mL M-GRO-QC-R-10ML $ 100 / 1 x 10 mL M-GRO-QC-R-10ML-PAK SAVE 20% $ 400 / 5 x 10 mL Compound Target Compound Target Oxygenate Wt. % Oxygenate Wt. % Compound Oxygenate Target Wt. % Methanol Ethanol Isopropanol t-Butanol Propanol MtBE sec-Butanol Di-isopropyl ether 1 1 1 1 1 3 1 3 Compound Oxygenate Target Wt. % iso-Butanol EtBE t-Pentanol Butanol TAME 1 3 1 1 3 RFA Gasoline 79 14 comps. Methanol Ethanol Isopropanol t-Butanol Propanol MtBE sec-Butanol Di-isopropyl ether 1 1 1 1 1 3 1 1 100 iso-Butanol EtBE t-Pentanol Butanol TAME 1 3 1 1 3 RFA Gasoline 81 14 comps. Revised Daily Quality Control Standard (with Internal Standard) M-GRO-QC/IS-5ML $ 75 / 1 x 5 mL M-GRO-QC/IS-5ML-PAK SAVE 27% $ 275 / 5 x 5 mL M-GRO-QC-R/IS-5ML $ 75 / 1 x 5 mL M-GRO-QC-R/IS-5ML-PAK SAVE 27% $ 275 / 5 x 5 mL Target Wt. % Methanol Ethanol Isopropanol t-Butanol Propanol MtBE sec-Butanol 1 1 1 1 1 3 1 Compound Oxygenate Target Wt. % Di-isopropyl ether iso-Butanol EtBE t-Pentanol Butanol TAME RFA Gasoline 3 1 3 1 1 3 Compound Oxygenate Target Wt. % Methanol Ethanol Isopropanol t-Butanol Propanol MtBE sec-Butanol 1 1 1 1 1 3 1 79 Compound Oxygenate Target Wt. % Di-isopropyl ether iso-Butanol EtBE t-Pentanol Butanol TAME RFA Gasoline 1 1 3 1 1 3 81 1,2-Dimethoxyethane (ISTD) is combined with 100 the above 14 comps. in a 4 to 100 weight ratio 1,2-Dimethoxyethane (ISTD) is combined with 100 the above 14 comps. in a 4 to 100 weight ratio 15 comps. 15 comps. Gasoline Refinery Blank (with Internal Standard) O-FID/EPA Gasoline Refinery Internal Standard M-GRO-BLNK/IS-10ML $ 15 / 1 x 10mL M-GRO-BLNK/IS-10ML-PAK SAVE 20% $ 60 / 5 x 10mL 2 comps. M-GRO-IS-5ML M-GRO-IS-5ML-PAK 1,2- Dimethoxyethane (ISTD) RFA Gasoline Wt. % 4 96 Technical Note The Daily Quality Control Standard M-GRO-QC-R was developed in response to your requests for a QC mix bracketed by the Calibration Curve. AccuStandard reduced the diisopropyl ether content from 3 Wt. % to 1 Wt. % to meet the method specifications. 100 Daily Quality Control Standard (with Internal Standard) Compound Oxygenate ASTM ASTM/EPA Oxygenate Quality Control Standards 9 D-559 Meets es uidelin EPA G FG for R is Analys Technical Note Additional Oxygenate calibration, check standards, and independent reference standards can be found in ASTM method D-4815 (page 24) or D-5622 (page 37). The required QA/QC procedures in EPA methods stipulate a calibration check standard be used once per analytical batch or per 10 sample set. AccuStandard has bulk packaged check standards to meet this increased usage. $ 10 / 1 x 5 mL SAVE 20% $ 40 / 5 x 5 mL 1,2- Dimethoxyethane (ISTD) O-FID Gasoline Refinery Blank M-GRO-BLNK-10ML M-GRO-BLNK-10ML-PAK $ 10 / 1 x 10mL SAVE 20% $ 40 / 5 x 10mL RFA Gasoline (neat) Fax 203-786-5287 • AccuStandard • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 35 Method Oxygenates Using O-FID 5599 ASTM Member EPA O-FID Oxygenate Petrochemical Standards ASTM AccuStandard has formulated this second oxygenate version to meet the specific analyte requirements set forth in the EPA methodology. Originally designed for D-5599-95 ASTM D-5599 EPA Gasoline Refinery Oxygenates Calibration Curves EPA O-FID Quantitative Calibration Mixes (without Internal Standard) M-GRO-CAL-EPA-SET-10ML Methanol Ethanol t-Butanol MtBE RFA Gasoline $ 350 / set of 5 x 10 mL 5 comps. Analyte Calibr. range Std. 1 Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % 0.30 0.30 0.30 0.30 6.00 0.30 0.30 15.00 78.40 12.00 3.00 6.00 7.50 71.50 3.00 6.00 9.00 11.25 70.75 0.30 9.00 12.00 3.75 74.95 9.00 12.00 3.00 0.30 75.70 - 12.00 12.00 12.00 15.00 For our complete line of Organic Standards, request a copy of our Catalog. EPA O-FID Quantitative Calibration Mixes (with Internal Standard) M-GRO-CAL-IS/EPA-SET $ 175 / set of 5 x 1 mL 6 comps. Methanol Ethanol t-Butanol MtBE 1,2-Dimethoxyethane (ISTD) RFA Gasoline Analyte Calibr. range Std. 1 Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % 0.29 0.29 0.29 0.29 5.70 0.29 0.29 14.25 5.00 74.48 11.40 2.85 5.70 7.13 5.00 67.93 2.85 5.70 8.55 10.69 5.00 67.31 0.29 8.55 11.40 3.56 5.00 71.20 8.55 11.40 2.85 0.29 5.00 71.92 - 11.40 11.40 11.40 14.29 EPA O-FID Quantitative Calibration Check Standard (without Internal Standard) EPA O-FID Quantitative Calibration Check Standard (with Internal Standard) M-GRO-EPA-CC-10ML $ 50 / 1 x 10 mL M-GRO-EPA-CC-10ML-PAKSAVE 20% $ 200 / 5 x 10 mL 5 comps. M-GRO-EPA-CC/IS-5ML $ 35 / 1 x 5 mL M-GRO-EPA-CC/IS-5MLPAK SAVE 20% $ 150 / 5 x 5 mL 6 comps. Wt./Wt. % Methanol 4.0 Ethanol 8.0 tert-Butanol 5.0 Wt./Wt. % Methanol 3.80 Ethanol 7.60 tert-Butanol 4.75 Wt./Wt. % Methyl tert-butyl ether 12.0 RFA gasoline 71.0 EPA O-FID Spiking Solution M-GRO-EPA-SP-5ML $ 50 / 1 x 5 mL M-GRO-EPA-SP-5ML-PAK SAVE 20% $ 200 / 5 x 5 mL 4 comps. Wt./Wt. % Methanol 14.3 Ethanol 28.6 Wt./Wt. % tert-Butanol 14.3 Methyl tert-butyl ether 42.8 Wt./Wt. % Methyl tert-butyl ether 11.40 RFA gasoline 67.45 DME (internal standard) 5.0 Oxygenate Free Gasoline Refinery Blank M-GRO-BLNK-10ML M-GRO-BLNK-10ML-PAK Technical Note Additional Oxygenate calibration, check standards, and independent reference standards can be found in ASTM method D-4815 (page 24) or D-5622 (page 37). The required QA/QC procedures in EPA methods stipulate a calibration check standard be used once per analytical batch or per 10 sample set. AccuStandard has bulk packaged check standards to meet this increased usage. $ 10 / 1 x 10 mL SAVE 20% $ 40 / 5 x 10 mL RFA Gasoline (neat) Internal Standard M-GRO-IS-5ML M-GRO-IS-5ML-PAK $ 10 / 1 x 10 mL SAVE 20% $ 40 / 5 x 10 mL 1,2-Dimethoxyethane (ISTD) Cross Reference Table ASTM IP ISO DIN JIS AFNOR sorted by ASTM Method see beginning of Catalog 36 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5600 5622 Member Originally designed for D-5600-98 ASTM D-5600 Trace Metals in Petroleum Coke by ICP-AES Hydrochloric Acid Diluent D-5600-01-1 $ 225 / 1 x 100 mL 500 µg/mL each in 2-5% HNO3 tr. HF 12 comps. D-5600-BLH-5 D-5600-BLH-L Aluminum Barium Calcium Iron Magnesium Manganese Nickel Silicon Sodium Titanium Vanadium Zinc Standards of Interest Individual ICP Standards are on pages 67-72. $ 50 / 1 x 500 mL $ 65 / 1 x 1 L 20% HCl in ASTM Type II water Lithium Borate Diluent D-5600-LIB-1 D-5600-LIB-5 $ 125 / 1 x 100 mL $ 180 / 1 x 500 mL 2.0% Lithium Borate in 10% HCl ASTM D-5622 Total Oxygen in Gasoline & MeOH Fuels by Reductive Pyrolysis Cat. No. Description (2 x 10 mL, plus an RFA gasoline blank) Oxygenate Wt. % ASTM-P-0061-SET * ASTM-P-0062-SET * ASTM-P-0063-SET * ASTM-P-0064-SET * ASTM-P-0065-SET * ASTM-P-0066-SET * ASTM-P-0067-SET * ASTM-P-0068-SET * ASTM-P-0069-SET * Ethanol in Oxygenate free RFA gasoline Ethanol in Oxygenate free RFA gasoline t-Amyl methyl ether in Oxygenate free RFA gasoline t-Amyl methyl ether in Oxygenate free RFA gasoline Ethyl t-butyl ether in Oxygenate free RFA gasoline Ethyl t-butyl ether in Oxygenate free RFA gasoline Methyl t-butyl ether in Oxygenate free RFA gasoline Methyl t-butyl ether in Oxygenate free RFA gasoline Methanol & t-Butanol in Oxygenate free RFA gasoline 5.0 10.0 10.0 15.0 10.0 15.0 10.0 15.0 10.0 & 5.0 * Each Set includes M-GRO-BLNK-10ML Oxygenate Free Gasoline Refinery Blank M-GRO-BLNK-10ML $ 10 / 1 x 10 mL RFA Gasoline (neat) Standards of Interests See ASTM Methods D-4815 (page 24) and D-5599 (pages 34-36) for additional oxygenate calibration standards. Unit 3 3 3 3 3 3 3 3 3 D-5600 Ready-to-Aspirate Standards AccuStandard has formulated the following stock standards for ASTM Method D-5600. We have prepared numerous Ready-toAspirate ICP multi-element solutions. Should your company want to eliminate the preparation process for Inorganic standards contact our Technical Department for a quote on a Ready-toAspirate working level Inorganic standard. Originally designed for D-5622-95 Price x x x x x x x x x 10 10 10 10 10 10 10 10 10 mL mL mL mL mL mL mL mL mL $ 50 50 50 50 50 50 50 50 50 Technical Note Use M-GRO-BLNK-10ML as an oxygenate free RFA gasoline matrix to make up your own oxygenate standards or call our Technical Dept. to have a Standard custom made for you. Technical Note AccuStandard’s Oxygenate reference fuel line was designed as a cost effective alternative for Petrochemical Laboratories. All oxygenate blends come with a certificate to maintain traceability links to NIST SRMs (when available). By packaging the standard in 10 mL sealed ampules your laboratory will realize cost savings. The 10 mL size avoids having special packaging and hazardous material fees billed to your invoice. For our complete line of Inorganic Standards, request a copy of our Inorganics Catalog. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 37 ASTM Multi-Element Calibration Standard Technical Note Method ASTM Standards 5623 Member ASTM ASTM D-5623 Originally designed for D-5623-94 Sulfur Compounds in Light Petroleum Liquids by GC and Sulfur Selective Detection This set of qualitative Sulfur Standards are formulated for research evaluation of the presence of the sulfur analytes or their breakdown products. ASTM-P-0091-10X-SET Approx. 2.0 mg/mL each in Toluene $ 625 / set of 22 x 1 mL Analyte Cat. No. Unit Hydrogen sulfide Carbonyl sulfide (Carbon oxysulfide) Methyl mercaptan (Methanethiol) Ethyl mercaptan (Ethanethiol) Methyl sulfide (Dimethyl sulfide) Carbon disulfide 2-Propanethiol (Isopropyl mercaptan 2-Methyl-2-propanethiol (t-butyl mercaptan) 1-Propanethiol (Propyl mercaptan) Ethyl methyl sulfide 1-Methyl-1-propanethiol (2-butanethiol) Thiophene 2-Methyl-1-propanethiol (Isobutyl mercaptan) Diethyl sulfide 1-Butanethiol (Butyl mercaptan) Methyl disulfide (Dimethyl disulfide) 2-Methylthiophene 3-Methylthiophene Diethyl disulfide (Ethyl disulfide) 3-Methylbenzo[b]thiophene 5-Methylbenzo[b]thiophene Diphenyl sulfide ASTM-P-0091-01-10X ASTM-P-0091-02-10X ASTM-P-0091-03-10X ASTM-P-0091-04-10X ASTM-P-0091-05-10X ASTM-P-0091-06-10X ASTM-P-0091-07-10X ASTM-P-0091-08-10X ASTM-P-0091-09-10X ASTM-P-0091-10-10X ASTM-P-0091-11-10X ASTM-P-0091-12-10X ASTM-P-0091-13-10X ASTM-P-0091-14-10X ASTM-P-0091-15-10X ASTM-P-0091-16-10X ASTM-P-0091-17-10X ASTM-P-0091-18-10X ASTM-P-0091-19-10X ASTM-P-0091-20-10X ASTM-P-0091-21-10X ASTM-P-0091-22-10X 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 x x x x x x x x x x x x x x x x x x x x x x 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 Price mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL $ 35 35 35 35 35 35 35 35 35 35 35 35 35 35 35 35 35 35 35 35 75 35 Custom Ampulling for Bulk Quantity Requirements • Fill Volumes from 0.2 mL to 20 mL • Flammables • QC Services available AccuStandard has the resources and equipment to meet your custom packaging requirements. Our full automated filler-sealer can accommodate a fill range from 0.2 to 20 mL, and ampule sizes from 1 mL to 20 mL. AccuStandard has extensive experience with Round Robin samples for ASTM committees. Call our Technical Department for a quotation. We can reduce your costs by using the Cozzoli Auto Filling/Sealing Machine to package just the right size product for your application. 38 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5599 Member ASTM D-5708 Nickel, Vanadium, & Iron in Crude Oils & Residual Fuels by ICP-AES Originally designed for D-5708-95a Test Method A - ICP with an Organic Solvent Specimen Solution Sulfur and Metals in Mineral Oil Cat. No. Sulfur Conc. (Wt. %) Iron Conc. (µg/g) Nickel Conc. (µg/g) Vanadium Conc. (µg/g) Price 100 mL 0.00 0.50 1.00 2.00 2.50 3.00 3.50 4.50 5.00 5.50 0 300 500 100 200 400 0 500 100 300 200 50 0 10 100 80 40 5 60 0 100 50 20 100 0 500 25 250 100 400 300 200 0 250 500 50 $ 200 200 200 200 200 200 200 200 200 200 200 200 D-5708-A-10X $ 150 / 4 oz. 100 µg/g in 20 cSt mineral oil 3 comps. Iron Nickel Vanadium Standards of Interests See Table of Contents for the Wear Metals Group pages. For our complete line of Inorganic Standards, request a copy of our Inorganics Catalog WEAR METALS ASTM-P-0102-01 ASTM-P-0102-02 ASTM-P-0102-03 ASTM-P-0102-04 ASTM-P-0102-05 ASTM-P-0102-06 ASTM-P-0102-07 ASTM-P-0102-08 ASTM-P-0102-09 ASTM-P-0102-10 ASTM-P-0102-11 ASTM-P-0102-12 Stock Multi-Element in Mineral Oil $ 1850 / 100 mL ASTM ASTM-P-0102-SET Sulfur and Metals in Residual Fuel Oil ASTM-P-0103-SET Cat. No. ASTM-P-0103-01 ASTM-P-0103-02 ASTM-P-0103-03 ASTM-P-0103-04 ASTM-P-0103-05 ASTM-P-0103-06 ASTM-P-0103-07 ASTM-P-0103-08 ASTM-P-0103-09 ASTM-P-0103-10 ASTM-P-0103-11 ASTM-P-0103-12 $ 2100 / 100 mL Sulfur Conc. (Wt. %) Iron Conc. (µg/g) Nickel Conc. (µg/g) Vanadium Conc. (µg/g) Price 100 mL 0.00 0.50 1.00 2.00 2.50 3.00 3.50 4.50 5.00 5.50 0 300 500 100 200 400 0 500 100 300 200 50 0 10 100 80 40 5 60 0 100 50 20 100 0 500 25 250 100 400 300 200 0 250 500 50 $ 200 200 200 200 200 200 200 200 200 200 200 200 Test Method B - ICP after Acid Decomposition of Sample Stock Multi-Element Aqueous Standard Working Level Multi-Element Aqueous Standard D-5708-B-10X-1 D-5708-B-10X-5 Each at 100 µg/mL in 2-5% HNO3 Iron Nickel $ 60 / 100 mL $ 115 / 500 mL 3 comps. Vanadium D-5708-B-5 Each at 10 µg/mL in 2-5% HNO3 Iron Nickel $ 105 / 500 mL 3 comps. Vanadium Nitric Acid Blank CLP-BLN-5 CLP-BLN-L $ 30 / 500 mL $ 45 / L (2 x 500 mL) 5% HNO3 in ASTM Type I Water Member AccuStandard is an active member in ASTM and strives to keep abreast of ASTM method revisions. If our listed formulation does not meet the most recent method revision, please contact Technical Support, ext. 117 for an updated product. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 39 Method ASTM Standards 5762 Member ASTM D-5762 Nitrogen in Petroleum & Petroleum Products by Boat-Inlet Chemiluminescence Originally designed for D-5762-98 Stock Nitrogen Standard ASTM D-5762-95-500X-PAK $ 45 / 5 x 1 mL Nitrogen @ 500 µg/mL in Xylene (Acridine @ 6397 µg/mL) Nitrogen Calibration Set Technical Note D-5762-95-CAL-SET $ 75 / 6 x 1 mL Cat. No. D-5762-95-BL D-5762-95-1X D-5762-95-5X D-5762-95-10X D-5762-95-50X D-5762-95-100X Description Xylene Blank Nitrogen @ 1.0 µg/mL in Xylene Nitrogen @ 5.0 µg/mL in Xylene Nitrogen @ 10 µg/mL in Xylene Nitrogen @ 50 µg/mL in Xylene Nitrogen @ 100 µg/mL in Xylene 1 1 1 1 1 1 x x x x x x Unit 1 mL 1 mL 1 mL 1 mL 1 mL 1 mL x x x x x x Unit 1 mL 1 mL 1 mL 1 mL 1 mL 1 mL Nitrogen introduced using Acridine. Low level Nitrogen Calibration Set Technical Note ASTM-P-0070-SET $ 75 / 6 x 1 mL Cat. No. ASTM-P-0070-BL ASTM-P-0070-1X ASTM-P-0070-2X ASTM-P-0070-4X ASTM-P-0070-10X ASTM-P-0070-20X Description Isooctane Blank Nitrogen @ 0.5 µg/g in Isooctane Nitrogen @ 1.0 µg/g in Isooctane Nitrogen @ 2.0 µg/g in Isooctane Nitrogen @ 5.0 µg/g in Isooctane Nitrogen @ 10.0 µg/g in Isooctane 1 1 1 1 1 1 Nitrogen introduced using Acridine. Low level Nitrogen & Sulfur Calibration Set ASTM-P-0071-SET Cat. No. ASTM-P-0071-BL ASTM-P-0071-01 ASTM-P-0071-02 ASTM-P-0071-03 $ 50 / 4 x 1 mL Description Benzene Blank Nitrogen @ 0.25 µg/g & Sulfur @ 0.25 µg/g in Benzene Nitrogen @ 0.50 µg/g & Sulfur @ 0.50 µg/g in Benzene Nitrogen @ 1.00 µg/g & Sulfur @ 1.00 µg/g in Benzene Technical Note 1 1 1 1 x x x x Unit 1 mL 1 mL 1 mL 1 mL The Nitrogen is introduced using Aniline and the Sulfur is introduced using n-Butyl sulfide. AccuPetroCheck and AccuPetroTest Real World Gasoline QC Standards In cooperation with ASTM D-02 subcommittee 3 and 4, AccuStandard ampulled 21 Real World gasoline reference fuels. Consensus Values have been determined for these reference fuels by various ASTM Round Robins to provide Petrochemical Laboratories with a source of well characterized gasoline standards for use in QA/QC applications and as Single Blind test samples over an extended period of time. As new ASTM D-02.03 and D-02.04 Test methods are promulgated they require mandatory Quality Control testing of real world samples. AccuStandard’s AccuPetroTest & AccuPetroCheck standards are being successfully used to achieve these new Quality Control requirements. QC Standards CARB Low Sulfur RFG QC Standard Conventional Gasoline QC Standard ASTM-FUEL-QCS-01-PAK $ 60 / 5 x 15 mL ASTM-FUEL-QCS-02-PAK $ 60 / 5 x 15 mL Parameter Total Aromatics Total Olefins Total Saturates Sulfur Sulfur Sulfur Sulfur Benzene Toluene Total Aromatics Benzene Total Olefins Value 24.5 5.3 58.3 0.0057 0.0078 55.76 59.31 0.80 4.92 23.42 0.78 5.3 Parameter Total Aromatics Total Olefins Total Saturates Sulfur Sulfur Sulfur Sulfur Benzene Toluene Total Aromatics Benzene Total Olefins 40 Method D-1319 D-1319 D-1319 D-2622 D-4294 D-5453 D-6344 D-5769 D-5769 D-5769 D-6227 D-6550 Conc. Vol.% Vol.% Vol.% Wt.% Wt.% µg/g µg/g Vol.% Vol.% Vol.% Vol.% Vol.% Method D-1319 D-1319 D-1319 D-2622 D-4294 D-5453 D-6344 D-5769 D-5769 D-5769 D-6227 D-6550 Value 34.6 12.4 62.8 0.0338 0.0368 317.36 338.78 0.55 5.53 32.51 0.52 12.4 Conc. Vol.% Vol.% Vol.% Wt.% Wt.% µg/g µg/g Vol.% Vol.% Vol.% Vol.% Vol.% AccuPetroCheck QC Standards Two of the fuels are available as AccuPetroCheck Consensus Value QC Standards. The AccuPetroCheck CARB and Conventional gasoline reference materials have all parameters listed on the certificate with the Consensus Values and the regression equations for reproducability. Use of these Reference Materials improve the quality of laboratory results. The Consensus Values listed reflect initial statistical treatment of the data at the time the catalog was published. The actual certificate provided with the AccuPetroCheck QC standard will have the accepted Consensus Value based on statistical treatment of the data. Quality System is Certified to comply with the International ISO 9001 Quality Standard Petrochemical Standards Member AccuPetroTest Sulfur in Diesel Fuel QC Standard $ 25 / 2 x 15 mL Parameter Sulfur Approx. Range 20 - 11000 mg/kg See ASTM Methods D-2622, D-3120, D-3246-92, D-4294, D-5453, for Sulfur Calibration Standards Sulfur in White Mineral Oil QC Standard SBPT-SWMO $ 25 / 2 x 15 mL Parameter Sulfur Approx. Range 20 - 11000 mg/kg See ASTM Methods D-2622, D-3120, D-3246-92, D-4294, D-5453 for Sulfur Calibration Standards AccuPetroTest Gasoline Low Sulfur QC Sample Olefin QC Sample SBPT-LSGAS SBPT-OLEFINSFC Parameter Sulfur $ 25 / 2 x 15 mL Method 5453 Approx. Range 0 - 50 µg/g Parameter Olefins $ 25 / 2 x 15 mL Method 6550 Approx. Range 1 - 40 Vol.% AccuPetroTest Gasoline QC Olefins QC Sample SBPT-OLEFIN Parameter Total Aromatics Total Olefins Total Saturates Sulfur QC Sample $ 25 / 2 x 15 mL Method D-1319 D-1319 D-1319 Approx. Range 8-60 Vol.% 1 - 40 Vol.% 30-80 Vol. % See ASTM Method D-1319 for Sulfur Calibration Standards Aromatics QC Sample SBPT-AROM Parameter Total Aromatics Parameter Sulfur Sulfur Sulfur Sulfur Approx. Range 8 - 60 Vol.% See ASTM Methods D-3606, D-5580-95, D-5769-95 for Benzene Calibration Standards SBPT-BENZ Parameter Benzene Toluene Approx. Range 0.1 - 2.0 Vol.% 1.0 - 15 Vol.% Technical Note $ 50 / 2 x 15 mL Method D-1319 D-1319 D-1319 D-2622 D-4294 D-5453 D-6344 D-5769 D-5769 D-5769 D-6277 D-6550 $ 25 / 2 x 15 mL Method D-5769 D-5769 See ASTM Methods D-3606, D-5580-95, D-5769-95 for Benzene Calibration Standards Comprehensive Single Blind Gasoline QC Sample Parameter Total Aromatics Total Olefins Total Saturates Sulfur Sulfur Sulfur Sulfur Benzene Toluene Total Aromatics Benzene Total Olefins Approx. Range 0.0001 - 0.0930 Wt.% 0.0016 - 0.0930 Wt.% 4.0 - 500 µg/g 1.0 - 1000 µg/g See ASTM Methods D-2622, D-3120, D-3246-92, D-4294, D-5453 for Sulfur Calibration Standards AccuPetroTest Gasoline SBPT-COMP $ 25 / 2 x 15 mL Method D-2622 D-4294 D-5453 D-XXXX Benzene/Toluene QC Sample $ 25 / 2 x 15 mL Method D-5769 SBPT-SGAS Approx. Range 8 - 60 1 - 40 30 - 80 0.0001 - 0.0930 0.0016 - 0.0930 0.5 -500 1.0 - 1000 0.1 - 2.0 1.0 - 15 8 - 60 0.1 - 2.0 1 - 40 AccuPetroTest Single Blind Standards Petrochemical Laboratories looking to test the performance of the laboratory for a specific parameter can order the Single Blind AccuPetroTest sample for the parameter of interest. Two real world gasoline samples will be sent for the test parameter requested and a separate sealed envelope containing the determined Consensus Value is also provided. The second sample is for repeatability testing or as a future QA/QC reference. Conc. Vol.% Vol.% Vol.% Wt.% Wt.% µg/g µg/g Vol.% Vol.% Vol.% Vol.% Vol.% Our new comprehensive single blind gasoline QC sample tests for more parameters from a single sample. The actual gasoline sample will have consensus values listed on the datasheet that fall within the range listed for each parameter. Test to Low ppb Sulfur See Pages 6-11 Conducting a Petrochemical Round Robin for a new ASTM method? Select AccuStandard to prepare the necessary samples for the Round Robin study. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 41 ASTM SBPT-SDF Sulfur Single Blind AccuPetroTest Alternative Matrices Standards AccuStandard has manufactured a number of Diesel and White Mineral Oil quality control products containing a gravimetrically prepared amount of Sulfur. Use of these alternative matrix materials can provide further evaluation of the QA/QC process in the laboratory. Two samples will be sent for the test parameter and a separate sealed envelope containing the gravimetrically prepared sulfur values is also provided. The second sample is for repeatability testing or for use as a future QA/QC reference. Method 5769 ASTM Standards Member ASTM Method D-5769-98 Benzene, Toluene, and Total Aromatics in Finished Gasoline by GC/MS ASTM ASTM D-5769 Benzene, Toluene & Total Aromatics in Finished Gasoline by GC/MS Originally designed for D-5769-98 All of your standards requirements for ASTM Method D-5769 have been put together in the following 10 pages. These standards and methods are used in the monitoring of Total Aromatics according to the latest methods and amendments to the US Clean Air Act. A set of Amendments, containing more stringent specifications became effective January 1, 1995 limiting the volatility and composition of reformulated gasoline. The D-02 Committee of the American Society of Testing Materials, developed a standard test method D-5769 for the determination of the analyte composition by GC/MS of reformulated gasoline. Aromatic Product Line yields the following important benefits Features: Benefits: Purity and Identity of all analytes verified .......... Impurity interferences in analyte retention time under identical operating conditions window are compensated. Certified method specific calibration standards . Increased confidence in analytical results. Eliminates preparation of calibration standards ..Time is utilized quantifying actual samples. Internal Standards Incorporated .........................Saves time. Weights and weight percents provided .............. Ease of use in performing back calculations. Includes all necessary solutions .........................Complete single source for reference materials. Variations in packaging size .............................. Meet laboratory sample volumes and demands. Low Cost ............................................................ More economical to purchase than to prepare standards. Flexibility ............................................................ Meet your lab requirements/method changes. Only 5 standards needed for a 5 Point Curve ... Generate a full calibration curve in 1/2 the time of the two set version composed of 10 standards. No charge disk deliverable calibration curve .... Direct computer uploading eliminates the input of 135 weights (CALAMTS™) separate data points. 42 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5769 Member ASTM D-5769 Benzene, Toluene & Total Aromatics in Finished Gasoline by GC/MS Originally designed for D-5769-95 ASTM Standards Designed for ASTM D-5769 as published in the 1997 Annual Book of ASTM Standards, Vol. 05.03 Petroleum Products and Lubricants (III): D-4636-latest; Catalysts The following M-GRA catalog numbers contain the necessary calibration curves, daily quality control, and internal standards designed to meet the promulgated GC/MS Aromatic method listed in the 1997 ASTM Book of Standards. AccuStandard offers two different versions of the M-GRA catalog numbers: M-GRA three component internal standard version, and the M-GRA four component internal standard version. The three component internal standard version contains the necessary deuterated analytes for full qualitative and quantitative analysis of the 25 components listed in the published version. The four component internal standard version was designed at the request of the petroleum refinery laboratories. This four internal standard version incorporates not only the Benzene-d6, Ethyl benzene-d10, Naphthalene-d8, but also Toluene-d8. Incorporating the Toluene-d8 as the internal standard for the quantification of gasolines with higher Toluene levels has improved analytical results for this analyte. Incorporation of a 6th Calibration Standard A 6th calibration standard has been formulated for the M-GRA product line to improve the linearity at the high end of the calibration curve see page 44. This sixth standard can be especially important in the quantification of gasoline samples containing high toluene levels. The formulation contains an analyte concentration between the high level standard and the next level, which is standard two. Use of the sixth standard provides an additional calibration point that is desirable when the calibration curve is developed using a quadratic fit. Aromatics Kits for analysis by GC/MS M-GRA-K1 (Original Formulations) Kit includes: M-GRA-CAL/IS-SET M-GRA-QC/IS-5ML M-GRA-IS-5ML M-GRA-ST $ 600 5 1 1 1 x x x x Units 1 mL 5 mL 5 mL 1 mL Function 5 Pt. Curve w/ 3 ISTD's Daily QC w/ 3 ISTD's Internal Std. 3 comps. Sensitivity Test Solution For your added convenience we have provided the following Aromatics Kits to meet the analytical requirements for this method. See page 44 for product description with analytes & conc. M-GRA-K2 $ 700 (Developed for improved high concentration linearity) Kit includes: M-GRA-CAL/IS-SET M-GRA-ADD/IS M-GRA-QC/IS-5ML M-GRA-IS-5ML M-GRA-ST 5 1 1 1 1 x x x x x Units 1 mL 1 mL 5 mL 5 mL 1 mL Function 5 Pt. Curve w/ 3 ISTD's 6th Std. for revison 5 F Daily QC w/ 3 ISTD's Internal Std. 3 comps. Sensitivity Test Solution See page 44 for product description with analytes & conc. M-GRA-K4 $ 850 (Used to meet the Toluene-d8 internal standard version recommended by a network of major petroleum refineries) Kit includes: Units M-GRA-CAL-R/IS-R-SET 5 x 1 mL M-GRA-ADD/IS-R 1 x 1 mL M-GRA-QC-R/IS-R-5ML 1 x 5 mL M-GRA-IS-R-10ML 1 x 10 mL M-GRA-ST 1 x 1 mL Function 5 Pt. Curve w/ 4 ISTD's 6th Standard for rev. 5 F Daily QC w/ 4 ISTD's Internal Std. 4 comps. Sensitivity Test Solution See page 45 for product description with analytes & conc. Cross Reference Table ASTM IP ISO DIN JIS AFNOR sorted by ASTM Method see beginning of Catalog Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 43 Method ASTM Standards 5769 Member ASTM ASTM D-5769 Calibration Curve with 3 Component Deuterated Internal Standard Added Aromatics Calibration Standards Kit (3 Internal Standard Version) M-GRA-CAL/IS-SET $ 375 / set of 5 x 1 mL Optional Sixth Standard with 3 Comp. Deuterated Internal Standard Added M-GRA-ADD/IS Core Calibr. Mix 24 Comps. Std. 1 Target Vol. % Benzene Toluene Ethylbenzene m-Xylene p-Xylene o-Xylene Isopropylbenzene n-Propylbenzene 1-Methyl-3-ethylbenzene 1-Methyl-4-ethylbenzene 1,3,5-Trimethylbenzene 1-Methyl-2-ethylbenzene 1,2,4-Trimethylbenzene 1,2,3-Trimethylbenzene Indan 1,4-Diethylbenzene n-Butylbenzene 1,2-Diethylbenzene 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Naphthalene Pentamethylbenzene 1-Methylnaphthalene 2-Methylnaphthalene Isooctane Internal Standard Benzene-d6 Ethylbenzene-d10 Naphthalene-d8 3 19 5 6 6 6 3 3 3 3 3 3 5 3 3 3 3 3 2 2 2 2 2 2 -- $ 100 / 1 x 1 mL Std. 2 Vol. % Std. 3 Vol. % Std. 4 Vol. % Std. 5 Vol. % Core Calibr. Mix 24 Comps. 1.50 9.50 2.50 3.00 3.00 3.00 1.50 1.50 1.50 1.50 1.50 1.50 2.50 1.50 1.50 1.50 1.50 1.50 1.00 1.00 1.00 1.00 1.00 1.00 Bal 0.75 4.75 1.25 1.50 1.50 1.50 0.75 0.75 0.75 0.75 0.75 0.75 1.25 0.75 0.75 0.75 0.75 0.75 0.50 0.50 0.50 0.50 0.50 0.50 Bal 0.375 2.375 0.625 0.750 0.750 0.750 0.375 0.375 0.375 0.375 0.375 0.375 0.625 0.375 0.375 0.375 0.375 0.375 0.250 0.250 0.250 0.250 0.250 0.250 Bal 0.1875 1.1875 0.3125 0.3750 0.3750 0.3750 0.1875 0.1875 0.1875 0.1875 0.1875 0.1875 0.3125 0.1875 0.1875 0.1875 0.1875 0.1875 0.1250 0.1250 0.1250 0.1250 0.1250 0.1250 Bal Benzene Toluene Ethylbenzene m-Xylene p-Xylene o-Xylene Isopropylbenzene n-Proplylbenzene 3-Ethyltoluene 4-Ethyltoluene 1,3,5-Trimethylbenzene 2-Ethyltoluene 1,2,4-Trimethylbenzene 1,2,3-Trimethylbenzene Indan 1,4-Diethylbenzene n-Butylbenzene 1,2-Diethylbenzene 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Naphthalene Pentamethylbenzene 1-Methylnaphthalene 2-Methylnaphthalene Isooctane (M-GRA-IS) 2 2 2 2 1 1 2 2 1 2 2 1 2 2 1 Optional Std. 6 Target Vol. % Internal Standard Benzene-d6 Ethylbenzene-d10 Naphthalene-d8 2.25 15 3.75 4.50 4.50 4.50 2.25 2.25 2.25 2.25 2.25 2.25 3.75 2.25 2.25 2.25 2.25 2.25 4.0 1.5 1.5 1.5 1.5 1.5 Bal (M-GRA-IS) 2 2 1 Daily Quality Control Standard (without Internal Standard) Daily Quality Control Standard (with Internal Standard) M-GRA-QC-10ML $ 125 / 1 x 10 mL M-GRA-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL M-GRA-QC/IS-5ML $ 100 / 1 x 5 mL M-GRA-QC/IS-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL Compound n-Hexane n-Heptane n-Octane n-Decane n-Dodecane Isooctane Benzene Wt. Ratio 12 17 17 12 5 12 1 Wt. Compound Ratio Toluene 9 Ethylbenzene 3 m-Xylene 3 o-Xylene 3 1,2,4-Trimethylbenzene 3 1,2,4,5-Tetramethylbenzene 3 13 Comp. Core Mix Compound n-Hexane n-Heptane n-Octane n-Decane n-Dodecane Isooctane Benzene Wt. Ratio 12 17 17 12 5 12 1 Use with any M-GRA Calibration Curve. 3 Comp. Deuterated Internal Std. Mix M-GRA-IS-5ML M-GRA-IS-5ML-PAK 44 CALAMTS™ (Disk containing “Calibration Amounts”) Each analyte in each standard is individually weighed. Actual weights and weight percents are provided. Includes M-GRA-IS (3 Comp. Internal Standards mix) combined with the above 13 Comp. Core QC Mix: M-GRA-QC in a 5 to 100 weight ratio. 16 comps. M-GRA-ST M-GRA-ST-PAK 100 µg/mL in Isooctane 1,4-Diethyl benzene Eliminates hand keyed-in data. 100 ASTM/EPA Sensitivity Test Solution $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL Disk Deliverable (At no additional charge) Wt. Compound Ratio Toluene 9 Ethylbenzene 3 m-Xylene 3 o-Xylene 3 1,2,4-Trimethylbenzene 3 1,2,4,5-Tetramethylbenzene 3 13 Comp. Core Mix 100 Technical Note Originally designed for D-5769-95 Compound Mix Ratio Benzene-d6 2 mL Ethylbenzene-d10 2 mL $ 150 / 1 x 5 mL SAVE 20% $ 600 / 5 x 5 mL 3 comps. Compound Mix Ratio Naphthalene-d8 1 gm Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5769 Member ASTM D-5769 Calibration Curve with 4 Component Deuterated Internal Standard Added M-GRA-CAL-R/IS-R-SET $ 425 / set of 5 x 1 mL Optional Sixth Standard with 4 Comp. Deuterated Internal Standard Added M-GRA-ADD/IS-R Core Calibr. Mix 24 Comps. Std. 1 Target Wt. % Benzene 3.13 Toluene 19.65 Ethylbenzene 5.12 m-Xylene 6.27 p-Xylene 6.33 o-Xylene 6.51 Isopropylbenzene 3.06 n-Propylbenzene 3.04 3-Ethyltoluene 3.08 4-Ethyltoluene 3.05 1,3,5-Trimethylbenzene 3.07 2-Ethyltoluene 3.14 1,2,4-Trimethylbenzene 5.18 1,2,3-Trimethylbenzene 3.19 Indan 3.46 1,4-Diethylbenzene 3.04 n-Butylbenzene 3.05 1,2-Diethylbenzene 3.22 1,2,4,5-Tetramethylbenzene 2.10 1,2,3,5-Tetramethylbenzene 2.09 Naphthalene 2.35 Pentamethylbenzene 2.16 1-Methylnaphthalene 2.32 2-Methylnaphthalene 2.41 Isooctane ----- (M-GRA-IS-R) Mix Ratio (2 mL) Benzene-d6 Ethylbenzene-d10 (2 mL) Naphthalene-d8 (1 gm) Toluene-d8 (7 mL) $ 100 / 1 x 1 mL Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % Core Calibr. Mix 24 Comps. 1.78 11.11 2.92 3.50 3.50 3.56 1.74 1.74 1.75 1.74 1.75 1.78 2.95 1.81 1.95 1.74 1.74 1.78 1.20 1.20 1.34 1.23 1.34 1.37 43.47 0.95 5.90 1.55 1.86 1.86 1.89 0.93 0.93 0.93 0.93 0.93 0.95 1.57 0.96 1.04 0.93 0.92 0.95 0.64 0.64 0.71 0.66 0.71 0.73 69.96 0.490 3.058 0.805 0.962 0.962 0.980 0.480 0.480 0.481 0.479 0.481 0.490 0.812 0.498 0.536 0.480 0.479 0.490 0.329 0.330 0.369 0.340 0.369 0.378 84.441 0.2490 1.5547 0.4090 0.4891 0.4891 0.4981 0.2439 0.2440 0.2446 0.2437 0.2448 0.2492 0.4130 0.2530 0.2726 0.2439 0.2434 0.2489 0.1674 0.1679 0.1877 0.1727 0.1877 0.1922 92.0905 Benzene Toluene Ethylbenzene m-Xylene p-Xylene o-Xylene Isopropylbenzene n-Propylbenzene 3-Ethyltoluene 4-Ethyltoluene 1,3,5-Trimethylbenzene 2-Ethyltoluene 1,2,4-Trimethylbenzene 1,2,3-Trimethylbenzene Indan 1,4-Diethylbenzene n-Butylbenzene 1,2-Diethylbenzene 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Naphthalene Pentamethylbenzene 1-Methylnaphthalene 2-Methylnaphthalene Isooctane Internal Standard ASTM Aromatics Calibration Standards Kit (4 Internal Standard Version) Originally designed for D-5769-95 Optional Std. 6 Target Wt. % 2.48 16.29 4.07 4.87 4.87 4.96 2.43 2.43 2.44 2.43 2.44 2.48 4.11 2.52 2.71 2.43 2.42 2.48 4.44 1.67 1.87 1.72 1.87 1.91 17.67 Technical Note This set of calibration solutions was formulated to improve quantification for Toluene by using Toluene-d8 as an additional Internal Standard. Internal Standard 16.57 16.76 8.78 57.88 16.57 16.76 8.78 57.88 16.57 16.76 8.78 57.88 16.57 16.76 8.78 57.88 16.57 16.76 8.78 57.88 (M-GRA-IS-R) Benzene-d6 Ethylbenzene-d10 Naphthalene-d8 Toluene-d8 Mix Ratio (2 mL) 16.57 (2 mL) 16.76 (1 mL) 8.78 (7 mL) 57.88 The 4 component internal standard mix (M-GRA-IS-R) is combined with the 25 component core calibration curve mixtures in a 12 to 100 weight ratio to formulate a complete calibration solution containing 29 comps. Daily Quality Control Standard (without Internal Standard) Daily Quality Control Standard (with Internal Standard M-GRA-IS-R) M-GRA-QC-10ML $ 125 / 1 x 10 mL M-GRA-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL M-GRA-QC/IS-R-5ML $ 125 / 1 x 5 mL M-GRA-QC/IS-R-5ML-PAKSAVE 20% $ 500 / 5 x 5mL Compound n-Hexane n-Heptane n-Octane n-Decane n-Dodecane Isooctane Benzene Wt. Ratio 12 17 17 12 5 12 1 Wt. Compound Ratio Toluene 9 Ethylbenzene 3 m-Xylene 3 o-Xylene 3 1,2,4-Trimethylbenzene 3 1,2,4,5-Tetramethylbenzene 3 Compound n-Hexane n-Heptane n-Octane n-Decane n-Dodecane Isooctane Benzene Wt. Ratio 12 17 17 12 5 12 1 Wt. Compound Ratio Toluene 9 Ethylbenzene 3 m-Xylene 3 o-Xylene 3 1,2,4-Trimethylbenzene 3 1,2,4,5-Tetramethylbenzene 3 4 Comp. Deuterated Internal Std. Mix 13 Comp. Core Mix 100 Includes M-GRA-IS-R (4 Comp. Internal Standards Mix) combined with the above 13 Comp. Core QC Mix: M-GRA-QC in a 12 to 100 weight ratio. 17 comps. M-GRA-IS-R-10ML $ 225 / 1 x 10 mL M-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL 4 comps. ASTM/EPA Sensitivity Test Solution 13 Comp. Core Mix Compound Mix Ratio 2 mL Benzene-d6 Ethylbenzene-d10 2 mL 100 Compound Mix Ratio Naphthalene-d8 1 gm Toluene-d8 7 mL Technical Note M-GRA-ST M-GRA-ST-PAK 100 µg/mL in Isooctane Standards of Interest For the mandatory real world QC samples stipulated in the Method, see pages 1-2 $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL 1,4-Diethyl benzene Use with any M-GRA Calibration Curve. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 45 Method ASTM Standards 5769 Member Originally designed for D-5769-98 ASTM ASTM D-5769 Version with No Internal Standard The following D-5769 and M-GRA Standards were formulated to address proposed and promulgated changes to ASTM Method D-5769-98 Aromatics by GC/MS. Many of these changes were evaluated and/ or adopted due to the results generated from the 1997 Round Robin, which used a select group of 21 gasolines ampulized by AccuStandard. AccuStandard is committed to staying abreast of ASTM committee D-02 method developments. We ask that you contact us when your analytical group finds a beneficial procedure or modification. Modifications A Sixth Standard was added to meet the latest D-5769 method requirements and provide improved linearity at the high end of the Calibration curve The Calibration Curve was packaged in two convenient sizes without the internal standard. This packaging scheme allows for the addition of any ISTD formulation or oxygenate components. The Quality Control Standard was reformulated in the latest D-5769 revision. The formulation changes include reducing the 1,2,4,5-Tetramethylbenzene weight ratio and adding Naphthalene. The Benzene Target Weight % has been increased to meet the latest D-5769 method requirements. Pentamethylbenzene has now been removed from the analyte list. Calibration Curve with No Internal Std. Added Optional Sixth Standard D-5769-CAL-SET-5ML D-5769-CAL-SET-10ML D-5769-ADD-5ML D-5769-ADD-10ML $ 1500 / Set of 5 x 5 mL $ 2750 / Set of 5 x 10 mL $ 150 / 1 x 5 mL $ 300 / 1 x 10 mL Std. 1 Target Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % Core Calibration Mix 23 Comps. Benzene 5.25 Toluene 19.67 Ethylbenzene 5.18 m-Xylene 6.19 p-Xylene 6.19 o-Xylene 6.30 Isopropylbenzene 3.09 n-Propylbenzene 3.09 3-Ethyltoluene 3.10 4-Ethyltoluene 3.08 1,3,5-Trimethylbenzene 3.10 2-Ethyltoluene 3.15 1,2,4-Trimethylbenzene 5.23 1,2,3-Trimethylbenzene 3.20 Indan 3.45 1,4-Diethylbenzene 3.09 n-Butylbenzene 3.08 1,2-Diethylbenzene 3.15 1,2,4,5-Tetramethylbenzene 2.12 1,2,3,5-Tetramethylbenzene 2.12 Naphthalene 2.37 1-Methylnaphthalene 2.37 2-Methylnaphthalene 2.43 Isooctane ----- 2.95 11.06 2.91 3.48 3.48 3.54 1.74 1.74 1.74 1.73 1.74 1.77 2.94 1.80 1.94 1.74 1.73 1.77 1.19 1.19 1.34 1.34 1.37 43.77 1.575 5.898 1.552 1.856 1.856 1.890 0.925 0.926 0.928 0.925 0.929 0.945 1.567 0.960 1.034 0.925 0.923 0.945 0.635 0.637 0.712 0.712 0.730 70.015 0.8144 3.0505 0.8026 0.9598 0.9598 0.9776 0.4786 0.4787 0.4801 0.4782 0.4804 0.4890 0.8104 0.4965 0.5350 0.4786 0.4776 0.4885 0.3284 0.3295 0.3683 0.3683 0.3773 84.4922 0.4143 1.5519 0.4083 0.4883 0.4883 0.4973 0.2435 0.2435 0.2442 0.2433 0.2444 0.2488 0.4123 0.2526 0.2722 0.2435 0.2430 0.2485 0.1671 0.1676 0.1874 0.1874 0.1919 92.1105 Benzene 4.16 Toluene 16.41 Ethylbenzene 4.10 m-Xylene 4.91 p-Xylene 4.91 o-Xylene 5.00 Isopropylbenzene 2.45 n-Propylbenzene 2.45 3-Ethyltoluene 2.45 4-Ethyltoluene 2.44 1,3,5-Trimethylbenzene 2.46 2-Ethyltoluene 2.50 1,2,4-Trimethylbenzene 4.14 1,2,3-Trimethylbenzene 2.54 Indan 2.73 1,4-Diethylbenzene 2.45 n-Butylbenzene 2.44 1,2-Diethylbenzene 2.50 1,2,4,5-Tetramethylbenzene 1.68 1,2,3,5-Tetramethylbenzene 1.68 Naphthalene 1.88 1-Methylnaphthalene 1.88 2-Methylnaphthalene 1.93 Isooctane 19.92 Core Calibr. Mix 23 Comps. 4 Comp. Deuterated Internal Std. Mix M-GRA-IS-R-10ML $ 225 / 1 x 10 mL M-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL 4 comps. Mix Compound Ratio 2 mL Benzene-d6 Ethylbenzene-d10 2 mL Mix Compound Ratio Naphthalene-d8 1 gm Toluene-d8 7 mL 3 Comp. Deuterated Internal Std. Mix M-GRA-IS-5ML M-GRA-IS-5ML-PAK Compound Benzene-d6 Ethylbenzene-d10 Naphthalene-d8 46 $ 150 / 1 x 5 mL SAVE 20% $ 600 / 5 x 5 mL 3 comps. Mix Ratio 2 mL 2 mL 1 gm Target Wt. % Disk Deliverable (At no additional charge) Eliminates hand keyed-in data. ® CALAMTS (Disk containing “Calibration Amounts”) Each analyte in each standard is individually weighed. Actual weights and weight percents are provided. Daily Quality Control Standard (without Internal Standard) D-5769-QC-10ML $ 125 / 1 x 10 mL D-5769-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL Compound n-Hexane n-Heptane n-Octane n-Decane n-Dodecane Isooctane Benzene Wt. Ratio 12 17 17 12 5 12 1 Wt. Compound Ratio Toluene 9 Ethylbenzene 3 m-Xylene 3 o-Xylene 3 1,2,4-Trimethylbenzene 3 1,2,4,5-Tetramethylbenzene 2 Naphthalene 1 14 Comp. Core Mix 100 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5769 Member Originally designed for D-5769-98 ASTM D-5769 Version with 3 Internal Standards Optional Sixth Standard with a 3 Comp. Deuterated Internal Standard added D-5769-CAL/IS-SET D-5769-ADD/IS $ 375 / 5 x 1 mL $ 100 / 1 x 1 mL Std. 1 Target Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % Core Calibration Mix 24 Comps. Benzene 5.25 Toluene 19.67 Ethylbenzene 5.18 m-Xylene 6.19 p-Xylene 6.19 o-Xylene 6.30 Isopropylbenzene 3.09 n-Propylbenzene 3.09 3-Ethyltoluene 3.10 4-Ethyltoluene 3.08 1,3,5-Trimethylbenzene 3.10 2-Ethyltoluene 3.15 1,2,4-Trimethylbenzene 5.23 1,2,3-Trimethylbenzene 3.20 Indan 3.45 1,4-Diethylbenzene 3.09 n-Butylbenzene 3.08 1,2-Diethylbenzene 3.15 1,2,4,5-Tetramethylbenzene 2.12 1,2,3,5-Tetramethylbenzene 2.12 Naphthalene 2.37 1-Methylnaphthalene 2.37 2-Methylnaphthalene 2.43 Isooctane ----- 2.95 11.06 2.91 3.48 3.48 3.54 1.74 1.74 1.74 1.73 1.74 1.77 2.94 1.80 1.94 1.74 1.73 1.77 1.19 1.19 1.34 1.34 1.37 43.77 1.575 5.898 1.552 1.856 1.856 1.890 0.925 0.926 0.928 0.925 0.929 0.945 1.567 0.960 1.034 0.925 0.923 0.945 0.635 0.637 0.712 0.712 0.730 70.015 0.8144 3.0505 0.8026 0.9598 0.9598 0.9776 0.4786 0.4787 0.4801 0.4782 0.4804 0.4890 0.8104 0.4965 0.5350 0.4786 0.4776 0.4885 0.3284 0.3295 0.3683 0.3683 0.3773 84.4922 0.4143 1.5519 0.4083 0.4883 0.4883 0.4973 0.2435 0.2435 0.2442 0.2433 0.2444 0.2488 0.4123 0.2526 0.2722 0.2435 0.2430 0.2485 0.1671 0.1676 0.1874 0.1874 0.1919 92.1105 Benzene Toluene Ethylbenzene m-Xylene p-Xylene o-Xylene Isopropylbenzene n-Propylbenzene 3-Ethyltoluene 4-Ethyltoluene 1,3,5-Trimethylbenzene 2-Ethyltoluene 1,2,4-Trimethylbenzene 1,2,3-Trimethylbenzene Indan 1,4-Diethylbenzene n-Butylbenzene 1,2-Diethylbenzene 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Naphthalene 1-Methylnaphthalene 2-Methylnaphthalene Isooctane Core Calibr. Mix 24 Comps. Internal Standard Compound Benzene-d6 Ethylbenzene-d10 Naphthalene-d8 M-GRA-IS Mix ratio 2 mL 2 mL 1 gm Wt. % 3.0 3.0 94 Sulfur See Pages 6-11 M-GRA-IS-5ML M-GRA-IS-5ML-PAK Compound Benzene-d6 Ethylbenzene-d10 Naphthalene-d8 $ 150 / 1 x 5 mL SAVE 20% $ 600 / 5 x 5 mL 3 comps. Mix Ratio 2 mL 2 mL 1 gm Sensitivity Test Solution M-GRA-ST M-GRA-ST-PAK 100 µg/mL in Isooctane $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL 1,4-Diethyl benzene 100 Resolution Standard 1,3,5-Trimethylbenzene 1-Methyl-2-ethylbenzene Isooctane Low ppb 3 Comp. Deuterated Internal Std. Mix D-5769-QC/IS-5ML $ 100 / 1 x 5 mL D-5769-QC/IS-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL 17 comps. Wt. Wt. Ratio Compound Ratio Compound 9 n-Hexane 12 Toluene 3 n-Heptane 17 Ethylbenzene 3 n-Octane 17 m-Xylene 3 n-Decane 12 o-Xylene 3 n-Dodecane 5 1,2,4-Trimethylbenzene Isooctane 12 1,2,4,5-Tetramethylbenzene 2 1 Benzene 1 Naphthalene M-GRA-RES M-GRA-RES-PAK 4.16 16.41 4.10 4.91 4.91 5.00 2.45 2.45 2.45 2.44 2.46 2.50 4.14 2.54 2.73 2.45 2.44 2.50 1.68 1.68 1.88 1.88 1.93 19.92 Test to The 3 Comp. Internal Standard Mix (M-GRA-IS) is combined with the 24 Comp. Core Calibration Curve Mixes above in a 5 to 100 weight ratio to formulate these 27 Comp. calibration solutions. Daily Quality Control Standard (with Internal Standard) Includes M-GRA-IS (3 component mix) added in 5 to 100 weight ratio Target Wt. % ASTM Calibration Curve with a 3 Comp. Deuterated Internal Standard added Fragmentation Pattern Standard $ 30 / 1 x 1 mL $ 120 / 5 x 1 mL 3 comps. M-GRA-FP M-GRA-FP-PAK 3.0% w/w in Isooctane $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 1,2,3-Trimethylbenzene Mass Scan Range Standard M-GRA-MSR M-GRA-MSR-PAK 3.0% w/w in Isooctane $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL Toluene Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 47 Method ASTM Standards 5769 Member Originally designed for D-5769-98 ASTM D-5769 4 Internal Standard Version (includes Toluene-d8) ASTM Calibration Curve with a 4 Comp. Deuterated Internal Standard added D-5769-CAL/IS-R-SET $ 425 / 5 x 1 mL Optional Sixth Standard with a 4 Comp. Deuterated Internal Standard added D-5769-ADD/IS-R Core Calibr. Mix 24 Comps. $ 100 / 1 x 1 mL Std. 1 Target Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % Core Calibration Mix 24 Comp. Benzene 5.25 Toluene 19.67 Ethylbenzene 5.18 m-Xylene 6.19 p-Xylene 6.19 o-Xylene 6.30 Isopropylbenzene 3.09 n-Propylbenzene 3.09 3-Ethyltoluene 3.10 4-Ethyltoluene 3.08 1,3,5-Trimethylbenzene 3.10 2-Ethyltoluene 3.15 1,2,4-Trimethylbenzene 5.23 1,2,3-Trimethylbenzene 3.20 Indan 3.45 1,4-Diethylbenzene 3.09 n-Butylbenzene 3.08 1,2-Diethylbenzene 3.15 1,2,4,5-Tetramethylbenzene 2.12 1,2,3,5-Tetramethylbenzene 2.12 Naphthalene 2.37 1-Methylnaphthalene 2.37 2-Methylnaphthalene 2.43 Isooctane ----- 2.95 11.06 2.91 3.48 3.48 3.54 1.74 1.74 1.74 1.73 1.74 1.77 2.94 1.80 1.94 1.74 1.73 1.77 1.19 1.19 1.34 1.34 1.37 43.77 1.575 5.898 1.552 1.856 1.856 1.890 0.925 0.926 0.928 0.925 0.929 0.945 1.567 0.960 1.034 0.925 0.923 0.945 0.635 0.637 0.712 0.712 0.730 70.015 0.8144 3.0505 0.8026 0.9598 0.9598 0.9776 0.4786 0.4787 0.4801 0.4782 0.4804 0.4890 0.8104 0.4965 0.5350 0.4786 0.4776 0.4885 0.3284 0.3295 0.3683 0.3683 0.3773 84.4922 0.4143 1.5519 0.4083 0.4883 0.4883 0.4973 0.2435 0.2435 0.2442 0.2433 0.2444 0.2488 0.4123 0.2526 0.2722 0.2435 0.2430 0.2485 0.1671 0.1676 0.1874 0.1874 0.1919 92.1105 Benzene Toluene Ethylbenzene m-Xylene p-Xylene o-Xylene Isopropylbenzene n-Propylbenzene 3-Ethyltoluene 4-Ethyltoluene 1,3,5-Trimethylbenzene 2-Ethyltoluene 1,2,4-Trimethylbenzene 1,2,3-Trimethylbenzene Indan 1,4-Diethylbenzene n-Butylbenzene 1,2-Diethylbenzene 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Naphthalene 1-Methylnaphthalene 2-Methylnaphthalene Isooctane Internal Standard M-GRA-IS-R Compound Mix ratio 2 mL Benzene-d6 Ethylbenzene-d10 2 mL Naphthalene-d8 1 gm Toluene-d8 7 mL Daily Quality Control Standard (with Internal Standard) Compound n-Hexane n-Heptane n-Octane n-Decane n-Dodecane Isooctane Benzene Wt. Compound Ratio Toluene 9 Ethylbenzene 3 m-Xylene 3 o-Xylene 3 1,2,4-Trimethylbenzene 3 1,2,4,5-Tetramethylbenzene 2 Naphthalene 1 Includes M-GRA-IS-R (4 component mix) added in 12 to 100 weight ratio The 4 Comp. Internal Standard Mix (M-GRA-IS-R) is combined with the 24 component core calibration curve mixtures above in a 12 to 100 weight ratio to formulate these 28 component calibration solutions. M-GRA-ST M-GRA-ST-PAK 100 µg/mL in Isooctane $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL 1,4-Diethyl benzene Resolution Standard M-GRA-RES M-GRA-RES-PAK $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 3 comps. Compound Wt. % 1,3,5-Trimethylbenzene 3.0 1-Methyl-2-ethylbenzene 3.0 Isooctane 94 100 4 Comp. Deuterated Internal Std. Mix Fragmentation Pattern Standard M-GRA-IS-R-10ML $ 225 / 1 x 10 mL M-GRA-IS-R-10ML-PAK SAVE 20% $ 900/ 5 x 10 mL M-GRA-FP M-GRA-FP-PAK 3.0 w/w in Isooctane Compound Mix Ratio Benzene-d6 2 mL Ethylbenzene-d10 2 mL 48 4.16 16.41 4.10 4.91 4.91 5.00 2.45 2.45 2.45 2.44 2.46 2.50 4.14 2.54 2.73 2.45 2.44 2.50 1.68 1.68 1.88 1.88 1.93 19.92 Sensitivity Test Solution D-5769-QC/IS-R-5ML $ 100 / 1 x 5 mL D-5769-QC/IS-R-5ML-PAK SAVE 20% $ 400/5 x 5 mL 18 comps. Wt. Ratio 12 17 17 12 5 12 1 Target Wt. % Compound Mix Ratio 1 gm Naphthalene-d8 Toluene-d8 7 mL $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 1,2,3-Trimethylbenzene Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5769 Member Originally designed for D-5769-98 ASTM D-5769 New Proposed / Promulgated Method Modifications D-5769-CAL/IS-R2-SET $ 375 / 5 x 1 mL Optional Sixth Standard with a 3 Comp. Chlorinated Internal Standard added D-5769-ADD/IS-R2 $ 100 / 1 x 1 mL Std. 1 Target Wt. % Std. 2 Wt. % Std. 3 Wt. % Std. 4 Wt. % Std. 5 Wt. % Core Calibration Mix 24 Component Benzene 5.25 Toluene 19.67 Ethylbenzene 5.18 m-Xylene 6.19 p-Xylene 6.19 o-Xylene 6.30 Isopropylbenzene 3.09 n-Propylbenzene 3.09 3-Ethyltoluene 3.10 4-Ethyltoluene 3.08 1,3,5-Trimethylbenzene 3.10 2-Ethyltoluene 3.15 1,2,4-Trimethylbenzene 5.23 1,2,3-Trimethylbenzene 3.20 Indan 3.45 1,4-Diethylbenzene 3.09 n-Butylbenzene 3.08 1,2-Diethylbenzene 3.15 1,2,4,5-Tetramethylbenzene 2.12 1,2,3,5-Tetramethylbenzene 2.12 Naphthalene 2.37 1-Methylnaphthalene 2.37 2-Methylnaphthalene 2.43 Isooctane ----- 2.95 11.06 2.91 3.48 3.48 3.54 1.74 1.74 1.74 1.73 1.74 1.77 2.94 1.80 1.94 1.74 1.73 1.77 1.19 1.19 1.34 1.34 1.37 43.77 1.575 5.898 1.552 1.856 1.856 1.890 0.925 0.926 0.928 0.925 0.929 0.945 1.567 0.960 1.034 0.925 0.923 0.945 0.635 0.637 0.712 0.712 0.730 70.015 0.8144 3.0505 0.8026 0.9598 0.9598 0.9776 0.4786 0.4787 0.4801 0.4782 0.4804 0.4890 0.8104 0.4965 0.5350 0.4786 0.4776 0.4885 0.3284 0.3295 0.3683 0.3683 0.3773 84.4922 0.4143 1.5519 0.4083 0.4883 0.4883 0.4973 0.2435 0.2435 0.2442 0.2433 0.2444 0.2488 0.4123 0.2526 0.2722 0.2435 0.2430 0.2485 0.1671 0.1676 0.1874 0.1874 0.1919 92.1105 Benzene Toluene Ethylbenzene m-Xylene p-Xylene o-Xylene Isopropylbenzene n-Propylbenzene 3-Ethyltoluene 4-Ethyltoluene 1,3,5-Trimethylbenzene 2-Ethyltoluene 1,2,4-Trimethylbenzene 1,2,3-Trimethylbenzene Indan 1,4-Diethylbenzene n-Butylbenzene 1,2-Diethylbenzene 1,2,4,5-Tetramethylbenzene 1,2,3,5-Tetramethylbenzene Naphthalene 1-Methylnaphthalene 2-Methylnaphthalene Isooctane Core Calibr. Mix 24 Comps. Internal Standard M-GRA-IS-R2 Compound Mix ratio Chlorobenzene 2 mL 1,2-Dichlorobenzene 2 mL 1,2,4-Trichlorobenzene 1 mL Daily Quality Control Standard (with Internal Standard) Includes M-GRA-IS-R2 (3 component mix) added in 5 to 100 weight ratio 4.16 16.41 4.10 4.91 4.91 5.00 2.45 2.45 2.45 2.44 2.46 2.50 4.14 2.54 2.73 2.45 2.44 2.50 1.68 1.68 1.88 1.88 1.93 19.92 The 3 Comp. Internal Standard Mix (M-GRA-IS-R2) is combined with the 24 Comp. Core Calibration Curve mixtures above in a 5 to 100 weight ratio to formulate these 27 Comp. calibration solutions. M-GRA-ST M-GRA-ST-PAK 100 µg/mL in Isooctane Eliminates hand keyed-in data. ® CALAMTS (Disk containing “Calibration Amounts”) Each analyte in each standard is individually weighed. Actual weights and weight percents are provided. $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL Standards of Interest 1,4-Diethyl benzene Fragmentation Pattern Standard M-GRA-FP M-GRA-FP-PAK 3.0 w/w in Isooctane Disk Deliverable (At no additional charge) For the mandatory real world QC samples stipulated in the Method, see pages 1-2. $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 1,2,3-Trimethylbenzene 100 3 Comp. Chlorinated Internal Std. Mix M-GRA-IS-R2-SET M-GRA-IS-R2-25ML Target Wt.% Sensitivity Test Solution D-5769-QC/IS-R2-5ML $ 100 / 1 x 5 mL D-5769-QC/IS-R2-5ML-PAKSAVE 20% $400/5 x 5 mL 17 comps. Wt. Wt. Compound Ratio Compound Ratio n-Hexane 12 Toluene 9 n-Heptane 17 Ethylbenzene 3 n-Octane 17 m-Xylene 3 n-Decane 12 o-Xylene 3 n-Dodecane 5 1,2,4-Trimethylbenzene 3 Isooctane 12 1,2,4,5-Tetramethylbenzene 2 Benzene 1 Naphthalene 1 ASTM Calibration Curve with a 3 Comp. Chlorinated Internal Standard added $125 / set of 25 x 1 mL $ 100 / 1 x 25 mL 3 comps. Compound Mix Ratio Chlorobenzene 2 mL 1,2-Dichlorobenzene 2 mL 1,2,4-Trichlorobenzene 1 mL Resolution Standard M-GRA-RES M-GRA-RES-PAK $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 3 comps. Compound Wt. % 1,3,5-Trimethylbenzene 3.0 1-Methyl-2-ethylbenzene 3.0 Isooctane 94 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 49 Method ASTM Standards 5769 Member Originally designed for D-5769-98 ASTM ASTM D-5769 Special QA/QC Formulations Daily Quality Control Standard (without Internal Standard) Technical Note M-GRA-QC-R-10ML $ 125 / 1 x 10 mL M-GRA-QC-R-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL Compound n-Hexane n-Heptane n-Octane n-Decane n-Dodecane Isooctane Benzene Toluene Wt. Ratio 12 17 17 12 5 12 1 9 Wt. Compound Ratio Ethylbenzene 3 m-Xylene 3 o-Xylene 3 1,2,4-Trimethylbenzene 3 1,2,4,5-Tetramethylbenzene 1 Pentamethylbenzene 1 1-Methylnaphthalene 1 15 Comp. Core Mix Specially formulated Daily Quality Control Standards originally designed in response to client requests for QC mixes that bracket the curve and contain more C9+ analytes to verify the instrument and QC solution integrity. Save 20-40% Buy AccuPAKs 100 For use with any M-GRA Calibration Curve Daily Quality Control Standard (with Internal Standard M-GRA-IS) Daily Quality Control Standard (with Internal Std. M-GRA-IS-R) M-GRA-QC-R/IS-5ML $ 100 / 1 x 5 mL M-GRA-QC-R/IS-5ML-PAK SAVE 20% $ 400 / 5 x 5 mL 18 comps. Wt. Wt. Compound Ratio Compound Ratio n-Hexane 12 Ethylbenzene 3 n-Heptane 17 m-Xylene 3 n-Octane 17 o-Xylene 3 n-Decane 12 1,2,4-Trimethylbenzene 3 n-Dodecane 5 1,2,4,5-Tetramethylbenzene 1 Isooctane 12 Pentamethylbenzene 1 Benzene 1 1-Methylnaphthalene 1 Toluene 9 M-GRA-QC-R/IS-R-5ML $ 125 / 1 x 5 mL M-GRA-QC-R/IS-R-5ML-PAK SAVE $ 500 / 5 x 5 mL 19 comps. Wt. Wt. Ratio Compound Ratio Compound 3 n-Hexane 12 Ethylbenzene 3 n-Heptane 17 m-Xylene 3 n-Octane 17 o-Xylene 3 n-Decane 12 1,2,4-Trimethylbenzene n-Dodecane 5 1,2,4,5-Tetramethylbenzene 1 1 Isooctane 12 Pentamethylbenzene 1 Benzene 1 1-Methylnaphthalene Toluene 9 100 Includes M-GRA-IS-R (4 Comp. Internal Standards mix) combined with the above 15 Comp. Core QC Mix: M-GRA-QC-R in a 12 to 100 Wt. ratio Includes M-GRA-IS (3 Comp. Internal Standards Mix) combined with the above 15 Comp. Core QC Mix: M-GRA-QC-R in a 5 to 100 weight ratio 100 3 Comp. Deuterated Internal Std. Mix 4 Comp. Deuterated Internal Std. Mix M-GRA-IS-5ML M-GRA-IS-5ML-PAK M-GRA-IS-R-10ML $ 225 / 1 x 10 mL M-GRA-IS-R-10ML-PAK SAVE 20% $ 900 / 5 x 10 mL 4 comps. Compound Mix Ratio 2 mL Benzene-d6 Ethylbenzene-d10 2 mL Naphthalene-d8 1 gm Toluene-d8 7 mL Compound Benzene-d6 Ethylbenzene-d10 Naphthalene-d8 $ 150 / 1 x 5 mL SAVE 20% $ 600 / 5 x 5 mL 3 comps. Mix Ratio 2 mL 2 mL 1 gm AccuPAK Reduce reordering frequency Reduce data entry time for Calibration tables due to Lot No. consistency Economical Custom Ampulling for Bulk Quantity Requirements Volumes from 0.2 mL to 20 mL • Fill Flammables • QC Services available • AccuStandard has the resources and equipment to meet your custom packaging requirements. Our full automated filler-sealer can accommodate a fill range from 0.5 to 20 mL, and ampule sizes from 1 mL to 20 mL. AccuStandard has extensive experience with Round Robin samples for ASTM committees. Call our Technical Department for a quotation. 50 ® Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5769 Member Through a collaborative effort involving the instrument manufactures, Petrochemical end users, and Chemical Reference Standard manufacturers, the following proposed D-5769 method is under consideration. A number of end users would like to evaluate this proposed D-5769 method and have asked AccuStandard to make the standards. We have formulated the following certified standards to meet those requests. ASTM D-5769-XX Calibration Curve with No Internal Standard Added ASTM-P-0140-SET $ 1500 / Set of 5 x 5 mL 05 014 -0 -P M ST A 04 014 -0 -P M ST 03 A 014 -0 -P M ST 02 A 014 -0 -P M ST 01 A 014 -0 -P M ST A Core Calibr. Mix Level 1 Compound Target Mass % Level 2 Level 3 Level 4 Level 5 Mass % Mass % Mass % Mass % Benzene 5 Toluene 12 Ethylbenzene 5 1,3-Dimethylbenzene 10 1,4-Dimethylbenezene 5 1,2-Dimethylbenezene 5 (1-Methylethyl)-benzene 3 1-Methyl-3-ethylbenzene 3 1-Methyl-4-ethylbenzene 3 1,3,5-Trimethylbenzene 3 1-Methyl-2-ethylbenzene 3 1,2,4-Trimethylbenzene 6 1,2,3-Trimethylbenzene 3 Indan 3 1,2-Diethylbenzene 2 2 NaphthaleneA A 2-Methylnaphthalene 2 1-MethylnaphthaleneA 2 Isooctane (solvent) * balance 3 9 3.75 7.5 3.75 3.75 2.25 2.25 2.25 2.25 2.25 4.5 2.25 2.25 1.5 1.5 1.5 1.5 balance 1 6 2.5 5 2.5 2.5 1.5 1.5 1.5 1.5 1.5 3 1.5 1.5 1 1 1 1 balance 0.5 3 1.25 2.5 1.25 1.25 0.75 0.75 0.75 0.75 0.75 1.5 0.75 0.75 0.5 0.5 0.5 0.5 balance 0.1 0.5 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.2 0.1 0.1 0.1 balance A = This component is a solid at room temperature Technical Note 4 Comp. Deuterated Internal Std. Mix 4 Comp. Deuterated Internal Std. Mix ASTM-P-0140-IS ASTM-P-0140-IS-PAK ASTM-P-0140-IS2 ASTM-P-0140-IS2-PAK Compound Mass % Benzene-d6 2 Ethylbenzene-d10 2 $ 75 / 1 x 10 mL $ 300 / 5 x 10 mL 4 comps. Compound Mass % Naphthalene-d8 1 Isooctane * balance Compound Mass % Benzene-d6 2 Ethylbenzene-d10 2 $ 95 / 1 x 10 mL $ 380 / 5 x 10 mL 5 comps. Compound Mass % Naphthalene-d8 1 Toluene-d8 7 Isooctane * balance Performance Evalutation Standard Composition of Daily QC Standard ASTM-P-0140-PES ASTM-P-0140-PES-PAK ASTM-P-0140-QC ASTM-P-0140-QC-PAK $ 55 / 1 x 1 mL $ 220 / 5 x 1 mL 11 comps. Target Compound Mass % Benzene 1 1,2-Diethylbenzene 0.005 1,3,5-Trimethylbenzene 1 1-Methyl-2-ethylbenzene 1 Styrene 0.1 Indene 0.1 Biphenyl 0.1 1,2,4,5-Tetramethylbenzene 1 1,2,3,5-Tetramethylbenzene 1 Hexadecane 1 Isooctane:Toluene(1:1) * balance Compound Benzene Toluene Ethylbenzene 1,3-Dimethylbenzene 1,2-Dimethylbenzene 1,2,4-Trimethylbenzene 1,2-Diethylbenzene Naphthalene Isooctane (solvent) * * The isooctane balance is the amount of material to make up a 100 mL calibration standard. Certificate will reflect actual weight of each component in the 100 mL batch including the isooctane. $ 125 / 1 x 10 mL $ 500 / 5 x 10 mL 9 comps. Target Mass % 1 10 3 6 3 3 0.02 1 balance Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 51 ASTM Summary Proposed Modifications for D-5769 • Calibration standards when combined with internal standards are diluted into significantly more isooctane. • The analytes in the Performance Standard have been expanded to better tune the GC/MS system for optimum performance. • The number of components in the QA/QC mix has been reduced with new QA/QC tolerances. • The number of analytes in the calibration mix has been reduced. • Samples that exceed the linear range are to be diluted, reducing the number of extra calibration points required. Method ASTM Standards 5771 5772 5773 5863 Member ASTM D-5771 Cloud Point of Petroleum Products ASTM See page 5 for AccuStandard’s comprehensive line of certified Cloud Point Standards. ASTM D-5772 Cloud Point of Petroleum Products (Linear Cooling Rate Method) See page 5 for AccuStandard’s comprehensive line of certified Cloud Point Standards. ASTM D-5773 Cloud Point of Petroleum Products (Constant Cooling Rate Method) WEAR METALS See page 5 for AccuStandard’s comprehensive line of certified Cloud Point Standards. ASTM D-5863 Nickel, Vanadium, Iron, & Sodium in Crude Oils & Residual Fuels by Flame AA Spectrometry Originally designed for D-5863-00 Test Method A - Sample Decomposition with Acid for Total Ni, V and Fe Determination Stock Multi-Element Matrix Blank Aqueous Standard Nitric Acid Blank D-5863-95A-10X-1 2-5% HNO3 Iron Nickel µg/mL 100 200 $ 75 / 1 x 100 mL 3 comps. Vanadium µg/mL 200 CLP-BLN-5 CLP-BLN-L $ 30 / 500 mL SAVE 33% $ 45 / L (2 x 500 mL) 5% HNO3 in ASTM Type I Water Individual High Concentration Elements in Aqueous Matrix Element Matrix Iron Fe 1,000 µg/mL Conc. Cat. No. Price Unit 500 mL ICP-27N-5 $ 67 in HNO3 Nickel Ni in HNO3 500 mL ICP-37N-5 67 Vanadium V2O5 500 mL ICP-67N-5 67 Standards of Interest See page 73-75 for additional Trace Metal Standards by AA. in HNO3 Test Method B - Sample Dilution with Organic Solvent for the Determination of Ni, V and Na using Oil-Soluble Metals as Calibrants. Stock Multi-Element Standard in Mineral Oil D-5863-95B-10X At stated conc. in 20 cst Mineral Oil Sodium Nickel 52 µg/g 50 200 Vanadium $ 160 / 1 x 4 oz 3 comps. µg/g 150 Standards of Interest See pages 59-65 for AccuStandard’s comprehensive line of Certified Oil Dissolved Wear Metal calibration standards designed for flame AA Applications. Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 5901 5986 Member ASTM D-5901 Freezing Point Aviation Fuels (Automated Optical Method) Standards of Interest See page 5 for AccuStandard’s comprehensive line of Certified Freezing Point Standards. ASTM D-5972 Freezing Point Aviation Fuels (Automated Phase Transition Method) See page 5 for AccuStandard’s comprehensive line of Certified Freezing Point Standards. ASTM D-5986 Oxygenates, Benzene, Toluene, C8-C12, Aromatics & Total Aromatics in Finished Gasolines by GC/FTIR Technical Note Daily Quality Control Standard (without Internal Standard) M-GRA-QC-10ML $ 125 / 1 x 10 mL M-GRA-QC-10ML-PAK SAVE 20% $ 500 / 5 x 10 mL Compound n-Hexane n-Heptane n-Octane n-Decane n-Dodecane Isooctane Benzene Wt. Ratio 12 17 17 12 5 12 1 Wt. Compound Ratio Toluene 9 Ethylbenzene 3 m-Xylene 3 o-Xylene 3 1,2,4-Trimethylbenzene 3 1,2,4,5-Tetramethylbenzene 3 13 Comp. Core Mix AccuStandard formulated this quality control standard to meet Section 11 of ASTM D-5986-96 specifications stipulating to “analyze the quality control reference material before every batch of samples. Bracket the samples with the reference materials”. Oxygenate QC samples are available on pages 1- 2 or can be custom formulated. Originally designed for D-5986-96 Standards of Interest See page 34 for AccuStandard’s Oxygenate Calibration Curve (Cat. No. M-GRO-CAL-SET) and page 46 for AccuStandard’s Aromatic Calibration Curve (Cat. No. D-5769-CAL-SET-5ML). 100 Cross Reference Table ASTM IP ISO DIN JIS AFNOR sorted by ASTM Method see beginning of Catalog Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 53 ASTM Also see Cloud Point standards used for ASTM Method D-2500 on page 5. Method ASTM Standards 6160 6258 6277 Member Originally designed for D-6160-98 ASTM D-6160 Polychlorinated Biphenyls (PCBs in Waste Materials by GC) SAVE 20% in PAK ASTM Aroclor Solutions (Individual and Kit) Aroclor # (35 µg/mL in Isooctane) Cat. No. (35 µg/mL in MeOH) Cat. No. (35 µg/mL in Hexane) Cat. No. Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor Aroclor C-216S C-221S C-232S C-242S C-248S C-254S C-260S C-262S C-268S C-216S-M C-221S-M C-232S-M C-242S-M C-248S-M C-254S-M C-260S-M C-262S-M C-268S-M C-216S-H-10X C-221S-H-10X C-232S-H-10X C-242S-H-10X C-248S-H-10X C-254S-H-10X C-260S-H-10X C-262S-H-10X C-268S-H-10X Z-008S Z-008S-M Z-008S-H-10X 1016 1221 1232 1242 1248 1254 1260 1262 1268 Kit of all 9 above 1 x 1 mL Price $ 15 15 15 15 15 15 15 15 15 Cat. No. Cat. Cat. Cat. Cat. Cat. Cat. Cat. Cat. Cat. 5 x 1 mL Price #-PAK #-PAK #-PAK #-PAK #-PAK #-PAK #-PAK #-PAK #-PAK $ 60 60 60 60 60 60 60 60 60 $ 78 / 9 x 1 mL Additional Ready-to-Inject PCB Aroclor Calibration Curves available in our Organic Catalog Originally designed for D-6258-98 ASTM D-6258 Solvent Red 164 Dye Concentration in Diesel Fuels Stock Solvent Red 26 Standard D-6258-CONC-5ML $ 45 / 1 x 5 mL Solvent Red 26 @ 300 µg/mL in Xylene D-6258 Calibration Curve D-6258-CAL-SET-5ML $ 125 / set of 6 x 5 mL Set includes the following Cat. No.’s Cat. No. Description D-6258-BL D-6258-01 D-6258-02 D-6258-03 D-6258-04 D-6258-05 Xylene Blank Solvent Red 26 Solvent Red 26 Solvent Red 26 Solvent Red 26 Solvent Red 26 Unit Dye Dye Dye Dye Dye @ @ @ @ @ 3 6 9 12 15 µg/mL in µg/mL in µg/mL in µg/mL in µg/mL in Xylene Xylene Xylene Xylene Xylene 1 1 1 1 1 1 x x x x x x 5 5 5 5 5 5 mL mL mL mL mL mL ASTM D-6277 Benzene in Spark - Ignition Engine Fuels using Mid Infrared Spectroscopy See page 1 for AccuStandard’s QA/QC material reference in the method. Member 54 Technical Note Solvent Red 26 is the azo dye standard against which the concentration of Solvent Red 164 is measured. The visible spectrum of Solvent Red 164 is virtually identical to the spectrum of Solvent Red 26. AccuStandard is an active member in ASTM and strives to keep abreast of ASTM method revisions. If our listed formulation does not meet the most recent method revision, please contact Technical Support, ext. 117 for an updated product. Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method 6293 6296 Member ASTM D-6293 Oxygenates & Paraffin, Olefin, Naphthene, Aromatics (O-PONA) Hydrocarbon types in Low-Olefin Spark-Ignition Engine Fuels by GC Originally designed for D-6293-98 O-PONA Olefin Mix ASTM-P-0080 ASTM-P-0080-PAK ASTM-P-0081 $ 45 / 1 x 1 mL ASTM-P-0081-PAK $ 180 / 5 x 1 mL At stated conc. in Hexane : Heptane (1:1) 5 comps. Wt./Wt. % 1-Pentene 5.0 1-Hexene 2.0 1-Heptene 2.0 1-Octene 2.0 1-Nonene 3.0 $ 135 / 1 x 1 mL SAVE 26% $ 500 / 5 x 1 mL 33 comps. Wt./Wt. % Cyclopentane 1.5 n-Pentane 1.5 Cyclohexane 2.0 2,3-Dimethylbutane 2.0 n-Hexane 2.0 1-Hexene 1.5 Methylcyclohexane 3.5 4-Methyl-1-hexene 1.5 n-Heptane 3.0 cis-1,2-Dimethylcyclohexane 4.5 Isooctane 4.0 n-Octane 4.0 1,2,4-Trimethylcyclohexane 3.5 n-Nonane 3.0 n-Decane 3.5 n-Undecane 2.0 n-Dodecane 2.0 Wt./Wt. % Benzene 2.5 Toluene 2.5 trans-Decahydronaphthelene 3.5 n-Tetradecane 2.0 Ethylbenzene 3.5 o-Xylene 3.0 n-Propylbenzene 3.5 1,2,4-Trimethylbenzene 3.0 1,2,3-Trimethylbenzene 2.0 1,2,4,5-Tetramethylbenzene 2.0 Pentamethylbenzene 2.5 Ethanol 5.0 t-Butanol 4.0 MtBE 8.0 ETBE 3.0 TAME 5.0 ASTM O-PONA System Validation Mixture O-PONA Paraffin Mix ASTM-P-0082 $ 25 / 1 x 1 mL ASTM-P-0082-PAK $ 100 / 5 x 1 mL At stated conc. in Hexane : Heptane (1:1) 2 comps. Wt./Wt. % n-Nonane 5.0 n-Decane 2.0 O-PONA Paraffin Mix Standards of Interest ASTM-P-0082-R1 $ 25 / 1 x 1 mL ASTM-P-0082-R1-PAK $ 100 / 5 x 1 mL At stated conc. in Hexane : Heptane (1:1) 2 comps. For the mandatory real world QC samples stipulated in QA/QC section 8.6 of the method see pages 1-2. Wt./Wt. % 3.0 3.0 n-Nonane n-Decane ASTM D-6296 Total Olefins in Spark-Ignition Engine Fuels by Multidimensional GC Originally designed for D-6296-98 System Setup & Verification Standards D-6296-VER-SET $ 40 / 2 x 1 mL Set contains 1 ampule of each Cat. No. listed below D-6296-VER-SET-PAK SAVE 23% $ 150 / 5 x (2 x 1 mL) 5 sets containing 1 ampule of each Cat. No. listed below System Setup & Verification Standards System Setup & Verification Standards D-6296-VER1 D-6296-VER2 1 x 1 mL 2 comps. Wt. % 5% 95% MTBE Isooctane 1 x 1 mL 2 comps. Wt. % 5% 95% ETBE Isooctane Calibration Standard with MTBE Calibration Standard with ETBE D-6296-CAL1 D-6296-CAL1-PAK D-6296-CAL2 D-6296-CAL2-PAK Pentene Hexene Heptene Octene Nonene Wt. % 1.0 1.0 1.0 1.0 1.0 $ 65 / 1 x 1 mL SAVE 23% $ 250 / 5 x 1 mL 10 comps. Decene Undecane Dodecane Isooctane MTBE Wt. % 1.0 1.0 1.0 87.0 5.0 Pentene Hexene Heptene Octene Nonene Decene Wt. % 1.0 1.0 1.0 1.0 1.0 1.0 $ 65 / 1 x 1 mL SAVE 23% $ 250 / 5 x 1 mL 11 comps. Decane Undecane Dodecane Isooctane ETBE Wt. % 1.0 1.0 1.0 86.0 5.0 Isooctane Blank Compensation Standard D-6296-BL $ 15 / 1 x 5 mL Isooctane (Neat) Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 55 Method ASTM Standards 6304 6334 6352 Member ASTM ASTM D-6304 Determination of Water in Petroleum Products Lubricating oil, and additives by Coulometric Karl Fischer Titration See page 5 for AccuStandard’s comprehensive line of Certified Water Standards, for Karl Fischer Analysis. ASTM D-6334 Sulfur in Gasoline by Wavelength Dispersive X-Ray Fluorescence See Sulfur Standards Group listing in the Table of Contents for AccuStandard’s comprehensive line of Certified Sulfur Calibration Standards. ASTM D-6352 Boiling Range Distribution of Petroleum Distillates from 174 to 700ºC by GC Polywax 850® Polywax 500® ASTM-P-0051N-2G $ 20 / 2 grams ASTM-P-0137N-2G Contact AccuStandard’s Technical Department regarding the availability of a QA/QC Reference Oil Sample under development in ASTM. Polywax 1000® Polywax 655® $ 20 / 2 grams ASTM-P-0138N-2G $ 20 / 2 grams Polywax 1000 Polywax 655 Calibration Mix Hydrocarbon Window Defining Standard* DRH-008S-R2 $ 65 / 1 x 1 mL DRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL 500 µg/mL each in Chloroform 35 comps. Octane Nonane Decane Undecane Dodecane Tridecane Tetradecane Pentadecane Hexadecane Heptadecane Octadecane Pristane Standards of Interest $ 20 / 2 grams Polywax 850 Polywax 500 ASTM-P-0053N-2G Originally designed for D-6352-98 Nonadecane Phytane Eicosane Heneicosane Docosane Tricosane Tetracosane Pentacosane Hexacosane Heptacosane Octacosane Nonacosane Triacontane n-Hentriacontane Dotriacontane Tritriacontane Tetratriacontane Pentatriacontane Hexatriacontane Heptatriacontane Octatriacontane Nonatriacontane Tetracontane * Can be shipped by Air and Sea ASTM D-6378 DRH-002N DRH-002N-10X Wt. % n-Hexane 6 n-Heptane 6 n-Octane 8 n-Nonane 8 n-Decane 12 n-Undecane 12 n-Dodecane 12 n-Tetradecane 12 n-Hexadecane 10 $ 10 / 100 mg $ 40 / 1 gm 17 comps. Wt. n-Octadecane n-Eicosane n-Tetracosane n-Octacosane n-Dotriacontane n-Hexatriacontane n-Tetracontane n-Tetratetracontane % 5 2 2 1 1 1 1 1 Column Test Mixture ASTM-D2887 1% v/v in n-Octane n-Hexadecane $ 10 / 1 x 1 mL 2 comps. n-Octadecane Vapor Pressure (VPx) of Petroleum Products, Hydrocarbons, & Hydrocarbon-Oxygenate Mixtures (Triple Expansion Method) See pages 29 & 32 for AccuStandard’s comprehensive line of Vapor Pressure Standards & Instrument Quality Control Samples. 56 Quality System is Certified to comply with the International ISO 9001 Quality Standard ASTM Standards Method Member ASTM D-6379 Aromatic Hydrocarbon Types in Aviation Fuels & Petroleum Distillates HPLC method with Refractive Index D-6379 Calibration Curve D-6379-SRS $ 40 / 1 x 1 mL D-6379-SRS-PAK SAVE 30% $ 140 / 5 x 1 mL At stated Conc. in n-Heptane 3 comps. D-6379-SET $ 100 / 4 x 1 mL D-6379-SET-PAK SAVE 30% $ 350 / 5 x (4 x 1 mL) At stated Conc. in n-Heptane Cyclohexane o-Xylene 1-Methyl naphthalene 10 mg/mL 0.5 mg/mL 0.05 mg/mL Analyte Std. 1 (mg/mL) Cyclohexane o-Xylene 1-Methyl naphthalene D-6591 IP 391 Std. 2 (mg/mL) Std. 3 (mg/mL) Std. 4 (mg/mL) 2 5 1.0 0.5 1.0 0.2 0.1 0.1 0.05 5 15 5 Originally designed for D-6379-99 ASTM System Resolution Standard Aromatic Hydrocarbon Types in Middle Distillates HPLC method with Refractive Index Detection System Performance Standard IP 391-95 Calibration Curve ASTM-P-0135 ASTM-P-0135-PAK SAVE 20% At stated Conc. in n-Heptane Cyclohexane o-Xylene Dibenzothiophene 9-Methylanthracene ASTM-P-0136-SET At stated Conc. in n-Heptane ASTM D-6417 $ 75 / 1 x 5 mL $ 300 / 5 x 5 mL 4 comps. 10 mg/mL 5.0 mg/mL 0.5 mg/mL 0.5 mg/mL Analyte $ 145 / 4 x 1 mL Std. 1 (mg/mL) Std. 2 (mg/mL) Std. 3 (mg/mL) Std. 4 (mg/mL) 50 40 40 4 20 10 10 2 5 2.5 2.5 0.5 1 0.5 0.2 0.1 Cyclohexane o-Xylene 1-Methyl naphthalene Phenanthrene Standards of Interest Estimation of Engine Oil Volatility by Capillary GC See ASTM Methods D-3710, D-5307, D-5442, D-6352 for additional calibration standards for hydrocarbon analysis. See page 15 for Alkane and Polywax standards suitable for D-6417. ASTM D-6428 Sulfur by Combustion and Electrochemical Detection D-6428-R1-4-SET D-6428-R1-SET Sulfur as Dibenzothiophene D-6428-R1-4-SET Cat. No. Unit D-6428-R1-SET Cat. No. Sulfur Sulfur Sulfur Sulfur Sulfur Sulfur Sulfur D-6428-BL-4 D-6428-0.1X-4 D-6428-0.5X-4 D-6428-1X-4 D-6428-2.5X-4 D-6428-5X-4 D-6428-10X-4 4 4 4 4 4 4 4 D-6428-BL D-6428-0.1X D-6428-0.5X D-6428-1X D-6428-2.5X D-6428-5X D-6428-10X Blank @ 0.1 µg/g @ 0.5 µg/g @ 1.0 µg/g @ 2.5 µg/g @ 5.0 µg/g @ 10 µg/g oz oz oz oz oz oz oz D-6428-R2-4-SET D-6428-R2-SET Sulfur as Dibenzothiophene Unit 1 1 1 1 1 1 1 mL mL mL mL mL mL mL $ 275 / 6 x 4 oz $ 65 / 6 x 1 mL Description D-6428-R2-4-SET Cat. No. Unit D-6428-R2-SET Cat. No. Sulfur Sulfur Sulfur Sulfur Sulfur Sulfur D-6428-BL-4 D-6428-10X-4 D-6428-25X-4 D-6428-50X-4 D-6428-75X-4 D-6428-100X-4 4 4 4 4 4 4 D-6428-BL D-6428-10X D-6428-25X D-6428-50X D-6428-75X D-6428-100X Blank @ 10 µg/g @ 25 µg/g @ 50 µg/g @ 75 µg/g @ 100 µg/g NEW $ 300 / 7 x 4 oz $ 65 / 7 x 1 mL Description oz oz oz oz oz oz Unit 1 1 1 1 1 1 6379 IP 391 6417 6428 mL mL mL mL mL mL Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 57 Method ASTM Standards 6443 6481 6550 Member ASTM ASTM D-6443 Cat. No. Ca (Wt.%) Cl (Wt.%) Cu (Wt.%) Mg (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.020 0.020 0.020 0.020 0.400 0.400 0.400 0.400 0.200 0.000 0.030 0.020 0.200 0.200 0.020 0.020 0.200 0.200 0.100 0.000 0.010 0.050 0.010 0.050 0.010 0.050 0.010 0.050 0.025 0.000 0.200 0.200 0.040 0.040 0.040 0.040 0.200 0.200 0.080 0.000 0.250 0.020 0.250 0.020 0.020 0.250 0.020 0.250 0.150 0.000 1.000 0.020 0.150 1.000 1.000 0.020 0.020 1.000 0.500 0.000 0.020 0.250 0.250 0.020 0.250 0.020 0.050 0.250 0.100 0.000 ASTM D-6445 Originally designed for D-6443-99 Standards of Interest Lubricating Oil, Elements, WLXRF ASTM Method (Nominal Value) Wt.% listed below ASTM-P-0117-SET $ 2100 / 10 x 100 mL ASTM-P-0117-01 ASTM-P-0117-02 ASTM-P-0117-03 ASTM-P-0117-04 ASTM-P-0117-05 ASTM-P-0117-06 ASTM-P-0117-07 ASTM-P-0117-08 ASTM-P-0117-09 ASTM-P-0117-10 WEAR METALS Ca, Cl, Cu, Mg, P, S, Zn in Unused Lubricating Oils & Additives by Wavelength Dispersive X-ray Fluorescence & Spectrometry See the Wear Metal Group listing in the Table of Contents for AccuStandard’s comprehensive line of Certified Oil Dissolved Wear Metal Calibration Standards. Sulfur in Gasoline by ED - XRF See the Sulfur Standards Group listing in the Table of Contents for AccuStandard’s comprehensive line of Certified Sulfur Calibration Standards. ASTM D-6481 P, S, Ca and Zn in Lube Oils by ED-XRF Originally designed for D-6481-99 Lubricating Oil, Elements, EDXRF ASTM Method (Nominal Value) Wt.% listed below ASTM-P-0114-SET $ 1900 / 17 x 100 mL Cat. No. ASTM-P-0114-01 ASTM-P-0114-02 ASTM-P-0114-03 ASTM-P-0114-04 ASTM-P-0114-05 ASTM-P-0114-06 ASTM-P-0114-07 ASTM-P-0114-08 ASTM-P-0114-09 ASTM-P-0114-10 ASTM-P-0114-11 ASTM-P-0114-12 ASTM-P-0114-13 ASTM-P-0114-14 ASTM-P-0114-15 ASTM-P-0114-16 ASTM-P-0114-17 Ca (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.005 0.600 0.000 1.000 0.000 0.005 0.500 0.010 0.050 0.100 0.200 0.400 0.600 0.800 1.000 0.400 0.000 0.005 0.000 0.300 0.000 0.000 0.250 0.150 0.200 0.010 0.150 0.200 0.005 0.100 0.010 0.300 0.050 0.000 0.050 0.000 0.000 1.000 0.000 0.800 0.500 0.100 0.400 0.200 0.800 0.800 0.500 0.050 1.000 0.600 0.000 0.050 0.000 0.000 0.000 0.300 0.300 0.150 0.250 0.075 0.200 0.100 0.300 0.050 0.100 0.150 0.250 0.000 ASTM D-6550 Olefin Content of Gasolines by SFC Stock Olefin Calibration Standard D-6550-CONC D-6550-CONC-5ML At stated Conc. by Wt. % Wt. % 1-Nonene 2.5 Cyclohexene 5 1-Hexene 5 1-Octene 5 1-Decene 5 2-Methyl-1,3-butadiene 5 4-Methyl-1-pentene 5 1,5-Hexadiene 3 58 $ 80 / 1 x 1 mL $ 350 / 1 x 5 mL 15 comps. Wt. % 3-Methyl-1,3-pentadiene 2 2-Methyl-1-butene 25 2-Methyl-2-pentene 10 1-Heptene 10 2-Methyl-1-octene 2.5 2-Methyl-1-heptene 5 5-Methyl-1-hexene 10 Originally designed for D-6550-00 Standards of Interest Technical Note AccuStandard worked in conjunction with the D-02 technical committee and Shell Oil to develop this stock Olefin Standard proven useful in creating the required calibration curve. See page 2 for consensus value QA/QC material available for this method. Quality System is Certified to comply with the International ISO 9001 Quality Standard Organometallic Standards Wear Metals for AA, ICP, DCP & XRF Analysis These Standards were formulated for the analysis of metals in oils and other organic matrices. These Standards and curves provide a convenient way to analyze for metals (wear metals, additives and contaminants) in lubricating oils, gasolines, residual oils, crude oils, turbine fuels and environmental samples. All standards undergo rigorous quality assurance checks. Major constituents in the final Standard are typically analyzed by both plasma emission and rotrode techniques. Organometallic Standards listed on this page may contain sulfur which can be introduced by possible sulfonate starting materials used to formulate the actual organometallic standard. AccuStandard has developed a New Premium Organometallic line for those clients preferring to have organometallic standards with <1 ppm sulfur or phosphorous (see Table of Contents). Single & Multi Element Standards Prepared Calibration Curves Formulated from Ultra High Purity Organometallic Starting materials & matrices Comprehensive Certificate of Analysis Organometallic Wear Metals 21 Wear Metal Multi-Element Standard Conc. (µg/g) Cat. No. Price 10 30 50 100 300 500 900 WM-21-1X-4 WM-21-3X-4 WM-21-5X-4 WM-21-10X-4 WM-21-30X-4 WM-21-50X-4 WM-21-90X-4 $ 80 80 85 90 145 210 320 WM-21-SET-4 $ 900 set of above 7 x 4 oz. 12 Wear Metal Multi-Element Standard Cat. No. Price Conc. (µg/g) Cat. No. WM-21-1X-8 WM-21-3X-8 WM-21-5X-8 WM-21-10X-8 WM-21-30X-8 WM-21-50X-8 WM-21-90X-8 $ 100 100 105 160 260 380 580 10 30 50 100 300 500 900 WM-12-1X-4 WM-12-3X-4 WM-12-5X-4 WM-12-10X-4 WM-12-30X-4 WM-12-50X-4 WM-12-90X-4 WM-21-SET-8 $ 1500 set of above 7 x 8 oz. Price Cat. No. $ 70 70 80 85 100 150 210 Price WM-12-1X-8 WM-12-3X-8 WM-12-5X-8 WM-12-10X-8 WM-12-30X-8 WM-12-50X-8 WM-12-90X-8 WM-12-SET-4 $ 700 set of above 7 x 4 oz. $ 90 90 100 150 180 270 380 WM-12-SET-8 $ 1100 set of above 7 x 8 oz. Each Wear Metal Standard contains the below list of 21 elements in hydrocarbon oil at the stated concentration Each Wear Metal Standard contains the below list of 12 elements in hydrocarbon oil at the stated concentration Ag (Silver) Al (Aluminum) B (Boron) Ba (Barium) Ca (Calcium) Cd (Cadmium) Ag (Silver) Al (Aluminum) Cr (Chromium) Cu (Copper) Cr (Chromium) Cu (Copper) Fe (Iron) Mg (Magnesium) Mn (Manganese) Mo (Molybdenum) Na (Sodium) Ni (Nickel) P (Phosphorus) Pb (Lead) Si (Silicon) Sn (Tin) Ti (Titanium) V (Vanadium) Zn (Zinc) Organometallic Wear Metals Single Elements Matrix Oil & Stabilizer Organometallic ICP/XRF @ 1000 µg/g in 20 cSt base oil 2 oz. bottle Organometallic ICP/XRF @ 5000 µg/g in 75 cSt base oil 2 oz. bottle Element Cat. No. Cat. No. Cat. No. Aluminum Antimony Arsenic Barium Bismuth Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Lithium Magnesium Manganese Mercury Molybdenum Nickel Phosphorous Potassium Scandium Silicon Silver Sodium Strontium Thallium Tin Titanium Vanadium Zinc Zirconium WM-AA-01 WM-AA-02 -------------WM-AA-04 -------------WM-AA-07 WM-AA-08 WM-AA-09 WM-AA-13 WM-AA-14 WM-AA-15 WM-AA-27 WM-AA-29 WM-AA-30 WM-AA-32 WM-AA-33 -------------WM-AA-35 WM-AA-37 WM-AA-41 WM-AA-43 -------------WM-AA-52 WM-AA-53 WM-AA-54 WM-AA-55 -------------WM-AA-63 WM-AA-64 WM-AA-67 WM-AA-70 -------------- $ 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 36 WM-20CST-01 WM-20CST-02 WM-20CST-03 WM-20CST-04 WM-20CST-06 WM-20CST-07 WM-20CST-08 WM-20CST-09 WM-20CST-13 -------------------WM-20CST-15 WM-20CST-27 WM-20CST-29 WM-20CST-30 WM-20CST-32 WM-20CST-33 WM-20CST-34 WM-20CST-35 WM-20CST-37 WM-20CST-41 WM-20CST-43 WM-20CST-50 WM-20CST-52 WM-20CST-53 WM-20CST-54 WM-20CST-55 WM-20CST-60 WM-20CST-63 WM-20CST-64 WM-20CST-67 WM-20CST-70 WM-20CST-71 Price $ 32 32 40 32 32 32 32 32 32 56 32 32 32 32 32 42 32 32 32 32 130 56 56 32 32 42 32 32 32 32 32 WM-75CST-01-5X WM-75CST-02-5X -----------------------WM-75CST-04-5X WM-75CST-06-5X WM-75CST-07-5X WM-75CST-08-5X WM-75CST-09-5X WM-75CST-13-5X -----------------------WM-75CST-15-5X WM-75CST-27-5X WM-75CST-29-5X WM-75CST-30-5X WM-75CST-32-5X WM-75CST-33-5X -----------------------WM-75CST-35-5X WM-75CST-37-5X WM-75CST-41-5X WM-75CST-43-5X -----------------------WM-75CST-52-5X WM-75CST-53-5X WM-75CST-54-5X ----------------------------------------------WM-75CST-63-5X WM-75CST-64-5X WM-75CST-67-5X WM-75CST-70-5X WM-75CST-71-5X Desc. Cat. No. Price ORGANOMETALLIC C Organometallic AA @ 1000 µg/g in hydrocarbon oil 100 mL Price Pb (Lead) Si (Silicon) Sn (Tin) Ti (Titanium) Fe (Iron) Mg (Magnesium) Na (Sodium) Ni (Nickel) 75 cSt Oil MOSOL-75-16 $ 10 / 16 oz. 20 cSt Oil MOSOL-20-16 $ 10 / 16 oz. Price $ 45 45 45 45 45 45 45 45 170 45 45 45 45 45 45 45 45 45 170 170 45 Stabilizer IS-7281-2OZ $ 95 / 1 x 2 oz. Metals Additives Standards MA-900-4 MA-900-8 $ 100 / 4 oz. $ 140 / 8 oz. Ba, Ca, Mg, P and Zn at 900 µg/g each in Hydrocarbon oil Test to Low ppb Sulfur See Pages 6-11 45 45 45 45 45 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 59 Organometallic Standards Wear Metals Premium Sulfur-Free These highly concentrated stabilized solutions can be used for customer specific formulations of additive elements in lubricating oils, iron, nickel and vanadium in residual oil, and wear metals in oils. These organometallic solutions can also be used to prepare single element or multi-element standards for plasma emission (ICP or DCP), rotating disk (rotrode), or atomic absorption spectroscopy (AA). The starting materials for the standards are PURE REAGENTS and have been certified against NIST SRM’s whenever available. THEY DO NOT CONTAIN PHOSPHORUS OR SULFUR. TRACE IMPURITIES ARE DOCUMENTED ON THE CERTIFICATE OF ANALYSIS. Highly Concentrated Liquid Organo-Metallic Standards Sulfur/Phosphorous free (< 1 ppm) Stabilized Ready for Use Organometallic Single-Element Concentrates Element Conc. (Wt. %) ORGANOMETALLIC C Aluminum Barium Boron Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Phosphorus Praseodymium Selenium Strontium Thallium Titanium Vanadium Zinc Zirconium 3 12.5 2.5 10 5 2.5 7.5 6 4 20 3 7.5 5 5 5 3 3.5 10 5 5 2 6 5 Cat. No. Price 25 grams WM-NMS-01-30X-25G WM-NMS-04-125X-25G WM-NMS-07-25X-25G WM-NMS-08-100X-25G WM-NMS-09-50X-25G WM-NMS-13-25X-25G WM-NMS-14-75X-25G WM-NMS-15-60X-25G WM-NMS-27-40X-25G WM-NMS-29-200X-25G WM-NMS-32-30X-25G WM-NMS-33-75X-25G WM-NMS-35-50X-25G WM-NMS-37-50X-25G WM-NMS-41-50X-25G WM-NMS-44-30X-25G WM-NMS-51-35X-25G WM-NMS-55-100X-25G WM-NMS-60-50X-25G WM-NMS-64-50X-25G WM-NMS-67-20X-25G WM-NMS-70-60X-25G WM-NMS-71-50X-25G $ 150 540 130 510 250 145 330 250 220 900 180 330 215 250 250 175 200 510 265 215 115 270 250 Cat. No. Premium Sulfur-Free Price 50 grams WM-NMS-01-30X-50G WM-NMS-04-125X-50G WM-NMS-07-25X-50G WM-NMS-08-100X-50G WM-NMS-09-50X-50G WM-NMS-13-25X-50G WM-NMS-14-75X-50G WM-NMS-15-60X-50G WM-NMS-27-40X-50G WM-NMS-29-200X-50G WM-NMS-32-30X-50G WM-NMS-33-75X-50G WM-NMS-35-50X-50G WM-NMS-37-50X-50G WM-NMS-41-50X-50G WM-NMS-44-30X-50G WM-NMS-51-35X-50G WM-NMS-55-100X-50G WM-NMS-60-50X-50G WM-NMS-64-50X-50G WM-NMS-67-20X-50G WM-NMS-70-60X-50G WM-NMS-71-50X-50G $ 210 780 180 710 355 200 450 355 300 1260 252 450 294 350 350 240 270 710 360 295 150 380 355 Sulfur below detection limits Organometallic Single-Element Stock Standards Technical Note Element Sulfur free Organometallic @ 1000 µg/g Price Cat. No. 50 mL Sulfur free Organometallic @ 5000 µg/g Price Cat. No. 50 mL Aluminum Antimony Barium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Molybdenum Nickel Phosphorous Potassium Selenium Silicon Sodium Strontium Thallium Tin Titanium Vanadium Yttrium Zinc Zirconium WM-NMS-01 WM-NMS-02 WM-NMS-04 WM-NMS-08 WM-NMS-09 WM-NMS-13 WM-NMS-14 WM-NMS-15 WM-NMS-27 WM-NMS-29 WM-NMS-32 WM-NMS-33 WM-NMS-35 WM-NMS-37 WM-NMS-41 WM-NMS-43 WM-NMS-51 WM-NMS-52 WM-NMS-54 WM-NMS-55 WM-NMS-60 WM-NMS-63 WM-NMS-64 WM-NMS-67 WM-NMS-68 WM-NMS-70 WM-NMS-71 WM-NMS-01-5X WM-NMS-02-5X WM-NMS-04-5X WM-NMS-08-5X WM-NMS-09-5X WM-NMS-13-5X WM-NMS-14-5X WM-NMS-15-5X WM-NMS-27-5X WM-NMS-29-5X WM-NMS-32-5X WM-NMS-33-5X WM-NMS-35-5X WM-NMS-37-5X WM-NMS-41-5X WM-NMS-43-5X WM-NMS-51-5X WM-NMS-52-5X WM-NMS-54-5X WM-NMS-55-5X WM-NMS-60-5X WM-NMS-63-5X WM-NMS-64-5X WM-NMS-67-5X WM-NMS-68-5X WM-NMS-70-5X WM-NMS-71-5X These standards are sulfur free (below detection limits) organometallic standards for X-ray Fluorescence (XRF), plasma emission (ICP or DCP), rotating disk (rotrode), or atomic absorption (AA). They are stabilized for blending together with other Analytes to prepare multi-element standards. 60 $ 50 50 50 50 50 50 75 75 50 50 50 50 50 50 50 50 60 75 50 50 60 50 50 50 60 50 50 $ 90 90 90 90 90 90 110 110 90 90 90 90 90 90 90 90 100 110 90 90 100 90 90 90 100 90 90 Stabilization Solutions The solutions were specifically designed for chelating and solubilizing the organometallic line of solids and solutions for single and multi-element standards. Stabilizer Solutions A ASTM-P-0122-0.5 ASTM-P-0122-1 $ 80 / 50 mL $ 120 / 100 mL Stabilizer Solutions B ASTM-P-0123-0.5 $ 80 / 50 mL ASTM-P-0123-1 $ 120 / 100 mL (use in conjunction with stabilizer solution A) Quality System is Certified to comply with the International ISO 9001 Quality Standard Organometallic Standards Wear Metals Premium Sulfur-Free Wear Metals Multi-Element 12 Wear Metal Multi-Element Standard Containing No Metallic Sulfonates 11 Wear Metal Multi-Element Standard Containing No Metallic Sulfonates Conc. (µg/g) Cat. No. Price Conc. (µg/g) Cat. No. Price 10 30 50 100 300 500 900 WM-11-NMS-1X-1 WM-11-NMS-3X-1 WM-11-NMS-5X-1 WM-11-NMS-10X-1 WM-11-NMS-30X-1 WM-11-NMS-50X-1 WM-11-NMS-90X-1 $ 130 130 130 140 165 245 325 10 30 50 100 300 500 WM-12-NMS-1X-1 WM-12-NMS-3X-1 WM-12-NMS-5X-1 WM-12-NMS-10X-1 WM-12-NMS-30X-1 WM-12-NMS-50X-1 $ 135 135 135 145 170 250 Each Wear Metal Standard contains 12 elements in hydrocarbon oil at the stated concentration Each Wear Metal Standard contains 11 elements in hydrocarbon oil at the stated concentration Ag (Silver) Al (Aluminum) Cr (Chromium) Cu (Copper) Fe (Iron) Mg (Magnesium) Ni (Nickel) Pb (Lead) Si (Silicon) Sn (Tin) Ti (Titanium) Na (Sodium) Ni (Nickel) Pb (Lead) Si (Silicon) Sn (Tin) Ti (Titanium) 21 Wear Metal Multi-Element Standard Containing No Metallic Sulfonates 20 Wear Metal Multi-Element Standard Containing No Metallic Sulfonates Cat. No. Price Conc. (µg/g) Cat. No. Price 10 30 50 100 300 500 900 WM-20-NMS-1X-1 WM-20-NMS-3X-1 WM-20-NMS-5X-1 WM-20-NMS-10X-1 WM-20-NMS-30X-1 WM-20-NMS-50X-1 WM-20-NMS-90X-1 $ 150 150 150 170 230 350 500 10 30 50 100 300 500 WM-21-NMS-1X-1 WM-21-NMS-3X-1 WM-21-NMS-5X-1 WM-21-NMS-10X-1 WM-21-NMS-30X-1 WM-21-NMS-50X-1 $ 160 160 160 180 240 350 ORGANOMETALLIC C Conc. (µg/g) WM-21-NMS-SET-1 $ 1050 set of above 6 x 100 mL WM-20-NMS-SET-1 $ 1450 set of above 7 x 100 mL Each Wear Metal Standard contains 21 elements in hydrocarbon oil at the stated concentration Each Wear Metal Standard contains 20 elements in hydrocarbon oil at the stated concentration Al (Aluminum) B (Boron) Ba (Barium) Ca (Calcium) Cd (Cadmium) Cr (Chromium) Cu (Copper) Fe (Iron) Mg (Magnesium) Mn (Manganese) Sulfur below detection limits WM-12-NMS-SET-1 $ 850 set of above 6 x 100 mL WM-11-NMS-SET-1 $ 1100 set of above 7 x 100 mL Al (Aluminum) Cr (Chromium) Cu (Copper) Fe (Iron) Mg (Magnesium) Na (Sodium) Premium Sulfur-Free Ag (Silver) Al (Aluminum) B (Boron) Ba (Barium) Ca (Calcium) Cd (Cadmium) Cr (Chromium) Cu (Copper) Fe (Iron) Mg (Magnesium) Mn (Manganese) Mo (Molybdenum) Na (Sodium) Ni (Nickel) P (Phosphorus) Pb (Lead) Si (Silicon) Sn (Tin) Ti (Titanium) V (Vanadium) Zn (Zinc) Mo (Molybdenum) Na (Sodium) Ni (Nickel) P (Phosphorus) Pb (Lead) Si (Silicon) Sn (Tin) Ti (Titanium) V (Vanadium) Zn (Zinc) Test to Low ppb Sulfur See Pages 6-11 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 61 Organometallic Standards Wear Metals for AA, ICP, DCP & XRF Analysis Technical Note Concentration for the sets on pages 62-65 are targets. Actual production lots may vary. Sulfur & Metals in Oil Sulfur and Metals in Mineral Oil Sulfur and Metals in Residual Fuel Oil ASTM-P-0100-SET ASTM-P-0101-SET Cat. No. $ 1650 / 12 x 100 mL Sulfur Conc. (Wt. %) Nickel Conc. (µg/g) Vanadium Conc. (µg/g) Price 100 mL 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 0 10 100 80 40 5 60 0 100 50 20 100 0 500 25 250 100 400 300 200 0 250 500 50 $ 200 200 200 200 200 200 200 200 200 200 200 200 ASTM-P-0100-01 ASTM-P-0100-02 ASTM-P-0100-03 ASTM-P-0100-04 ASTM-P-0100-05 ASTM-P-0100-06 ASTM-P-0100-07 ASTM-P-0100-08 ASTM-P-0100-09 ASTM-P-0100-10 ASTM-P-0100-11 ASTM-P-0100-12 ORGANOMETALLIC C Cat. No. Vanadium Conc. (µg/g) Price 100 mL 0.00 0.50 1.00 1.50 2.00 2.50 3.00 3.50 4.00 4.50 5.00 5.50 0 10 100 80 40 5 60 0 100 50 20 100 0 500 25 250 100 400 300 200 0 250 500 50 $ 200 200 200 200 200 200 200 200 200 200 200 200 Sulfur and Metals in Residual Fuel Oil ASTM-P-0103-SET $ 1850 / 12 x 100 mL Sulfur Conc. (Wt. %) Iron Conc. (µg/g) Nickel Conc. (µg/g) Vanadium Conc. (µg/g) Price 100 mL 0.00 0.50 1.00 ----2.00 2.50 3.00 3.50 ----4.50 5.00 5.50 0 300 500 100 200 400 0 500 100 300 200 50 0 10 100 80 40 5 60 0 100 50 20 100 0 500 25 250 100 400 300 200 0 250 500 50 $ 200 200 200 200 200 200 200 200 200 200 200 200 ASTM-P-0102-01 ASTM-P-0102-02 ASTM-P-0102-03 ASTM-P-0102-04 ASTM-P-0102-05 ASTM-P-0102-06 ASTM-P-0102-07 ASTM-P-0102-08 ASTM-P-0102-09 ASTM-P-0102-10 ASTM-P-0102-11 ASTM-P-0102-12 Nickel Conc. (µg/g) ASTM-P-0101-01 ASTM-P-0101-02 ASTM-P-0101-03 ASTM-P-0101-04 ASTM-P-0101-05 ASTM-P-0101-06 ASTM-P-0101-07 ASTM-P-0101-08 ASTM-P-0101-09 ASTM-P-0101-10 ASTM-P-0101-11 ASTM-P-0101-12 ed for Design 08-95a D-57 M T S A Sulfur and Metals in Mineral Oil ASTM-P-0102-SET Cat. No. $ 1800 / 12 x 100 mL Sulfur Conc. (Wt. %) Cat. No. ASTM-P-0103-01 ASTM-P-0103-02 ASTM-P-0103-03 ASTM-P-0103-04 ASTM-P-0103-05 ASTM-P-0103-06 ASTM-P-0103-07 ASTM-P-0103-08 ASTM-P-0103-09 ASTM-P-0103-10 ASTM-P-0103-11 ASTM-P-0103-12 ed for Design 08-95a 7 -5 D ASTM $ 2100 / 12 x 100 mL Sulfur Conc. (Wt. %) Iron Conc. (µg/g) Nickel Conc. (µg/g) Vanadium Conc. (µg/g) Price 100 mL 0.00 0.50 1.00 ----2.00 2.50 3.00 3.50 ----4.50 5.00 5.50 0 300 500 100 200 400 0 500 100 300 200 50 0 10 100 80 40 5 60 0 100 50 20 100 0 500 25 250 100 400 300 200 0 250 500 50 $ 200 200 200 200 200 200 200 200 200 200 200 200 ISO/CD 14597 Vanadium and Nickel Standards with Manganese Internal Standard for ISO/CD 14597 Vanadium Standards - Low Range for ISO/CD 14597 with 0.05% Manganese Internal Standard in Xylene-Mineral Oil ASTM-P-0104-SET $ 1050 / 9 x 100 mL Cat. No. ASTM-P-0104-01 ASTM-P-0104-02 ASTM-P-0104-03 ASTM-P-0104-04 ASTM-P-0104-05 ASTM-P-0104-06 ASTM-P-0104-07 ASTM-P-0104-08 ASTM-P-0104-09 Vanadium Conc. (Wt.%) Price 100 mL 0.0005 0.0025 0.0050 0.0075 0.0100 0.0125 0.0150 0.0175 0.0200 $ 150 150 150 150 150 150 150 150 150 Vanadium Standards - High Range for ISO/CD 14597 with 0.05% Manganese Internal Standard in Xylene-Mineral Oil ASTM-P-0105-SET $ 780 / 7 x 100 mL Cat. No. Vanadium Conc. (Wt.%) Price 100 mL 0.0000 0.0300 0.0400 0.0500 0.0600 0.0800 0.1000 $ 135 135 135 135 135 135 135 ASTM-P-0105-01 ASTM-P-0105-02 ASTM-P-0105-03 ASTM-P-0105-04 ASTM-P-0105-05 ASTM-P-0105-06 ASTM-P-0105-07 Nickel Standards for ISO/CD 14597 with 0.05% Manganese Internal Standard in Xylene-Mineral Oil ASTM-P-0106-SET Cat. No. $ 780 / 7 x 100 mL Nickel Conc. (Wt.%) Price 100 mL 0.0000 0.0005 0.0010 0.0025 0.0050 0.0075 0.0100 $ 135 135 135 135 135 135 135 ASTM-P-0106-01 ASTM-P-0106-02 ASTM-P-0106-03 ASTM-P-0106-04 ASTM-P-0106-05 ASTM-P-0106-06 ASTM-P-0106-07 Internal Standard ASTM-P-0107-5 $ 235 / 500 mL Manganese @ 0.05 Wt. % in Xylene-Mineral Oil 62 Quality System is Certified to comply with the International ISO 9001 Quality Standard Organometallic Standards Wear Metals for AA, ICP, DCP & XRF Analysis Lubricating Oil Standards ed for Design 481-99 -6 D ASTM Lubricating Oil, Elements Wt.% (Nominal Value) listed below ASTM-P-0109-SET $ 1600 / 17 x 100 mL Lubricating Oil, Elements Wt.% (Nominal Value) listed below ASTM-P-0108-SET $ 1900 / 17 x 100 mL Cat. No. P (Wt.%) S (Wt.%) Zn (Wt.%) 0.600 0.500 0.400 0.260 0.005 0.400 0.300 0.200 0.060 0.060 0.050 0.025 0.005 0.170 0.100 0.010 0.000 0.005 0.200 0.150 0.250 0.005 0.025 0.060 0.100 0.080 0.050 0.120 0.150 0.200 0.250 0.100 0.010 0.000 0.175 0.050 0.300 0.150 0.450 0.350 0.250 0.450 0.300 0.200 0.100 0.200 0.400 0.550 0.200 0.600 0.000 0.060 0.080 0.180 0.120 0.070 0.100 0.120 0.100 0.130 0.050 0.075 0.130 0.150 0.110 0.200 0.250 0.000 Standard Cat. No. ASTM-P-0109-01 ASTM-P-0109-02 ASTM-P-0109-03 ASTM-P-0109-04 ASTM-P-0109-05 ASTM-P-0109-06 ASTM-P-0109-07 ASTM-P-0109-08 ASTM-P-0109-09 ASTM-P-0109-10 ASTM-P-0109-11 ASTM-P-0109-12 ASTM-P-0109-13 ASTM-P-0109-14 ASTM-P-0109-15 ASTM-P-0109-16 ASTM-P-0109-17 Ca (Wt.%) Cl (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.600 0.500 0.400 0.260 0.005 0.400 0.300 0.200 0.060 0.060 0.050 0.025 0.005 0.170 0.100 0.010 0.000 0.100 0.000 0.010 0.500 1.000 0.400 0.100 0.010 0.050 0.200 0.500 0.800 1.000 0.600 0.200 0.400 0.000 0.005 0.200 0.150 0.250 0.005 0.025 0.060 0.100 0.080 0.050 0.120 0.150 0.200 0.250 0.100 0.010 0.000 0.175 0.050 0.300 0.150 0.450 0.350 0.250 0.450 0.300 0.200 0.100 0.200 0.400 0.550 0.200 0.600 0.000 0.060 0.080 0.180 0.120 0.070 0.100 0.120 0.100 0.130 0.050 0.075 0.130 0.150 0.110 0.200 0.250 0.000 ed for Design 927-96 -4 D ASTM Lubricating Oil, Elements Wt.% (Nominal Value) listed below ASTM-P-0110-SET $ 2300 / 17 x 100 mL Cat. No. Ca (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.100 0.175 0.000 0.025 0.150 0.000 0.200 0.000 0.100 0.050 0.075 0.010 0.005 0.000 0.000 0.005 0.000 0.600 0.500 0.400 0.260 0.005 0.400 0.300 0.200 0.060 0.060 0.050 0.025 0.005 0.170 0.100 0.010 0.000 0.005 0.200 0.150 0.250 0.005 0.025 0.060 0.100 0.080 0.050 0.120 0.150 0.200 0.250 0.100 0.010 0.000 0.175 0.050 0.300 0.150 0.450 0.350 0.250 0.450 0.300 0.200 0.100 0.200 0.400 0.550 0.200 0.600 0.000 0.060 0.080 0.180 0.120 0.070 0.100 0.120 0.100 0.130 0.050 0.075 0.130 0.150 0.110 0.200 0.250 0.000 Lubricating Oil, Elements Wt.% (Nominal Value) listed below ASTM-P-0112-SET $ 2300 / 16 x 100 mL Cat. No. ASTM-P-0112-01 ASTM-P-0112-02 ASTM-P-0112-03 ASTM-P-0112-04 ASTM-P-0112-05 ASTM-P-0112-06 ASTM-P-0112-07 ASTM-P-0112-08 ASTM-P-0112-09 ASTM-P-0112-10 ASTM-P-0112-11 ASTM-P-0112-12 ASTM-P-0112-13 ASTM-P-0112-14 ASTM-P-0112-15 ASTM-P-0112-16 ASTM-P-0112-17 Ca (Wt.%) Mg (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.600 0.500 0.400 0.260 0.005 0.400 0.300 0.200 0.060 0.060 0.050 0.025 0.005 0.170 0.100 0.010 0.000 0.100 0.150 0.350 0.225 0.450 0.500 0.325 0.250 0.100 0.400 0.300 0.200 0.375 0.175 0.425 0.275 0.000 0.005 0.200 0.150 0.250 0.005 0.025 0.060 0.100 0.080 0.050 0.120 0.150 0.200 0.250 0.100 0.010 0.000 0.175 0.050 0.300 0.150 0.450 0.350 0.250 0.450 0.300 0.200 0.100 0.200 0.400 0.550 0.200 0.600 0.000 0.060 0.080 0.180 0.120 0.070 0.100 0.120 0.100 0.130 0.050 0.075 0.130 0.150 0.110 0.200 0.250 0.000 Lubricating Oil, Elements Wt.% (Nominal Value) listed below ASTM-P-0111-SET $ 2800 / 17 x 100 mL Cat. No. ASTM-P-0111-01 ASTM-P-0111-02 ASTM-P-0111-03 ASTM-P-0111-04 ASTM-P-0111-05 ASTM-P-0111-06 ASTM-P-0111-07 ASTM-P-0111-08 ASTM-P-0111-09 ASTM-P-0111-10 ASTM-P-0111-11 ASTM-P-0111-12 ASTM-P-0111-13 ASTM-P-0111-14 ASTM-P-0111-15 ASTM-P-0111-16 ASTM-P-0111-17 Ba (Wt.%) Ca (Wt.%) Cl (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.100 0.175 0.000 0.025 0.150 0.000 0.200 0.000 0.100 0.050 0.075 0.010 0.005 0.000 0.000 0.005 0.000 0.600 0.500 0.400 0.260 0.005 0.400 0.300 0.200 0.060 0.060 0.050 0.025 0.005 0.170 0.100 0.010 0.000 0.100 0.000 0.010 0.500 1.000 0.400 0.100 0.010 0.050 0.200 0.500 0.800 1.000 0.600 0.200 0.400 0.000 0.005 0.200 0.150 0.250 0.005 0.025 0.060 0.100 0.080 0.050 0.120 0.150 0.200 0.250 0.100 0.010 0.000 0.175 0.050 0.300 0.150 0.450 0.350 0.250 0.450 0.300 0.200 0.100 0.200 0.400 0.550 0.200 0.600 0.000 0.060 0.080 0.180 0.120 0.070 0.100 0.120 0.100 0.130 0.050 0.075 0.130 0.150 0.110 0.200 0.250 0.000 A S TM ed for Design & D-4927-96 -97 D-4628 Lubricating Oil, Elements Wt.% (Nominal Value) listed below ASTM-P-0113-SET $ 2850 / 17 x 100 mL Cat. No. ASTM-P-0113-01 ASTM-P-0113-02 ASTM-P-0113-03 ASTM-P-0113-04 ASTM-P-0113-05 ASTM-P-0113-06 ASTM-P-0113-07 ASTM-P-0113-08 ASTM-P-0113-09 ASTM-P-0113-10 ASTM-P-0113-11 ASTM-P-0113-12 ASTM-P-0113-13 ASTM-P-0113-14 ASTM-P-0113-15 ASTM-P-0113-16 ASTM-P-0113-17 Ba (Wt.%) Ca (Wt.%) Mg (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.025 0.000 0.100 0.175 0.150 0.000 0.100 0.200 0.050 0.075 0.010 0.000 0.175 0.005 0.000 0.005 0.000 0.600 0.500 0.400 0.260 0.005 0.400 0.300 0.200 0.060 0.060 0.050 0.025 0.005 0.170 0.100 0.010 0.000 0.100 0.150 0.350 0.225 0.450 0.500 0.325 0.250 0.100 0.400 0.300 0.200 0.375 0.175 0.425 0.275 0.000 0.005 0.200 0.150 0.250 0.005 0.025 0.060 0.100 0.080 0.050 0.120 0.150 0.200 0.250 0.100 0.010 0.000 0.175 0.050 0.300 0.150 0.450 0.350 0.250 0.450 0.300 0.200 0.100 0.200 0.400 0.550 0.200 0.600 0.000 0.060 0.080 0.180 0.120 0.070 0.100 0.120 0.100 0.130 0.050 0.075 0.130 0.150 0.110 0.200 0.250 0.000 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 63 ORGANOMETALLIC C ASTM-P-0110-01 ASTM-P-0110-02 ASTM-P-0110-03 ASTM-P-0110-04 ASTM-P-0110-05 ASTM-P-0110-06 ASTM-P-0110-07 ASTM-P-0110-08 ASTM-P-0110-09 ASTM-P-0110-10 ASTM-P-0110-11 ASTM-P-0110-12 ASTM-P-0110-13 ASTM-P-0110-14 ASTM-P-0110-15 ASTM-P-0110-16 ASTM-P-0110-17 Ba (Wt.%) ed for Design 927-96 -4 D ASTM WEAR METALS ASTM-P-0108-01 ASTM-P-0108-02 ASTM-P-0108-03 ASTM-P-0108-04 ASTM-P-0108-05 ASTM-P-0108-06 ASTM-P-0108-07 ASTM-P-0108-08 ASTM-P-0108-09 ASTM-P-0108-10 ASTM-P-0108-11 ASTM-P-0108-12 ASTM-P-0108-13 ASTM-P-0108-14 ASTM-P-0108-15 ASTM-P-0108-16 ASTM-P-0108-17 Ca (Wt.%) Organometallic Standards for Wear Metals AA, ICP, DCP & XRF Analysis Lubricating Oil Standards Continued ed for Design 481-99 D-6 M T S Lubricating Oil, Elements, EDXRF ASTM Method A Lubricating Oil, Elements Wt.% (Nominal Value) listed below Wt.% (Nominal Value) listed below ASTM-P-0115-SET $ 2300 / 17 x 100 mL ASTM-P-0114-SET $ 1900 / 17 x 100 mL ORGANOMETALLIC C WEAR METALS Cat. No. ASTM-P-0114-01 ASTM-P-0114-02 ASTM-P-0114-03 ASTM-P-0114-04 ASTM-P-0114-05 ASTM-P-0114-06 ASTM-P-0114-07 ASTM-P-0114-08 ASTM-P-0114-09 ASTM-P-0114-10 ASTM-P-0114-11 ASTM-P-0114-12 ASTM-P-0114-13 ASTM-P-0114-14 ASTM-P-0114-15 ASTM-P-0114-16 ASTM-P-0114-17 Ca (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.005 0.600 0.000 1.000 0.000 0.005 0.500 0.010 0.050 0.100 0.200 0.400 0.600 0.800 1.000 0.400 0.000 0.005 0.000 0.300 0.000 0.000 0.250 0.150 0.200 0.010 0.150 0.200 0.005 0.100 0.010 0.300 0.050 0.000 0.050 0.000 0.000 1.000 0.000 0.800 0.500 0.100 0.400 0.200 0.800 0.800 0.500 0.050 1.000 0.600 0.000 0.050 0.000 0.000 0.000 0.300 0.300 0.150 0.250 0.075 0.200 0.100 0.300 0.050 0.100 0.150 0.250 0.000 Cat. No. ASTM-P-0115-01 ASTM-P-0115-02 ASTM-P-0115-03 ASTM-P-0115-04 ASTM-P-0115-05 ASTM-P-0115-06 ASTM-P-0115-07 ASTM-P-0115-08 ASTM-P-0115-09 ASTM-P-0115-10 ASTM-P-0115-11 ASTM-P-0115-12 ASTM-P-0115-13 ASTM-P-0115-14 ASTM-P-0115-15 ASTM-P-0115-16 ASTM-P-0115-17 Ca (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) Mg (Wt.%) 0.005 0.600 0.000 1.000 0.000 0.005 0.500 0.010 0.050 0.100 0.200 0.400 0.600 0.800 1.000 0.400 0.000 0.005 0.000 0.300 0.000 0.000 0.250 0.150 0.200 0.010 0.150 0.200 0.005 0.100 0.010 0.300 0.050 0.000 0.050 0.000 0.000 1.000 0.000 0.800 0.500 0.100 0.400 0.200 0.800 0.800 0.500 0.050 1.000 0.600 0.000 0.050 0.000 0.000 0.000 0.300 0.300 0.150 0.250 0.075 0.200 0.100 0.300 0.050 0.100 .0150 0.250 0.000 0.100 0.150 0.350 .0225 0.450 0.500 0.325 0.250 0.050 0.400 0.300 0.200 0.375 0.175 0.425 0.275 0.000 Lubricating Oil, Additives Wt.% (Nominal Value) listed below ASTM-P-0116-SET $ 2450 / 11 x 100 mL Cat. No. ASTM-P-0116-01 ASTM-P-0116-02 ASTM-P-0116-03 ASTM-P-0116-04 ASTM-P-0116-05 ASTM-P-0116-06 ASTM-P-0116-07 ASTM-P-0116-08 ASTM-P-0116-09 ASTM-P-0116-10 ASTM-P-0116-11 Ca (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.500 3.000 2.000 5.000 4.000 2.500 4.000 0.500 1.000 2.500 0.000 1.000 1.000 1.250 1.500 0.500 0.750 0.500 2.000 0.750 1.200 0.000 0.500 3.000 1.000 0.500 1.500 4.000 2.000 5.000 2.000 3.000 0.000 0.500 2.000 1.500 1.200 0.750 1.000 1.250 1.000 1.500 0.500 0.000 Lubricating Oil, Elements, WLXRF ASTM Method Wt.% (Nominal Value) listed below ASTM-P-0117-SET $ 2100 / 10 x 100 mL Cat. No. ASTM-P-0117-01 ASTM-P-0117-02 ASTM-P-0117-03 ASTM-P-0117-04 ASTM-P-0117-05 ASTM-P-0117-06 ASTM-P-0117-07 ASTM-P-0117-08 ASTM-P-0117-09 ASTM-P-0117-10 Ca (Wt.%) Cl (Wt.%) Cu (Wt.%) Mg (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.020 0.020 0.020 0.020 0.400 0.400 0.400 0.400 0.200 0.000 0.030 0.020 0.200 0.200 0.020 0.020 0.200 0.200 0.100 0.000 0.010 0.050 0.010 0.050 0.010 0.050 0.010 0.050 0.025 0.000 0.200 0.200 0.040 0.040 0.040 0.040 0.200 0.200 0.080 0.000 0.250 0.020 0.250 0.020 0.020 0.250 0.020 0.250 0.150 0.000 1.000 0.020 0.150 1.000 1.000 0.020 0.020 1.000 0.500 0.000 0.020 0.250 0.250 0.020 0.250 0.020 0.050 0.250 0.100 0.000 ed for Design 443-99 -6 D M AST Lubricating Oil, Elements, WLXRF ASTM Method Wt.% (Nominal Value) listed below ASTM-P-0118-SET $ 2400 / 10 x 100 mL Cat. No. ASTM-P-0118-01 ASTM-P-0118-02 ASTM-P-0118-03 ASTM-P-0118-04 ASTM-P-0118-05 ASTM-P-0118-06 ASTM-P-0118-07 ASTM-P-0118-08 ASTM-P-0118-09 ASTM-P-0118-10 64 Ba (Wt.%) Ca (Wt.%) Cl (Wt.%) Cu (Wt.%) Mg (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.020 0.250 0.020 0.250 0.020 0.250 0.020 0.250 0.130 0.000 0.020 0.020 0.020 0.020 0.400 0.400 0.400 0.400 0.200 0.000 0.030 0.020 0.200 0.200 0.020 0.020 0.200 0.200 0.100 0.000 0.010 0.050 0.010 0.050 0.010 0.050 0.010 0.050 0.025 0.000 0.200 0.200 0.040 0.040 0.040 0.040 0.200 0.200 0.080 0.000 0.250 0.020 0.250 0.020 0.020 0.250 0.020 0.250 0.150 0.000 1.000 0.020 0.150 1.000 1.000 0.020 0.020 1.000 0.500 0.000 0.020 0.250 0.250 0.020 0.250 0.020 0.050 0.250 0.100 0.000 STM 6 for A ned -4927-9 g i s De -97, D 43-99 28 64 D-46 1-96, D5 9 4 D Quality System is Certified to comply with the International ISO 9001 Quality Standard Organometallic Standards for Wear Metals AA, ICP, DCP & XRF Analysis Lubricating Oil Standards Continued Lubricating Oil, Elements Wt.% (Nominal Value) listed below ASTM-P-0119-SET Cat. No. ASTM-P-0119-01 ASTM-P-0119-02 ASTM-P-0119-03 ASTM-P-0119-04 ASTM-P-0119-05 ASTM-P-0119-06 ASTM-P-0119-07 ASTM-P-0119-08 ASTM-P-0119-09 ASTM-P-0119-10 ASTM-P-0119-11 ASTM-P-0119-12 ASTM-P-0119-13 ASTM-P-0119-14 ASTM-P-0119-15 ASTM-P-0119-16 ASTM-P-0119-17 ASTM-P-0119-18 ASTM-P-0119-19 ASTM-P-0119-20 ASTM-P-0119-21 ASTM-P-0119-22 $ 2900 / 22 x 100 mL Ca (Wt.%) Cl (Wt.%) Cu (Wt.%) Mg (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.300 0.250 0.500 0.350 0.110 0.200 0.000 0.150 0.250 0.110 0.260 0.200 0.000 0.070 0.050 0.400 0.180 0.400 0.010 0.050 0.200 0.000 0.080 0.100 0.000 0.010 0.000 0.100 0.050 0.030 0.150 0.150 0.050 0.000 0.000 0.150 0.000 0.000 0.020 0.010 0.020 0.005 0.050 0.000 0.030 0.000 0.035 0.000 0.015 0.000 0.025 0.000 0.010 0.040 0.000 0.005 0.005 0.020 0.000 0.001 0.020 0.001 0.040 0.050 0.020 0.000 0.060 0.010 0.160 0.120 0.100 0.200 0.000 0.100 0.160 0.005 0.000 0.140 0.020 0.080 0.000 0.080 0.000 0.010 0.010 0.000 0.080 0.000 0.060 0.150 0.150 0.080 0.100 0.050 0.000 0.030 0.000 0.030 0.000 0.080 0.020 0.140 0.150 0.000 0.020 0.020 0.020 0.008 0.050 0.000 0.275 0.000 0.000 0.200 0.300 0.250 0.450 0.400 0.350 0.750 0.750 0.500 0.200 0.650 0.000 0.500 0.600 0.000 0.200 0.000 0.275 0.000 0.060 0.150 0.020 0.000 0.050 0.150 0.020 0.040 0.080 0.150 0.000 0.080 0.020 0.150 0.000 0.020 0.060 0.000 0.100 0.120 0.050 0.000 Lubricating Oil, Elements Wt.% (Nominal Value) listed below ASTM-P-0120-SET Cat. No. $ 3100 / 23 x 100 mL Ca (Wt.%) Cl (Wt.%) Cu (Wt.%) Mg (Wt.%) P (Wt.%) S (Wt.%) Zn (Wt.%) 0.100 0.175 0.040 0.020 0.150 0.000 0.200 0.000 0.000 0.000 0.100 0.050 0.000 0.080 0.010 0.000 0.000 0.000 0.150 0.005 0.100 0.120 0.000 0.300 0.250 0.500 0.350 0.110 0.200 0.000 0.150 0.250 0.110 0.260 0.200 0.000 0.070 0.050 0.400 0.180 0.400 0.010 0.050 0.200 0.200 0.000 0.080 0.100 0.000 0.010 0.000 0.100 0.050 0.030 0.150 0.150 0.050 0.000 0.000 0.150 0.000 0.000 0.020 0.010 0.020 0.005 0.050 0.000 0.000 0.030 0.000 0.035 0.000 0.015 0.000 0.025 0.000 0.010 0.040 0.000 0.005 0.005 0.020 0.000 0.001 0.020 0.001 0.040 0.050 0.020 0.000 0.000 0.060 0.010 0.160 0.120 0.100 0.200 0.000 0.100 0.160 0.005 0.000 0.140 0.020 0.080 0.000 0.080 0.000 0.010 0.010 0.000 0.080 0.000 0.000 0.060 0.150 0.150 0.080 0.100 0.050 0.000 0.030 0.000 0.030 0.000 0.080 0.020 0.140 0.150 0.000 0.020 0.020 0.020 0.008 0.050 0.000 0.000 0.275 0.000 0.000 0.200 0.300 0.250 0.450 0.400 0.350 0.750 0.750 0.500 0.200 0.650 0.000 0.500 0.600 0.000 0.200 0.000 0.275 0.750 0.000 0.060 0.150 0.020 0.000 0.050 0.150 0.020 0.040 0.080 0.150 0.000 0.080 0.020 0.150 0.000 0.020 0.060 0.000 0.100 0.120 0.050 0.000 0.000 Stabilization Solutions Metal Working Fluid Wt.% (Nominal Value) listed below ASTM-P-0121-SET $ 1300 / 13 x 100 mL ASTM-P-0121-01 ASTM-P-0121-02 ASTM-P-0121-03 ASTM-P-0121-04 ASTM-P-0121-05 ASTM-P-0121-06 ASTM-P-0121-07 ASTM-P-0121-08 ASTM-P-0121-09 ASTM-P-0121-10 ASTM-P-0121-11 ASTM-P-0121-12 ASTM-P-0121-13 Concentration for the sets on pages 62-65 are targets. Actual production lots may vary. Ba (Wt.%) Metal Working Fluids Standard No. Technical Note ORGANOMETALLIC C ASTM-P-0120-01 ASTM-P-0120-02 ASTM-P-0120-03 ASTM-P-0120-04 ASTM-P-0120-05 ASTM-P-0120-06 ASTM-P-0120-07 ASTM-P-0120-08 ASTM-P-0120-09 ASTM-P-0120-10 ASTM-P-0120-11 ASTM-P-0120-12 ASTM-P-0120-13 ASTM-P-0120-14 ASTM-P-0120-15 ASTM-P-0120-16 ASTM-P-0120-17 ASTM-P-0120-18 ASTM-P-0120-19 ASTM-P-0120-20 ASTM-P-0120-21 ASTM-P-0120-22 ASTM-P-0120-23 TM r AS ed fo 927-96 n g i Des 97, D-4 -99 28443 D-46 -96, D-6 1 5 D-49 Cl (Wt.%) P (Wt.%) S (Wt.%) 0.000 0.750 0.050 1.000 0.100 1.500 2.000 1.000 0.500 2.000 0.000 1.250 0.050 0.000 0.025 0.100 0.500 0.005 0.200 0.005 0.050 0.400 0.200 0.500 0.010 0.300 0.000 0.500 3.000 2.500 2.000 1.000 3.000 0.100 0.000 1.500 1.500 0.050 0.050 The solutions were specifically designed for chelating and solubilizing the organometallic line of solids and solutions for single and multi-element standards. Stabilizer Solutions A ASTM-P-0122-0.5 ASTM-P-0122-1 $ 80 / 50 mL $ 120 / 100 mL Stabilizer Solutions B ASTM-P-0123-0.5 $ 80 / 50 mL ASTM-P-0123-1 $ 120 / 100 mL (use in conjunction with stabilizer solution A) Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 65 Petrochemical Standards Wear Metals Proposed ASTM Method Trace Metals ASTM-P-0090-SET Phosphorous, Sulfur, Calcium, & Zinc in Lubrication Oils by XRF $ 1600 / 16 x 4 oz. Cat. No. Calcium Wt.% Phosphorus Wt.% Sulfur Wt.% Zinc Wt.% Unit Price ASTM-P-0090-01 ASTM-P-0090-02 ASTM-P-0090-03 ASTM-P-0090-04 ASTM-P-0090-05 ASTM-P-0090-06 ASTM-P-0090-07 ASTM-P-0090-08 ASTM-P-0090-09 ASTM-P-0090-10 ASTM-P-0090-11 ASTM-P-0090-12 ASTM-P-0090-13 ASTM-P-0090-14 ASTM-P-0090-15 ASTM-P-0090-16 0 0 0.005 0.025 0.05 0.075 0.1 0.1 0.15 0.2 0.25 0.3 0.35 0.4 0.5 0.6 0 0.02 0 0.175 0.15 0.225 0.01 0.125 0.1 0.008 0.05 0.06 0.004 0.2 0.03 0.005 0 0.3 0.55 0.35 0.2 0.5 0.45 0.6 0.25 0.075 0.125 0.1 0.4 0.175 0.15 0.05 0 0.175 0.14 0.1 0.2 0.15 0.25 0.06 0.089 0.12 0 0.13 0.11 0.05 0.07 0.08 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 4 $ 200 200 200 200 200 200 200 200 200 200 200 200 200 200 200 200 oz. oz. oz. oz. oz. oz. oz. oz. oz. oz. oz. oz. oz. oz. oz. oz. Proposed ASTM Method for Chlorine in Lube Oils Chlorine in Lube Oils ORGANOMETALLIC C ASTM-P-0092-SET $ 400 / 7 x 4 oz. Cat. No. Chlorine Wt. % Chlorine µg/g Unit ASTM-P-0092-BL ASTM-P-0092-0.1X ASTM-P-0092-1X ASTM-P-0092-5X ASTM-P-0092-10X ASTM-P-0092-100X ASTM-P-0092-500X Blank 0.001 0.01 0.05 0.1 1 5 Blank 10 100 500 1,000 10,000 50,000 4 4 4 4 4 4 4 oz. oz. oz. oz. oz. oz. oz. Price $ 10 75 75 75 75 75 75 The Organo Tin standards shown below were developed in response to concerns about Organo Tin as an endocrine disrupter. Organo Tin compounds such as Tributyl Tin were used as marine antifouling agents and Triphenyl Tin as a crop pesticide. Organo Tin Analysis Sample Extraction, Derivatization & Cleanup with Analysis by Flame-Photometric Detector Butyltin Chloride Standard OMT-001 $ 40 / 1 x 1 mL OMT-001-PAK SAVE 20% $ 160 / 5 x 1 mL 2000 µg/mL each in CH2Cl2 4 comps. Butyltin trichloride Dibutyltin dichloride Tetrabutyltin Tributyltin chloride Phenyltin Chloride Standard OMT-002 $ 40 / 1 x 1 mL OMT-002-PAK SAVE 20% $ 160 / 5 x 1 mL 2000 µg/mL each in CH2Cl2 4 comps. Diphenyltin dichloride Phenyltin trichloride 66 Tetraphenyltin Triphenyltin chloride Tri-n-propyltin Chloride Surrogate Standard Tetra-n-propyltin chloride Internal Standard OMT-003 $ 30 / 1 x 1 mL OMT-003-PAK SAVE 20% $ 120 / 5 x 1 mL 2000 µg/mL in CH2Cl2 OMT-005 $ 40 / 1 x 1 mL OMT-005-PAK SAVE 20% $ 160 / 5 x 1 mL 2000 µg/mL in CH2Cl2 Tri-n-propyltin chloride Tetra-n-propyl tin chloride Tripentyltin Chloride Surrogate Standard Tetrapentyltin Chloride Internal Standard OMT-004 $ 30 / 1 x 1 mL OMT-004-PAK SAVE 20% $ 120 / 5 x 1 mL 2000 µg/mL in CH2Cl2 OMT-006 $ 30 / 1 x 1 mL OMT-006-PAK SAVE 20% $ 120 / 5 x 1 mL 2000 µg/mL in CH2Cl2 Tripentyltin chloride Tetrapentyltin chloride Quality System is Certified to comply with the International ISO 9001 Quality Standard Inorganic Standards INO ICP, ICP/MS, AA, Ion Chrom Used for influent and effluent monitoring in aqueous matrices by ASTM and other EPA Methods in the Petrochemical Industry. • • • • • • Formulated from High Purity Starting Materials, Water & Acids Concentration verified by Wet Chemical & Instrumental Analysis Certificate of Analysis provided with each Standard Actual Lot Analysis provided on label & Certificate of Analysis Packaged in specially prepared pre-cleaned bottles 18 Month Stability Dating Inorganic Petrochemical Reference Standards ICP IPC/MS AA Ion Chrom page 68-71 72 73-75 76-79 Traceable to NIST Reference Materials Stop Paying Hazardous Shipping Fees! AccuNoHaz Empty Pre-Washed 500 mL Bottle ICP HAZ FEE 20 mL Concentrate 69 elements at 10K µg/mL & 59 elements at 25K µg/mL see pages 68-71 AA 69 elements at 10K µg/mL & 59 elements at 25K µg/mL see pages 73-75 20 mL meets the Excepted Quantity rule under DOT & IATA regulations which do not require hazardous shipping fees. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 67 INORGANIC All NoHaz products come as kits including 20 mL of concentrate, pre-cleaned and prelabeled dilution bottle, instructions and Certificate of Analysis ICP Single Element Standards Plasma Emission Spectroscopy NoHaz Package (No Hazardous Charges) * 10,000 µg/mL 25,000 µg/mL Element Starting Mat'l Matrix Aluminum Al(NO3)3 • 9H2O 2-5% Nitric acid Antimony Sb 2-5% Nitric acid Arsenic As 2-5% Nitric acid Barium Ba(NO3)2 2-5% Nitric acid Beryllium BeO(C2H3O2)6 2-5% Nitric acid Bismuth Bi 2-5% Nitric acid Boron H3BO3 Water tr. NH4OH Cadmium Cd 2-5% Nitric acid Calcium CaCO3 2-5% Nitric acid Cerium Ce(NO3)3 2-5% Nitric acid ICP Cesium CsNO3 2-5% Nitric acid Chromium reduced to (+3) state (NH4)2Cr2O7 2-5% Nitric acid Chromium reduced to (+3) state Cr 2-5% Nitric acid Cobalt Co 2-5% Nitric acid Copper Cu 2-5% Nitric acid Dysprosium Dy2O3 2-5% Nitric acid Erbium Er2O3 2-5% Nitric acid Europium Eu2O3 2-5% Nitric acid Gadolinium Gd2O3 2-5% Nitric acid 68 1000 µg/mL Unit Cat. No. 10,000 µg/mL Price 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 50 100 500 mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL ----------ICP-01N-1 ICP-01N-5 ----------ICP-02N-1 ICP-02N-5 ----------ICP-03N-1 ICP-03N-5 ----------ICP-04N-1 ICP-04N-5 ----------ICP-05N-1 ICP-05N-5 ----------ICP-06N-1 ICP-06N-5 ----------ICP-07W-1 ICP-07W-5 ----------ICP-08N-1 ICP-08N-5 ----------ICP-09N-1 ICP-09N-5 ----------ICP-11N-1 ICP-11N-5 ----------ICP-12N-1 ICP-12N-5 ----------ICP-13N-1 ICP-13N-5 -------------ICP-13H-1 ICP-13H-5 --$ 34 67 --34 67 --34 67 --34 67 --34 67 --34 67 --34 67 --34 67 --34 67 --34 67 --42 82 --34 67 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL ----------ICP-14N-1 ICP-14N-5 ----------ICP-15N-1 ICP-15N-5 ----------ICP-16N-1 ICP-16N-5 ----------ICP-17N-1 ICP-17N-5 ----------ICP-18N-1 ICP-18N-5 ----------ICP-19N-1 ICP-19N-5 Cat. No. Price Cat. No. Price Cat. No. Price 34 67 -----ICP-01N-0.5-10X ICP-01N-1-10X ICP-01N-5-10X -----ICP-02N-0.5-10X ICP-02N-1-10X ICP-02N-5-10X -----ICP-03N-0.5-10X ICP-03N-1-10X ICP-03N-5-10X -----ICP-04N-0.5-10X ICP-04N-1-10X ICP-04N-5-10X -----ICP-05N-0.5-10X ICP-05N-1-10X ICP-05N-5-10X -----ICP-06N-0.5-10X ICP-06N-1-10X ICP-06N-5-10X -----ICP-07W-0.5-10X ICP-07W-1-10X ICP-07W-5-10X -----ICP-08N-0.5-10X ICP-08N-1-10X ICP-08N-5-10X -----ICP-09N-0.5-10X ICP-09N-1-10X ICP-09N-5-10X -----ICP-11N-0.5-10X ICP-11N-1-10X ICP-11N-5-10X -----ICP-12N-0.5-10X ICP-12N-1-10X ICP-12N-5-10X -----ICP-13N-0.5-10X ICP-13N-1-10X ICP-13N-5-10X ICP-13H-0.5-10X ICP-13H-1-10X ICP-13H-5-10X -$ 34 59 175 -36 65 135 -32 54 120 -32 54 120 -32 54 240 -36 65 135 -32 54 120 -32 54 120 -32 54 120 -32 54 168 -45 75 231 -34 59 125 34 59 125 ICP-01N-10X-20ML ---------------ICP-02N-10X-20ML ---------------ICP-03N-10X-20ML ---------------ICP-04N-10X-20ML ---------------ICP-05N-10X-20ML ---------------ICP-06N-10X-20ML ---------------ICP-07W-10X-20ML ---------------ICP-08N-10X-20ML ---------------ICP-09N-10X-20ML ---------------ICP-11N-10X-20ML ---------------ICP-12N-10X-20ML ---------------ICP-13N-10X-20ML ---------------ICP-13H-0.5-10X ----------- $ 37 ---37 ---37 ---37 ---37 ---37 ---37 ---37 ---37 ---37 ---55 ---37 ---34 --- ICP-01N-25X-20ML -----------------------------------ICP-03N-25X-20ML ---------------ICP-04N-25X-20ML -----------------------------------ICP-06N-25X-20ML -----------------------------------ICP-08N-25X-20ML ---------------ICP-09N-25X-20ML ---------------ICP-11N-25X-20ML ---------------ICP-12N-25X-20ML ---------------ICP-13N-25X-20ML ------------------------------- $ 70 -------70 ---70 -------70 -------70 ---70 ---80 ---100 ---70 ------- --34 67 --34 67 --42 82 --42 82 --42 82 --42 82 -----ICP-14N-0.5-10X ICP-14N-1-10X ICP-14N-5-10X -----ICP-15N-0.5-10X ICP-15N-1-10X ICP-15N-5-10X -----ICP-16N-0.5-10X ICP-16N-1-10X ICP-16N-5-10X -----ICP-17N-0.5-10X ICP-17N-1-10X ICP-17N-5-10X -----ICP-18N-0.5-10X ICP-18N-1-10X ICP-18N-5-10X -----ICP-19N-0.5-10X ICP-19N-1-10X ICP-19N-5-10X -32 54 168 -32 54 120 -45 75 231 -52 85 259 -52 85 185 -69 115 315 ICP-14N-10X-20ML ---------------ICP-15N-10X-20ML ---------------ICP-16N-10X-20ML ---------------ICP-17N-10X-20ML ---------------ICP-18N-10X-20ML ---------------ICP-19N-10X-20ML ---------------- 37 ---37 ---55 ---55 ---55 ---55 ---- ICP-14N-25X-20ML ---------------ICP-15N-25X-20ML ---------------ICP-16N-25X-20ML ---------------ICP-17N-25X-20ML ---------------ICP-18N-25X-20ML ---------------ICP-19N-25X-20ML ---------------- 70 ---70 ---100 ---100 ---100 ---100 ---- Quality System is Certified to comply with the International ISO 9001 Quality Standard ICP Single Element Standards Plasma Emission Spectroscopy NoHaz Package (No Hazardous Charges) * 10,000 µg/mL 25,000 µg/mL Element Starting Mat'l Matrix Gallium Ga 2-5% Nitric acid 1000 µg/mL Unit mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL Cat. No. ----------ICP-20N-1 ICP-20N-5 ----------ICP-21W-1 ICP-21W-5 ----------ICP-22H-1 ICP-22H-5 ----------ICP-23N-1 ICP-23N-5 ----------ICP-24N-1 ICP-24N-5 ----------ICP-25N-1 ICP-25N-5 ----------ICP-26H-1 ICP-26H-5 ----------ICP-27N-1 ICP-27N-5 ----------ICP-28N-1 ICP-28N-5 ----------ICP-29N-1 ICP-29N-5 ----------ICP-30N-1 ICP-30N-5 ----------ICP-31N-1 ICP-31N-5 ----------ICP-32N-1 ICP-32N-5 ----------ICP-33N-1 ICP-33N-5 ----------ICP-34N-1 ICP-34N-5 ----------ICP-35W-1 ICP-35W-5 ----------ICP-36N-1 ICP-36N-5 ----------ICP-37N-1 ICP-37N-5 * see page 67 for details Price --$ 42 82 --42 82 --78 152 --60 118 --42 82 --42 82 --78 152 --34 67 --34 67 --34 67 --34 67 --75 285 --34 67 --34 67 --34 67 --34 67 --34 67 --34 67 Cat. No. Price -----ICP-20N-0.5-10X ICP-20N-1-10X ICP-20N-5-10X -----ICP-21W-0.5-10X ICP-21W-1-10X ICP-21W-5-10X -----ICP-22H-0.5-10X ICP-22H-1-10X ICP-22H-5-10X -----ICP-23N-0.5-10X ICP-23N-1-10X ICP-23N-5-10X -----ICP-24N-0.5-10X ICP-24N-1-10X ICP-24N-5-10X -----ICP-25N-0.5-10X ICP-25N-1-10X ICP-25N-5-10X -----ICP-26H-0.5-10X ICP-26H-1-10X ICP-26H-5-10X -----ICP-27N-0.5-10X ICP-27N-1-10X ICP-27N-5-10X -----ICP-28N-0.5-10X ICP-28N-1-10X ICP-28N-5-10X -----ICP-29N-0.5-10X ICP-29N-1-10X ICP-29N-5-10X -----ICP-30N-0.5-10X ICP-30N-1-10X ICP-30N-5-10X -----ICP-31N-0.5-10X ICP-31N-1-10X ICP-31N-5-10X -----ICP-32N-0.5-10X ICP-32N-1-10X ICP-32N-5-10X -----ICP-33N-0.5-10X ICP-33N-1-10X ICP-33N-5-10X -----ICP-34N-0.5-10X ICP-34N-1-10X ICP-34N-5-10X -----ICP-35W-0.5-10X ICP-35W-1-10X ICP-35W-5-10 -----ICP-36N-0.5-10X ICP-36N-1-10X ICP-36N-5-10X -----ICP-37N-0.5-10X ICP-37N-1-10X ICP-37N-5-10X -$ 45 75 165 -52 85 231 -175 295 695 -80 135 364 -52 85 259 -52 85 185 -175 295 695 -32 54 120 -32 54 168 -32 54 168 -32 54 120 -175 295 1393 -32 54 120 -32 54 168 -32 54 120 -32 54 120 -45 75 203 -32 54 120 Cat. No. ICP-20N-10X-20ML ---------------ICP-21W-10X-20ML ---------------ICP-22H-10X-20ML ---------------ICP-23N-10X-20ML ---------------ICP-24N-10X-20ML ---------------ICP-25N-10X-20ML ---------------ICP-26H-10X-20ML ---------------ICP-27N-10X-20ML ---------------ICP-28N-10X-20ML ---------------ICP-29N-10X-20ML ---------------ICP-30N-10X-20ML ---------------ICP-31N-10X-20ML ---------------ICP-32N-10X-20ML ---------------ICP-33N-10X-20ML ---------------ICP-34N-10X-20ML ---------------ICP-35W-10X-20ML ---------------ICP-36N-10X-20ML ---------------ICP-37N-10X-20ML ---------------- Price $ 55 ---55 ---95 ---75 ---55 ---55 ---95 ---37 ---37 ---37 ---37 ---90 ---37 ---37 ---37 ---37 ---37 ---37 ---- Cat. No. ----------------------------------------ICP-22H-25X-20ML ---------------ICP-23N-25X-20ML ---------------ICP-24N-25X-20ML ---------------ICP-25N-25X-20ML ---------------ICP-26H-25X-20ML ---------------ICP-27N-25X-20ML ---------------ICP-28N-25X-20ML ---------------ICP-29N-25X-20ML ---------------ICP-30N-25X-20ML ---------------ICP-31N-25X-20ML ---------------ICP-32N-25X-20ML ---------------ICP-33N-25X-20ML ---------------ICP-34N-25X-20ML ---------------ICP-35W-25X-20ML ---------------ICP-36N-25X-20ML ---------------ICP-37N-25X-20ML ---------------- Price --------$ 165 ---135 ---100 ---100 ---175 ---70 ---80 ---70 ---70 ---300 ---70 ---70 ---70 ---70 ---80 ---70 ---- Single Element Standards for Plasma Emission Spectroscopy Continued on Next Page Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 69 ICP 20 50 100 500 Germanium 20 50 (NH4)2GeF6 Water tr. HF 100 500 Gold 20 Au 50 10% HCl (min.) 100 500 Hafnium 20 50 HfO2 2-5% Nitric acid tr. HF 100 500 Holmium 20 50 Ho2O3 2-5% Nitric acid 100 500 Indium 20 In 50 2-5% Nitric acid 100 500 Iridium 20 50 IrCl3 • 3H20 10% HCl (min.) 100 500 Iron 20 Fe 50 2-5% Nitric acid 100 500 Lanthanum 20 50 La2O3 2-5% Nitric acid 100 500 Lead 20 Pb(NO3)2 50 2-5% Nitric acid 100 500 Lithium 20 50 Li2CO3 2-5% Nitric acid 100 500 Lutetium 20 50 Lu2O3 2-5% Nitric acid 100 500 Magnesium 20 MgO 50 2-5% Nitric acid 100 500 Manganese 20 50 Mn(C2H3O2)2 2-5% Nitric acid 100 500 Mercury 20 Hg 50 10% Nitric acid 100 500 Molybdenum 20 50 (NH4)2MoO4 100 Water tr. NH4OH 500 Neodymium 20 50 Nd2O3 2-5% Nitric acid 100 500 Nickel 20 Ni 50 2-5% Nitric acid 100 500 10,000 µg/mL ICP Single Element Standards Plasma Emission Spectoscopy NoHaz Package (No Hazardous Charges) * 10,000 µg/mL 25,000 µg/mL Element Starting Mat'l Matrix Niobium Nb2O5 Water tr. HF Palladium Pd 10% HCl (min.) Phosphorus NH4H2PO4 Water Platinum Pt 10% HCl (min.) Potassium KNO3 2-5% Nitric acid Praseodymium Pr6O11 2-5% Nitric acid Rhenium Re Water Rhodium RhCl3 • 3H2O 10% HCl (min.) Rubidium RbNO3 2-5% Nitric acid Ruthenium RuCl3 • 3H2O 10% HCl Samarium Sm2O3 2-5% Nitric acid ICP Scandium Sc2O3 2-5% Nitric acid Selenium Se 2-5% Nitric acid Silicon (NH4)2SiF6 Water tr. HF Silver AgNO3 2-5% Nitric acid Sodium NaNO3 2-5% Nitric acid Strontium Sr(NO3)2 2-5% Nitric acid Sulfur (NH4)2SO4 Water Tantalum Ta Water tr. HF 70 1000 µg/mL Unit 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL Cat. No. ----------ICP-38W-1 ICP-38W-5 ----------ICP-40H-1 ICP-40H-5 ----------ICP-41W-1 ICP-41W-5 ----------ICP-42H-1 ICP-42H-5 ----------ICP-43N-1 ICP-43N-5 ----------ICP-44N-1 ICP-44N-5 ----------ICP-45W-1 ICP-45W-5 ----------ICP-46H-1 ICP-46H-5 ----------ICP-47N-1 ICP-47N-5 ----------ICP-48H-1 ICP-48H-5 ----------ICP-49N-1 ICP-49N-5 ----------ICP-50N-1 ICP-50N-5 ----------ICP-51N-1 ICP-51N-5 ----------ICP-52W-1 ICP-52W-5 ----------ICP-53N-1 ICP-53N-5 ----------ICP-54N-1 ICP-54N-5 ----------ICP-55N-1 ICP-55N-5 ----------ICP-56W-1 ICP-56W-5 ----------ICP-57W-1 ICP-57W-5 Price --$ 34 67 --78 152 --34 67 --78 152 --34 67 --42 82 --78 152 --190 425 --36 70 --78 152 --42 82 --78 152 --34 67 --34 67 --34 67 --34 67 --34 67 --34 67 --42 82 10,000 µg/mL Cat. No. Price -----ICP-38W-0.5-10X ICP-38W-1-10X ICP-38W-5-10X -----ICP-40H-0.5-10X ICP-40H-1-10X ICP-40H-5-10X -----ICP-41W-0.5-10X ICP-41W-1-10X ICP-41W-5-10X -----ICP-42H-0.5-10X ICP-42H-1-10X ICP-42H-5-10X -----ICP-43N-0.5-10X ICP-43N-1-10X ICP-43N-5-10X -----ICP-44N-0.5-10X ICP-44N-1-10X ICP-44N-5-10X -----ICP-45W-0.5-10X ICP-45W-1-10X ICP-45W-5-10X -----ICP-46H-0.5-10X ICP-46H-1-10X ICP-46H-5-10X -----ICP-47N-0.5-10X ICP-47N-1-10X ICP-47N-5-10X -----ICP-48H-0.5-10X ICP-48H-1-10X ICP-48H-5-10X -----ICP-49N-0.5-10X ICP-49N-1-10X ICP-49N-5-10X -----ICP-50N-0.5-10X ICP-50N-1-10X ICP-50N-5-10X -----ICP-51N-0.5-10X ICP-51N-1-10X ICP-51N-5-10X -----ICP-52W-0.5-10X ICP-52W-1-10X ICP-52W-5-10X -----ICP-53N-0.5-10X ICP-53N-1-10X ICP-53N-5-10X -----ICP-54N-0.5-10X ICP-54N-1-10X ICP-54N-5-10X -----ICP-55N-0.5-10X ICP-55N-1-10X ICP-55N-5-10X -----ICP-56W-0.5-10X ICP-56W-1-10X ICP-56W-5-10X -----ICP-57W-0.5-10X ICP-57W-1-10X ICP-57W-5-10X -$ 38 64 175 -175 295 973 -32 54 120 -175 295 695 -32 54 120 -72 120 329 -175 295 695 -315 525 2050 -52 85 175 -175 295 695 -45 75 231 -175 295 973 -32 54 120 -32 54 168 -42 70 145 -34 59 175 -42 70 203 -32 54 120 -52 85 224 Cat. No. ICP-38W-10X-20ML ---------------ICP-40H-10X-20ML ---------------ICP-41W-10X-20ML ---------------ICP-42H-10X-20ML ---------------ICP-43N-10X-20ML ---------------ICP-44N-10X-20ML ---------------ICP-45W-10X-20ML ---------------ICP-46H-10X-20ML ---------------ICP-47N-10X-20ML ---------------ICP-48H-10X-20ML ---------------ICP-49N-10X-20ML ---------------ICP-50N-10X-20ML ---------------ICP-51N-10X-20ML ---------------ICP-52W-10X-20ML ---------------ICP-53N-10X-20ML ---------------ICP-54N-10X-20ML ---------------ICP-55N-10X-20ML ---------------ICP-56W-10X-20ML ---------------ICP-57W-10X-20ML ---------------- Price $ 37 ---95 ---37 ---95 ---37 ---55 ---95 ---250 ---37 ---95 ---55 ---95 ---37 ---37 ---37 ---37 ---37 ---37 ---55 ---- Cat. No. ICP-38W-25X-20ML ---------------ICP-40H-25X-20ML -----------------------------------ICP-42H-25X-20ML ---------------ICP-43N-25X-20ML ---------------ICP-44N-25X-20ML ---------------ICP-45W-25X-20ML ---------------ICP-46H-25X-20ML ---------------ICP-47N-25X-20ML ---------------ICP-48H-25X-20ML ---------------ICP-49N-25X-20ML ---------------ICP-50N-25X-20ML ---------------ICP-51N-25X-20ML -----------------------------------ICP-53N-25X-20ML ---------------ICP-54N-25X-20ML ---------------ICP-55N-25X-20ML ---------------ICP-56W-25X-20ML ---------------ICP-57W-25X-20ML ---------------- Quality System is Certified to comply with the International ISO 9001 Quality Standard Price $ 80 ---165 -------165 ---70 ---100 ---175 ---475 ---80 ---185 ---100 ---175 ---70 -------70 ---70 ---70 ---70 ---100 ---- ICP Single Element Standards Plasma Emission Spectroscopy NoHaz Package (No Hazardous Charges) * 10,000 µg/mL 25,000 µg/mL Element 1000 µg/mL Starting Mat'l Matrix Unit Tellurium Te 10% HCl (min.) Cat. No. 10,000 µg/mL Price Cat. No. Price Cat. No. Price Cat. No. Price 20 50 100 500 20 50 100 500 20 50 100 500 100 500 mL mL mL mL mL mL mL mL mL mL mL mL mL mL ----------ICP-58H-1 ICP-58H-5 ----------ICP-59N-1 ICP-59N-5 ----------ICP-60N-1 ICP-60N-5 ICP-61N-1 ICP-61N-5 --$ 34 67 --42 82 --34 67 34 67 -----ICP-58H-0.5-10X ICP-58H-1-10X ICP-58H-5-10X -----ICP-59N-0.5-10X ICP-59N-1-10X ICP-59N-5-10X -----ICP-60N-0.5-10X ICP-60N-1-10X ICP-60N-5-10X ----------- -$ 46 78 210 -69 115 315 -32 54 125 --- ICP-58H-10X-20ML ---------------ICP-59N-10X-20ML ---------------ICP-60N-10X-20ML -------------------------- $ 37 ---55 ---37 ------ --------------------ICP-59N-25X-20ML ---------------ICP-60N-25X-20ML -------------------------- ----$ 100 ---70 ------ 20 50 100 500 mL mL mL mL ----------ICP-62N-1 ICP-62N-5 --58 120 Tin Sn 50 2-5% Nitric acid tr. HF 100 500 Tin 50 Sn 100 HCl 500 mL mL mL mL mL mL -------------ICP-63N-1 ICP-63N-5 -------------ICP-63H-1 ICP-63H-5 34 67 -----ICP-62N-0.5-10X ICP-62N-1-10X ICP-62N-5-10X -----ICP-63N-0.5-10X ICP-63N-1-10X ICP-63N-5-10X -----ICP-63H-1-10X ICP-63H-5-10X -78 130 250 -42 70 135 -70 135 ICP-62N-10X-20ML ---------------ICP-63N-10X-20ML ---------------ICP-63H-0.5-10X ----------- 75 ---37 ---42 --- ICP-62N-25X-20ML ---------------ICP-63N-25X-20ML ------------------------------- 135 ---70 ------- 20 50 100 500 20 50 100 500 50 100 500 mL mL mL mL mL mL mL mL mL mL mL ----------ICP-64W-1 ICP-64W-5 ----------ICP-65W-1 ICP-65W-5 -----ICP-66N-1 ICP-66N-5 --34 67 --34 67 -42 82 -----ICP-64W-0.5-10X ICP-64W-1-10X ICP-64W-5-10X -----ICP-65W-0.5-10X ICP-65W-1-10X ICP-65W-5-10X ---------------- -32 54 120 -32 54 168 ---- ICP-64W-10X-20ML ---------------ICP-65W-10X-20ML ------------------------------- 37 ---37 ------- -------------------------------------------------------- 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 20 50 100 500 mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL ----------ICP-67N-1 ICP-67N-5 ----------ICP-68N-1 ICP-68N-5 ----------ICP-69N-1 ICP-69N-5 ----------ICP-70N-1 ICP-70N-5 ----------ICP-71N-1 ICP-71N-5 --34 67 --42 82 --34 67 --34 67 --34 67 -----ICP-67N-0.5-10X ICP-67N-1-10X ICP-67N-5-10X -----ICP-68N-0.5-10X ICP-68N-1-10X ICP-68N-5-10X -----ICP-69N-0.5-10X ICP-69N-1-10X ICP-69N-5-10X -----ICP-70N-0.5-10X ICP-70N-1-10X ICP-70N-5-10X -----ICP-71N-0.5-10X ICP-71N-1-10X ICP-71N-5-10X -36 65 135 -60 100 273 -32 54 120 -32 54 120 -42 70 203 ICP-67N-10X-20ML ---------------ICP-68N-10X-20ML ---------------ICP-69N-10X-20ML ---------------ICP-70N-10X-20ML ---------------ICP-71N-10X-20ML ---------------- 37 ---55 ---37 ---37 ---37 ---- ICP-67N-25X-20ML ---------------ICP-68N-25X-20ML ---------------ICP-69N-25X-20ML ---------------ICP-70N-25X-20ML ---------------ICP-71N-25X-20ML ---------------- Terbium Tb4O7 2-5% Nitric acid Thallium Tl 2-5% Nitric acid Thorium Th(NO3)4 • 4H2O 2-5% Nitric acid Thulium Tm2O3 2-5% Nitric acid Titanium (NH4)2TiF6 Water tr. HF Tungsten (NH4)2WO4 Water tr. NH4OH Uranium U3O8 Vanadium NH4VO3 2-5% Nitric acid Ytterbium Yb2O3 2-5% Nitric acid Zinc Zn 2-5% Nitric acid Zirconium ZrO(NO3)2 2-5% Nitric acid Nitric Acid Blank Hydrochloric Acid Blank Mixed Acid Blank Water Blank CLP-BLN-5 $ 30 / 500 mL CLP-BLN-L $ 45 / L (2 x 500 mL) CLP-BLH-5 $ 30 / 500 mL CLP-BLH-L $ 45 / L (2 x 500 mL) CLP-BLMA-5 CLP-BLMA-L CLP-BLW-5 $ 30 / 500 mL $ 40 / L (2 x 500 mL) 5% HCl in ASTM Type I Water 70 ---100 ---70 ---70 ---70 ---- * see page 67 for details Calibration and Matrix Blanks 5% HNO3 in ASTM Type I Water ------------ $ 30 / 500 mL $ 45 / L (2 x 500 mL) 5% HCl + 1% HNO3 in ASTM Type I Water ASTM Type I Water Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 71 ICP Yttrium Y2O3 2-5% Nitric acid 34 67 ICP/MS Single Element Standards Plasma Emission / Mass Spectroscopy Pure Matrix Special Packaging Traceability to NIST Reference Materials AccuStandard’s ICP/MS Standards are formulated to meet the needs of this very special instrument. As matrix effect is of utmost concern, each standard is formulated in specially purified de-ionized 18 megohm water and Parts per Trillion acids; after both wet chemical and instrumental analysis, the standards are packaged in acid leached FLPE containers to provide required protection and, of course, all standards are traceable to the National Institute of Standards and Technology (NIST) weights and Reference Materials. ICP/MS 100 µg/mL Conc. Element Matrix Unit Al (Aluminum) Sb (Antimony) As (Arsenic) Ba (Barium) Be (Beryllium) Bi (Bismuth) Cd (Cadmium) Ca (Calcium) Cr (Chromium) Co (Cobalt) Cu (Copper) Ge (Germanium) Au (Gold) In (Indium) Fe (Iron) Pb (Lead) Li (Lithium) Mg (Magnesium) Mn (Manganese) Hg (Mercury) Mo (Molybdenum) Ni (Nickel) P (Phosphorous) K (Potassium) Rh (Rhodium) Sc (Scandium) Se (Selenium) Ag (Silver) Na (Sodium) Sr (Strontium) S (Sulphur) Tb (Terbium) Tl (Thallium) Th (Thorium) Sn (Tin) Ti (Titanium) U (Uranium) V (Vanadium) Y (Yttrium) Zn (Zinc) 2% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 H2O tr. HF 10% HCl 2% HNO3 5% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 10% HNO3 H2O tr. NH4OH 2% HNO3 H2O 2% HNO3 10% HCl 2% HNO3 2% HNO3 2% HNO3 2% HNO3 2% HNO3 H2O 2% HNO3 2% HNO3 2% HNO3 2% HNO3 tr HF H2O tr. HF 2% HNO3 2% HNO3 2% HNO3 2% HNO3 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL Cat. No. ICP-MS-01N-0.01X-1 ICP-MS-02N-0.01X-1 ICP-MS-03N-0.01X-1 ICP-MS-04N-0.01X-1 ICP-MS-05N-0.01X-1 ICP-MS-06N-0.01X-1 ICP-MS-08N-0.01X-1 ICP-MS-09N-0.01X-1 ICP-MS-13N-0.01X-1 ICP-MS-14N-0.01X-1 ICP-MS-15N-0.01X-1 ICP-MS-21W-0.01X-1 ICP-MS-22H-0.01X-1 ICP-MS-25N-0.01X-1 ICP-MS-27N-0.01X-1 ICP-MS-29N-0.01X-1 ICP-MS-30N-0.01X-1 ICP-MS-32N-0.01X-1 ICP-MS-33N-0.01X-1 ICP-MS-34N-0.01X-1 ICP-MS-35W-0.01X-1 ICP-MS-37N-0.01X-1 ICP-MS-41W-0.01X-1 ICP-MS-43N-0.01X-1 ICP-MS-46H-0.01X-1 ICP-MS-50N-0.01X-1 ICP-MS-51N-0.01X-1 ICP-MS-53N-0.01X-1 ICP-MS-54N-0.01X-1 ICP-MS-55N-0.01X-1 ICP-MS-56W-0.01X-1 ICP-MS-59N-0.01X-1 ICP-MS-60N-0.01X-1 ICP-MS-61N-0.01X-1 ICP-MS-63N-0.01X-1 ICP-MS-64W-0.01X-1 ICP-MS-66N-0.01X-1 ICP-MS-67N-0.01X-1 ICP-MS-69N-0.01X-1 ICP-MS-70N-0.01X-1 Price $ 34 34 34 34 34 34 34 34 34 34 34 42 78 42 34 34 34 34 34 34 34 34 34 34 190 78 34 34 34 34 34 42 34 34 34 34 42 34 34 34 1,000 µg/mL Conc. Cat. No. ICP-MS-01N-0.1X-1 ICP-MS-02N-0.1X-1 ICP-MS-03N-0.1X-1 ICP-MS-04N-0.1X-1 ICP-MS-05N-0.1X-1 ICP-MS-06N-0.1X-1 ICP-MS-08N-0.1X-1 ICP-MS-09N-0.1X-1 ICP-MS-13N-0.1X-1 ICP-MS-14N-0.1X-1 ICP-MS-15N-0.1X-1 ICP-MS-21W-0.1X-1 ICP-MS-22H-0.1X-1 ICP-MS-25N-0.1X-1 ICP-MS-27N-0.1X-1 ICP-MS-29N-0.1X-1 ICP-MS-30N-0.1X-1 ICP-MS-32N-0.1X-1 ICP-MS-33N-0.1X-1 ICP-MS-34N-0.1X-1 ICP-MS-35W-0.1X-1 ICP-MS-37N-0.1X-1 ICP-MS-41W-0.1X-1 ICP-MS-43N-0.1X-1 ICP-MS-46H-0.1X-1 ICP-MS-50N-0.1X-1 ICP-MS-51N-0.1X-1 ICP-MS-53N-0.1X-1 ICP-MS-54N-0.1X-1 ICP-MS-55N-0.1X-1 ICP-MS-56W-0.1X-1 ICP-MS-59N-0.1X-1 ICP-MS-60N-0.1X-1 ICP-MS-61N-0.1X-1 ICP-MS-63N-0.1X-1 ICP-MS-64W-0.1X-1 ICP-MS-66N-0.1X-1 ICP-MS-67N-0.1X-1 ICP-MS-69N-0.1X-1 ICP-MS-70N-0.1X-1 Price $ 45 45 45 45 45 45 45 45 45 45 45 53 89 53 45 45 45 45 45 45 45 45 45 45 201 89 45 45 45 45 45 53 45 45 45 45 53 45 45 45 10,000 µg/mL Conc. Cat. No. ICP-MS-01N-1 ICP-MS-02N-1 ICP-MS-03N-1 ICP-MS-04N-1 ICP-MS-05N-1 ICP-MS-06N-1 ICP-MS-08N-1 ICP-MS-09N-1 ICP-MS-13N-1 ICP-MS-14N-1 ICP-MS-15N-1 ICP-MS-21W-1 ICP-MS-22H-1 ICP-MS-25N-1 ICP-MS-27N-1 ICP-MS-29N-1 ICP-MS-30N-1 ICP-MS-32N-1 ICP-MS-33N-1 ICP-MS-34N-1 ICP-MS-35W-1 ICP-MS-37N-1 ICP-MS-41W-1 ICP-MS-43N-1 ICP-MS-46H-1 ICP-MS-50N-1 ICP-MS-51N-1 ICP-MS-53N-1 ICP-MS-54N-1 ICP-MS-55N-1 ICP-MS-56W-1 ICP-MS-59N-1 ICP-MS-60N-1 ----------------ICP-MS-63N-1 ICP-MS-64W-1 ----------------ICP-MS-67N-1 ICP-MS-69N-1 ICP-MS-70N-1 If you need an element that is not listed above or you require a different matrix, size or concentration, our experienced chemists will provide you with a custom quotation. Get exactly what you need. 72 Quality System is Certified to comply with the International ISO 9001 Quality Standard Price $ 76 76 76 76 76 76 76 76 76 76 76 84 120 84 76 76 76 76 76 76 76 76 76 76 232 120 76 76 76 76 76 84 76 --76 76 --76 76 76 AA Single Element Standards Atomic Absorption Spectroscopy Traceable to NIST Reference Materials Most available in either Nitric or Hydrochloric acid matrix Certificate of Analysis included at No Charge with each Standard ISO 9001 Quality System Actual Concentration Analysis Each standard is prepared from high purity starting material, de-ionized water and high purity acids. Every standard is instrumentally assayed to verify concentration of specified element. Actual Lot Analysis is provided on the label and a Certificate of Analysis is included for ease of record keeping and availability at audits. Element Unit Aluminum 2-5% Nitric acid Antimony H2O tr. HNO3 tr. Tartaric acid Arsenic 2-5% Nitric acid Barium 2-5% Nitric acid Beryllium 2-5% Nitric acid Bismuth 2-5% Nitric acid Boron Water tr. NH4OH Cadmium 2-5% Nitric acid Calcium 2-5% Nitric acid Cerium 2-5% Nitric acid Cesium 2-5% Nitric acid Chromium 2-5% Nitric acid Cobalt 2-5% Nitric acid Dysprosium 2-5% Nitric acid Erbium 2-5% Nitric acid Europium 2-5% Nitric acid Gadolinium 2-5% Nitric acid Gallium 2-5% Nitric acid Gold 10% HCl (min.) 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 20 100 500 mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL Cat. No. Price -----AA01N-1 AA01N-5 -----AA02N-1 AA02N-5 -----AA03N-1 AA03N-5 -----AA04N-1 AA04N-5 -----AA05N-1 AA05N-5 -----AA06N-1 AA06N-5 -----AA07W-1 AA07W-5 -----AA08N-1 AA08N-5 -----AA09N-1 AA09N-5 -----AA11N-1 AA11N-5 -----AA12N-1 AA12N-5 -----AA13N-1 AA13N-5 -----AA14N-1 AA14N-5 -----AA15N-1 AA15N-5 -----AA16N-1 AA16N-5 -----AA17N-1 AA17N-5 -----AA18N-1 AA18N-5 -----AA19N-1 AA19N-5 -----AA20N-1 AA20N-5 -----AA21W-1 AA21W-5 -----AA22H-1 AA22H-5 -$ 13 33 -13 33 -13 33 -12 30 -19 48 -13 33 -13 33 -13 33 -12 30 -18 40 -15 36 -12 30 -12 30 -12 30 -20 45 -20 45 -20 45 -20 45 -15 36 -18 40 -66 179 Cat. No. AA01N-10X-20ML ----------AA02W-10X-20ML ----------AA03N-10X-20ML ----------AA04N-10X-20ML ----------AA05N-10X-20ML ----------AA06N-10X-20ML ----------AA07W-10X-20ML ----------AA08N-10X-20ML ----------AA09N-10X-20ML ----------AA11N-10X-20ML ----------AA12N-10X-20ML ----------AA13N-10X-20ML ----------AA14N-10X-20ML ----------AA15N-10X-20ML ----------AA16N-10X-20ML ----------AA17N-10X-20ML ----------AA18N-10X-20ML ----------AA19N-10X-20ML ----------AA20N-10X-20ML ----------AA21W-10X-20ML ----------AA22H-10X-20ML ----------- Price $ 20 --20 --20 --20 --20 --20 --20 --20 --20 --20 --35 --20 --20 --20 --35 --35 --35 --35 --45 --35 --80 --- Cat. No. AA01N-25X-20ML -------------------------AA03N-25X-20ML ----------AA04N-25X-20ML -------------------------AA06N-25X-20ML -------------------------AA08N-25X-20ML ----------AA09N-25X-20ML ----------AA11N-25X-20ML ----------AA12N-25X-20ML ----------AA13N-25X-20ML ----------AA14N-25X-20ML ----------AA15N-25X-20ML ----------AA16N-25X-20ML ----------AA17N-25X-20ML ----------AA18N-25X-20ML ----------AA19N-25X-20ML ----------------------------------------AA22H-25X-20ML ----------- * see page 67 for details Price $ 37 -----37 --37 -----37 -----37 --37 --45 --60 --37 --37 --37 --60 --60 --60 --60 --------200 --- Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com For your convenience these elements are also available in Other Matrices. Contact Technical Service for more info AA Copper 2-5% Nitric acid Germanium Water tr. HF NoHaz Package (No Hazardous Charges) * 10,000 µg/mL 25,000 µg/mL 1000 µg/mL Starting Mat'l Matrix 73 AA Single Element Standards Atomic Absorption Spectroscopy Element AA Starting Mat'l Matrix Unit Hafnium 20 2-5% Nitric acid tr. HF 100 500 Holmium 20 2-5% Nitric acid 100 500 Indium 20 2-5% Nitric acid 100 500 Iridium 20 10% HCl (min.) 100 500 Iron 20 2-5% Nitric acid 100 500 Lanthanum 20 2-5% Nitric acid 100 500 Lead 20 2-5% Nitric acid 100 500 Lithium 20 2-5% Nitric acid 100 500 Lutetium 20 2-5% Nitric acid 100 500 Magnesium 20 2-5% Nitric acid 100 500 Manganese 20 2-5% Nitric acid 100 500 Mercury 20 10% Nitric acid 100 500 Molybdenum 20 Water tr. NH4OH 100 500 Neodymium 20 2-5% Nitric acid 100 500 Nickel 20 2-5% Nitric acid 100 500 Niobium 20 Water tr. HF 100 500 Palladium 20 10% HCl (min.) 100 500 Phosphorus 20 Water 100 500 Platinum 20 10% HCl (min.) 100 500 Potassium 20 2-5% Nitric acid 100 500 Praseodymium 20 2-5% Nitric acid 100 500 Rhenium 20 Water 100 500 Rhodium 20 10% HCl (min.) 100 500 Rubidium 20 2-5% Nitric acid 100 500 Ruthenium 20 10% HCl 100 500 74 NoHaz Package (No Hazardous Charges) * 10,000 µg/mL 25,000 µg/mL 1000 µg/mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL Cat. No. Price -----AA23N-1 AA23N-5 -----AA24N-1 AA24N-5 -----AA25N-1 AA25N-5 -----AA26H-1 AA26H-5 -----AA27N-1 AA27N-5 -----AA28N-1 AA28N-5 -----AA29N-1 AA29N-5 -----AA30N-1 AA30N-5 -----AA31N-1 AA31N-5 -----AA32N-1 AA32N-5 -----AA33N-1 AA33N-5 -----AA34N-1 AA34N-5 -----AA35W-1 AA35W-5 -----AA36N-1 AA36N-5 -----AA37N-1 AA37N-5 -----AA38W-1 AA38W-5 -----AA40H-1 AA40H-5 -----AA41W-1 AA41W-5 -----AA42H-1 AA42H-5 -----AA43N-1 AA43N-5 -----AA44N-1 AA44N-5 -----AA45W-1 AA45W-5 -----AA46H-1 AA46H-5 -----AA47N-1 AA47N-5 -----AA48H-1 AA48H-5 -$ 45 110 -20 45 -18 40 -65 150 -12 30 -15 36 -12 30 -12 30 -65 250 -12 30 -11 28 -13 33 -13 33 -20 45 -12 30 -15 36 -62 145 -13 33 -62 145 -12 30 -20 45 -65 150 -80 385 -15 36 -65 150 Cat. No. AA23N-10X-20ML ----------AA24N-10X-20ML ----------AA25N-10X-20ML ----------AA26H-10X-20ML ----------AA27N-10X-20ML ----------AA28N-10X-20ML ----------AA29N-10X-20ML ----------AA30N-10X-20ML ----------AA31N-10X-20ML ----------AA32N-10X-20ML ----------AA33N-10X-20ML ----------AA34N-10X-20ML ----------AA35W-10X-20ML ----------AA36N-10X-20ML ----------AA37N-10X-20ML ----------AA38W-10X-20ML ----------AA40H-10X-20ML ----------AA41W-10X-20ML ----------AA42H-10X-20ML ----------AA43N-10X-20ML ----------AA44N-10X-20ML ----------AA45W-10X-20ML ----------AA46H-10X-20ML ----------AA47N-10X-20ML ----------AA48H-10X-20ML ----------- Price $ 60 --35 --35 --70 --20 --20 --20 --20 --80 --20 --20 --20 --20 --25 --20 --20 --80 --20 --80 --20 --35 --80 --210 --20 --80 --- Cat. No. AA23N-25X-20ML ----------AA24N-25X-20ML ----------AA25N-25X-20ML ----------AA26H-25X-20ML ----------AA27N-25X-20ML ----------AA28N-25X-20ML ----------AA29N-25X-20ML ----------AA30N-25X-20ML ----------AA31N-25X-20ML ----------AA32N-25X-20ML ----------AA33N-25X-20ML ----------AA34N-25X-20ML ----------AA35W-25X-20ML ----------AA36N-25X-20ML ----------AA37N-25X-20ML ----------AA38W-25X-20ML ----------AA40H-25X-20ML -------------------------AA42H-25X-20ML ----------AA43N-25X-20ML ----------AA44N-25X-20ML ----------AA45W-25X-20ML ----------AA46H-25X-20ML ----------AA47N-25X-20ML ----------AA48H-25X-20ML ----------- Price $ 125 --60 --60 --165 --37 --37 --37 --37 --275 --37 --37 --37 --37 --50 --37 --37 --175 -----175 --37 --60 --175 --425 --37 --165 --- Quality System is Certified to comply with the International ISO 9001 Quality Standard * see page 67 for details AA Single Element Standards Atomic Absorption Spectroscopy Element NoHaz Package (No Hazardous Charges) * 10,000 µg/mL 25,000 µg/mL 1000 µg/mL Starting Mat'l Matrix Unit Samarium 2-5% Nitric acid mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL mL Cat. No. Price -----AA49N-1 AA49N-5 -----AA50N-1 AA50N-5 -----AA51N-1 AA51N-5 -----AA52W-1 AA52W-5 -----AA53N-1 AA53N-5 -----AA54N-1 AA54N-5 -----AA55N-1 AA55N-5 -----AA56W-1 AA56W-5 -----AA57W-1 AA57W-5 -----AA58H-1 AA58H-5 -----AA59N-1 AA59N-5 -----AA60N-1 AA60N-5 -----AA61N-1 AA61N-5 -----AA62N-1 AA62N-5 -----AA63N-1 AA63N-5 -----AA64W-1 AA64W-5 -----AA65W-1 AA65W-5 -----AA66N-1 AA66N-5 -----AA67N-1 AA67N-5 -----AA68N-1 AA68N-5 -----AA69N-1 AA69N-5 -----AA70N-1 AA70N-5 -----AA71N-1 AA71N-5 -$ 20 45 -62 145 -19 46 -13 33 -16 40 -13 33 -12 30 -15 35 -15 35 -15 35 -20 45 -15 35 -20 45 -60 135 -19 46 -13 33 -15 35 -15 35 -13 33 -20 45 -15 35 -13 33 -15 35 Cat. No. AA49N-10X-20ML ----------AA50N-10X-20ML ----------AA51N-10X-20ML ----------AA-52W-10X-20ML ----------AA53N-10X-20ML ----------AA54N-10X-20ML ----------AA55N-10X-20ML ----------AA56W-10X-20ML ----------AA57W-10X-20ML ----------AA58H-10X-20ML ----------AA59N-10X-20ML ----------AA60N-10X-20ML -------------------------AA62N-10X-20ML ----------AA63N-10X-20ML ----------AA64W-10X-20ML ----------AA65W-10X-20ML -------------------------AA67N-10X-20ML ----------AA68N-10X-20ML ----------AA69N-10X-20ML ----------AA70N-10X-20ML ----------AA71N-10X-20ML ----------- Price $ 35 --75 --20 --20 --20 --20 --20 --20 --35 --20 --35 --20 -----65 --20 --20 --20 -----20 --35 --20 --20 --20 --- Cat. No. Price AA49N-25X-20ML ----------AA50N-25X-20ML ----------AA51N-25X-20ML -------------------------AA53N-25X-20ML ----------AA54N-25X-20ML ----------AA55N-25X-20ML ----------AA56W-25X-20ML ----------AA57W-25X-20ML ----------- $ 60 --160 --50 -----45 --37 --37 --37 --60 --- ----------AA59N-25X-20ML ----------AA60N-25X-20ML -------------------------AA62N-25X-20ML ----------AA63N-25X-20ML -------------------------- --60 --37 -----150 --50 ------ -------------------------AA67N-25X-20ML ----------AA68N-25X-20ML ----------AA69N-25X-20ML ----------AA70N-25X-20ML ----------AA71N-25X-20ML ----------- -----37 --60 --37 --37 --37 --- Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com AA 20 100 500 Scandium 20 2-5% Nitric acid 100 500 Selenium 20 2-5% Nitric acid 100 500 Silicon 20 Water tr. HF 100 500 Silver 20 2-5% Nitric acid 100 500 Sodium 20 2-5% Nitric acid 100 500 Strontium 20 2-5% Nitric acid 100 500 Sulfur 20 Water 100 500 Tantalum 20 Water tr. HF 100 500 Tellurium 20 10% HCl (min.) 100 500 Terbium 20 2-5% Nitric acid 100 500 Thallium 20 2-5% Nitric acid 100 500 Thorium 20 100 2-5% Nitric acid 500 Thulium 20 2-5% Nitric acid 100 500 Tin 20 2-5% Nitric acid tr. HF 100 500 Titanium 20 Water tr. HF 100 500 Tungsten 20 Water tr. NH4OH 100 500 Uranium 20 2-5% Nitric acid 100 500 Vanadium 20 2-5% Nitric acid 100 500 Ytterbium 20 2-5% Nitric acid 100 500 Yttrium 20 2-5% Nitric acid 100 500 Zinc 20 2-5% Nitric acid 100 500 Zirconium 20 2-5% Nitric acid 100 500 * see page 67 for details 75 Ion Chromatography IC Anion Singles • 99.999% High Purity Starting Materials • 18 Megohm, ASTM type 1 Water • Packaged in pre-cleaned high quality HDPE bottles Standard is Supplied with a Certificate of Analysis, • Each stating traceability to NIST, certified value and expiration date Solution is filtered through a 0.2 µm filter to • Final eliminate contaminants (such as suspended solids and microbes). This extends shelf life and protects your column. • Ready-To-Use Mixes and Calibration Sets • Standards may be used for other “Classical or Wet” methods • Most Complete Product Line Right Size” allows you to purchase as much or as little as you need • "The minimizing waste, and assuring Fresh Solution when you need it most Next Day Delivery on request Used for Influent & Effluent monitoring in aqueous matrices by ASTM & other EPA Methods in the Petrochemical Industry Ion Chrom - Anion Singles (Water Matrix) Symbol (Element) Unit Anion Conc. 100 µg/mL Price Anion Conc. 200 µg/mL Price Anion Conc. 1000 µg/mL Price F (Fluoride) 100 mL 500 mL IC-F-1X-1 IC-F-1X-5 $ 15 55 IC-F-2X-1 IC-F-2X-5 $ 25 60 IC-F-10X-1 IC-F-10X-5 $ 45 70 Cl (Chloride) 100 mL 500 mL IC-Cl-1X-1 IC-Cl-1X-5 $ 15 55 IC-Cl-2X-1 IC-Cl-2X-5 $ 25 60 IC-Cl-10X-1 IC-Cl-10X-5 $ 45 70 NO2 (Nitrite) 100 mL 500 mL IC-NO2-1X-1 IC-NO2-1X-5 $ 15 55 IC-NO2-2X-1 IC-NO2-2X-5 $ 25 60 IC-NO2-10X-1 IC-NO2-10X-5 $ 45 70 NO3 (Nitrate) 100 mL 500 mL IC-NO3-1X-1 IC-NO3-1X-5 $ 15 55 IC-NO3-2X-1 IC-NO3-2X-5 $ 25 60 IC-NO3-10X-1 IC-NO3-10X-5 $ 45 70 Br (Bromide) 100 mL 500 mL IC-BR-1X-1 IC-BR-1X-5 $ 15 55 IC-BR-2X-1 IC-BR-2X-5 $ 25 60 IC-BR-10X-1 IC-BR-10X-5 $ 45 70 PO4 (Phosphate) 100 mL 500 mL IC-PO4-1X-1 IC-PO4-1X-5 $ 15 55 IC-PO4-2X-1 IC-PO4-2X-5 $ 25 60 IC-PO4-10X-1 IC-PO4-10X-5 $ 45 70 SO4 (Sulfate) 100 mL 500 mL IC-SO4-1X-1 IC-SO4-1X-5 $ 15 55 IC-SO4-2X-1 IC-SO4-2X-5 $ 25 60 IC-SO4-10X-1 IC-SO4-10X-5 $ 45 70 Kit Price Anion Conc. 200 µg/mL Kit Price Anion Conc. 1000 µg/mL Kit Price IC Ion Chrom - Anion Kits (Water Matrix) Kit Price SAVE 25% Kit = one bottle of each analyte Unit Anion Conc. 100 µg/mL 100 mL IC-AN-KIT-1X-1 $ 75 7 x 100 mL IC-F-1X-1 IC-NO2-1X-1 IC-BR-1X-1 IC-SO4-1X-1 Kit Price SAVE 25% Kit = one bottle of each analyte 500 mL IC-AN-KIT-1X-5 $ 285 7 x 500 mL IC-F-1X-5 IC-NO2-1X-5 IC-BR-1X-5 IC-SO4-1X-5 76 IC-Cl-1X-1 IC-NO3-1X-1 IC-PO4-1X-1 IC-Cl-1X-5 IC-NO3-1X-5 IC-PO4-1X-5 IC-AN-KIT-2X-1 $ 130 7 x 100 mL IC-F-2X-1 IC-NO2-2X-1 IC-BR-2X-1 IC-SO4-2X-1 IC-Cl-2X-1 IC-NO3-2X-1 IC-PO4-2X-1 IC-AN-KIT-2X-5 $ 315 7 x 500 mL IC-F-2X-5 IC-NO2-2X-5 IC-BR-2X-5 IC-SO4-2X-5 IC-Cl-2X-5 IC-NO3-2X-5 IC-PO4-2X-5 IC-AN-KIT-10X-1$ 235 7 x 100 mL IC-F-10X-1 IC-NO2-10X-1 IC-BR-10X-1 IC-SO4-10X-1 IC-Cl-10X-1 IC-NO3-10X-1 IC-PO4-10X-1 IC-AN-KIT-10X-5$ 365 7 x 500 mL IC-F-10X-5 IC-NO2-10X-5 IC-BR-10X-5 IC-SO4-10X-5 IC-Cl-10X-5 IC-NO3-10X-5 IC-PO4-10X-5 Quality System is Certified to comply with the International ISO 9001 Quality Standard Ion Chromatography IC Anion Mixtures Anion Mixes Ion Chrom Standards Anion Mix #1 Anion Mix #7 Anion Mix #11 Anion Mix #15 IC-MAN-01-1 Water Matrix IC-MAN-07-SET $ 100 / 2 x 100 mL IC-MAN-07-R1-1 $ 85 / 100 mL Water Matrix 6 comps. IC-MAN-11-1 Water Matrix IC-MAN-15R-SET $ 80 / 2 x 100 mL IC-MAN-15-R2-1 $ 70 / 100 mL Water Matrix 3 comps. $ 100 / 100 mL 5 comps. F (Fluoride) Cl (Chloride) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) 20 30 100 150 150 µg/mL µg/mL µg/mL µg/mL µg/mL Anion Mix #2 IC-MAN-02-1 Water Matrix $ 115 / 100 mL 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) 100 200 400 400 600 400 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL Anion Mix #3 IC-MAN-03-1 Water Matrix $ 75 / 100 mL 3 comps. F (Fluoride) Cl (Chloride) SO4 (Sulfate) 100 µg/mL 100 µg/mL 100 µg/mL Anion Mix #4 IC-MAN-04-1 Water Matrix $ 115 / 100 mL 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) 100 100 100 100 100 100 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL Anion Mix #5 IC-MAN-05-SET $ 100 / 2 x 100 mL IC-MAN-05-R1-1 $ 85 / 100 mL Water Matrix 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL 100 mL 20 µg/mL Anion Mix #6 IC-MAN-06-SET $ 100 / 2 x 100 mL IC-MAN-06-R1-1 $ 85 / 100 mL Water Matrix 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) IC-NO2-0.05X-1 NO2 (Nitrite) 1 5 5 5 5 10 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL 100 mL 5 µg/mL Technical Note In order to enhance the shelf life and long term stability of our IC products. AccuStandard has split the Nitrite out of mixes that contain Nitrate. IC-NO2-0.1X-1 NO2 (Nitrite) 1 10 10 10 10 10 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL 100 mL 10 µg/mL Anion Mix #8 IC-MAN-08-SET $ 100 / 2 x 100 mL IC-MAN-08-R1-1 $ 85 / 100 mL Water Matrix 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) IC-NO2-0.2X-1 NO2 (Nitrite) 10 20 20 20 20 20 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL 100 mL 20 µg/mL Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) 1000 1000 1000 1000 1000 µg/mL µg/mL µg/mL µg/mL µg/mL Anion Mix #12 IC-MAN-12-1 Water Matrix $ 100 / 100 mL 5 comps. Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) 15 15 15 15 15 µg/mL µg/mL µg/mL µg/mL µg/mL Anion Mix #13 IC-MAN-13-1 Water Matrix $ 75 / 100 mL 3 comps. F (Fluoride) Cl (Chloride) SO4 (Sulfate) 25 µg/mL 50 µg/mL 100 µg/mL Anion Mix #9 Anion Mix #14 IC-MAN-09-SET $ 100 / 2 x 100 mL IC-MAN-09-R1-1 $ 85 / 100 mL Water Matrix 6 comps. IC-MAN-14-SET $ 115 / 2 x 100 mL IC-MAN-14-R3-1 $ 85 / 100 mL Water Matrix 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) IC-NO2-0.4X-1 NO2 (Nitrite) 20 40 40 40 40 40 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL 100 mL 40 µg/mL Anion Mix #10 IC-MAN-10-SET $ 100 / 2 x 100 mL IC-MAN-10-R1-1 $ 85 / 100 mL Water Matrix 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) IC-NO2-0.5X-1 NO2 (Nitrite) 25 50 50 50 50 50 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL 100 mL 50 µg/mL IC-MAN-CAL-SET $ 395 / 9 x 100 mL Contains one each of: CLP-BLW-5 (500 mL) IC-MAN-07-SET IC-MAN-09-SET IC-MAN-08-SET IC-MAN-10-SET Technical Note This Ready-to-Use set of standards can be used to generate a 5 point calibration curve (including blank). F (Fluoride) 20 µg/mL Cl (Chloride) 30 µg/mL 100 µg/mL NO3 (Nitrate) Br (Bromide) 100 µg/mL PO4 (Phosphate) 150 µg/mL SO4 (Sulfate) 150 µg/mL IC-NO2-1X-1 $ 15 / 100 mL 100 µg/mL NO2 (Nitrite) IC-MAN-14-R2-SET is perfect for US EPA Method 300.0 Anion Mix #14 Revised F (Fluoride) NO3 (Nitrate) PO4 (Phosphate) IC-NO2-1X-1 NO2 (Nitrite) 100 µg/mL 100 µg/mL 100 µg/mL $ 15 / 100 mL 100 µg/mL Anion Mix #16 IC-MAN-16-SET $ 115 / 2 x 100 mL IC-MAN-16-R1-1 $ 100 / 100 mL Water Matrix 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) IC-NO2-0.4X-1 NO2 (Nitrite) 100 200 100 20 30 20 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL $ 15 / 100 mL 40 µg/mL Anion Mix #17 IC-MAN-17-SET $ 100 / 2 x 100 mL IC-MAN-17-R1-1 $ 85 / 100 mL Water Matrix 5 comps. Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) 20 12 12 12 80 IC-NO2-0.12X-1 NO2 (Nitrite) µg/mL µg/mL µg/mL µg/mL µg/mL 100 mL 12 µg/mL Anion Mix #18 IC-MAN-18-SET $ 115 / 2 x 100 mL IC-MAN-18-R1-1 $ 85 / 100 mL Water Matrix 5 comps. F (Fluoride) Cl (Chloride) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) IC-NO2-1X-1 NO2 (Nitrite) 100 100 100 100 100 µg/mL µg/mL µg/mL µg/mL µg/mL $ 15 / 100 mL 100 µg/mL IC-MAN-14-R2-SET$ 115 / 2 x 100 mL IC-MAN-14-R2-1 $ 85 / 100 mL Water Matrix 6 comps. IC IC-NO2-0.2X-1 NO2 (Nitrite) 10 20 20 20 5 30 F (Fluoride) Cl (Chloride) Br (Bromide) NO3 (Nitrate) PO4 (Phosphate) SO4 (Sulfate) $ 175 / 100 mL 5 comps. F (Fluoride) 20 µg/mL Cl (Chloride) 30 µg/mL Br (Bromide) 100 µg/mL N-NO3 (Nitrogen-Nitrate) 100 µg/mL P-PO4 (Phosphorus-Phosphate) 150 µg/mL SO4 (Sulfate) 150 µg/mL IC-NO2-N-1X-1 $ 15 / 100 mL N-NO2 (Nitrogen-Nitrite) 100 µg/mL Don't see the solution you need ? Use our Custom Quotation FAX Form in the back of the catalog and take advantage of our technical experience to help you formulate the solutions for your problems. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 77 Ion Chromatography IC Used for Influent & Effluent monitoring in aqueous matrices by ASTM & other EPA Methods in the Petrochemical Industry Ion Chrom - Cation Singles (Dilute HNO3 Matrix) Symbol (Element) Unit 100 µg/mL Price 200 µg/mL Price 1000 µg/mL Price Ca (Calcium) 100 mL 500 mL IC-CA-1X-1 IC-CA-1X-5 $ 15 55 IC-CA-2X-1 IC-CA-2X-5 $ 25 60 IC-CA-10X-1 IC-CA-10X-5 $ 45 70 NH4 (Ammonium) 100 mL 500 mL IC-NH4-1X-1 IC-NH4-1X-5 $ 15 55 IC-NH4-2X-1 IC-NH4-2X-5 $ 25 60 IC-NH4-10X-1 * IC-NH4-10X-5 * $ 45 70 Mg (Magnesium) 100 mL 500 mL IC-MG-1X-1 IC-MG-1X-5 $ 15 55 IC-MG-2X-1 IC-MG-2X-5 $ 25 60 IC-MG-10X-1 IC-MG-10X-5 $ 45 70 K (Potassium) 100 mL 500 mL IC-K-1X-1 IC-K-1X-5 $ 15 55 IC-K-2X-1 IC-K-2X-5 $ 25 60 IC-K-10X-1 IC-K-10X-5 $ 45 70 Na (Sodium) 100 mL 500 mL IC-NA-1X-1 IC-NA-1X-5 $ 15 55 IC-NA-2X-1 IC-NA-2X-5 $ 25 60 IC-NA-10X-1 IC-NA-10X-5 $ 45 70 Li (Lithium) 100 mL 500 mL IC-LI-1X-1 IC-LI-1X-5 $ 15 55 IC-LI-2X-1 IC-LI-2X-5 $ 25 60 IC-LI-10X-1 IC-LI-10X-5 $ 45 70 Ba (Barium) 100 mL 500 mL IC-BA-1X-1 IC-BA-1X-5 $ 15 55 IC-BA-2X-1 IC-BA-2X-5 $ 25 60 IC-BA-10X-1 IC-BA-10X-5 $ 45 70 Sr (Strontium) 100 mL 500 mL IC-SR-1X-1 IC-SR-1X-5 $ 15 55 IC-SR-2X-1 IC-SR-2X-5 $ 25 60 IC-SR-10X-1 IC-SR-10X-5 $ 45 70 1000 µg/mL Price * These Standards are 1,000 µg/mL as Ammonium (NH4) Other Nitrogen species equivalents are: NH3 (Ammonia) = 944 µg/mL N (Nitrogen) = 776 µg/mL Ion Chrom - Cation Kits (Dilute HNO3 Matrix) Kit Price SAVE 25% Kit = one bottle of each analyte Kit Price SAVE 25% Kit = one bottle of each analyte Cation Mixes Unit 100 µg/mL 100 mL IC-CAT-KIT-1X-1 $ 75 8 x 100 mL IC-CAT-KIT-2X-1 $ 130 8 x 100 mL IC-CA-1X-1 IC-MG-1X-1 IC-NA-1X-1 IC-BA-1X-1 IC-CA-2X-1 IC-MG-2X-1 IC-NA-2X-1 IC-BA-2X-1 500 mL IC IC-NH4-1X-1 IC-K-1X-1 IC-LI-1X-1 IC-SR-1X-1 200 µg/mL Price IC-NH4-2X-1 IC-K-2X-1 IC-LI-2X-1 IC-SR-2X-1 IC-CAT-KIT-1X-5 $ 285 8 x 500 mL IC-CAT-KIT-2X-5 $ 315 8 x 500 mL IC-CA-1X-5 IC-MG-1X-5 IC-NA-1X-5 IC-BA-1X-5 IC-CA-2X-5 IC-MG-2X-5 IC-NA-2X-5 IC-BA-2X-5 IC-NH4-1X-5 IC-K-1X-5 IC-LI-1X-5 IC-SR-1X-5 IC-NH4-2X-5 IC-K-2X-5 IC-LI-2X-5 IC-SR-2X-5 IC-CAT-KIT-10X-1 $ 235 8 x 100 mL IC-CA-10X-1 IC-MG-10X-1 IC-NA-10X-1 IC-BA-10X-1 IC-NH4-10X-1 IC-K-10X-1 IC-LI-10X-1 IC-SR-10X-1 IC-CAT-KIT-10X-5 $ 365 8 x 500 mL IC-CA-10X-5 IC-MG-10X-5 IC-NA-10X-5 IC-BA-10X-5 IC-NH4-10X-5 IC-K-10X-5 IC-LI-10X-5 IC-SR-10X-5 Ion Chrom Standards Cation Mix #1 IC-MCA-01-1 Dilute HNO3 Ca (Calcium) 1000 µg/mL NH4 (Ammonium) 400 µg/mL Mg (Magnesium) 200 µg/mL $ 150 / 100 mL 6 comps. K (Potassium) 200 µg/mL Na (Sodium) 200 µg/mL Li (Lithium) 50 µg/mL Cation Mix #2 IC-MCA-02-1 Dilute HNO3 Ca (Calcium) 100 µg/mL NH4 (Ammonium) 100 µg/mL Mg (Magnesium) 100 µg/mL 78 Price $ 125 / 100 mL 6 comps. K (Potassium) 100 µg/mL Na (Sodium) 100 µg/mL Li (Lithium) 100 µg/mL Cation Mix #3 Cation Mix #5 IC-MCA-03-1 Dilute HNO3 IC-MCA-05-1 Dilute HNO3 $ 100 / 100 mL 4 comps. Ca (Calcium) NH4 (Ammonium) Na (Sodium) Li (Lithium) 100 100 50 10 µg/mL µg/mL µg/mL µg/mL NH4 (Ammonium) K (Potassium) Na (Sodium) Li (Lithium) Cation Mix #4 Cation Mix #6 IC-MCA-04-1 Dilute HNO3 IC-MCA-06-1 Dilute HNO3 $ 125 / 100 mL 4 comps. Ca (Calcium) Mg (Magnesium) Ba (Barium) Sr (Strontium) 400 200 1600 600 µg/mL µg/mL µg/mL µg/mL $ 125 / 100 mL 4 comps. 3 6 3 0.5 µg/mL µg/mL µg/mL µg/mL Ca (Calcium) 2 µg/mL NH4 (Ammonium) 1.5 µg/mL Mg (Magnesium) 2 µg/mL $ 125 / 100 mL 6 comps. K (Potassium) 2.5 µg/mL Na (Sodium) 1.5 µg/mL Li (Lithium) 0.2 µg/mL Quality System is Certified to comply with the International ISO 9001 Quality Standard Ion Chromatography IC Ion Chrom Eluents 0.5 M Sodium bicarbonate (100X concentrate) 50 mL $ 45 IC-ELU-01-0.5 100 mL $ 60 IC-ELU-01-1 5 x 50 mL $ 135 IC-ELU-01-0.5-PAK 5 x 100 mL $ 250 IC-ELU-01-1-PAK 0.5 M Sodium carbonate (100X concentrate) 50 mL $ 45 IC-ELU-02-0.5 100 mL $ 60 IC-ELU-02-1 5 x 50 mL $ 135 IC-ELU-02-0.5-PAK 5 x 100 mL $ 250 IC-ELU-02-1-PAK 0.18 M Sodium carbonate/ 0.17 M Sodium bicarbonate (100X concentrate) 50 mL $ 25 IC-ELU-03-0.5 100 mL $ 30 IC-ELU-03-1 5 x 50 mL $ 60 IC-ELU-03-0.5-PAK 5 x 100 mL $ 115 IC-ELU-03-1-PAK Easy to use, ready to dilute concentrates. Open a fresh bottle and dilute the volume (50 mL to 5 L or 100 mL to 10 L) and be assured of a fresh uncontaminated mobile phase. EPA 300.0, ASTM Method D-4327 Ion Chrom - Ion Singles as the Element Unit 100 µg/mL NO2-N (Nitrite-Nitrogen) Water Matrix 100 mL 500 mL IC-NO2-N-1X-1 IC-NO2-N-1X-5 Price $ 15 55 IC-NO2-N-10X-1 $ 45 IC-NO2-N-10X-5 70 1000 µg/mL Price NO3-N (Nitrate-Nitrogen) Water Matrix 100 mL 500 mL IC-NO3-N-1X-1 IC-NO3-N-1X-5 $ 15 55 IC-NO3-N-10X-1 $ 45 IC-NO3-N-10X-5 70 PO4-P (Phosphate-Phosphorous) Water Matrix 100 mL 500 mL IC-PO4-P-1X-1 IC-PO4-P-1X-5 $ 15 55 IC-PO4-P-10X-1 $ 45 IC-PO4-P-10X-5 70 SO4-S (Sulfate-Sulfur) Water Matrix 100 mL 500 mL IC-SO4-S-1X-1 IC-SO4-S-1X-5 $ 15 55 IC-SO4-S-10X-1 $ 45 IC-SO4-S-10X-5 70 NH4-N (Ammonium-Nitrogen) Water Matrix 100 mL 500 mL IC-NH4-N-1X-1 IC-NH4-N-1X-5 $ 15 55 IC-NH4-N-10X-1 $ 45 IC-NH4-N-10X-5 70 Anion Mix #14 Revised Anion Singles Kits IC-AN-KIT-R-10X-1 Each at 1000 µg/mL IC-F-10X-1 IC-Cl-10X-1 IC-NO2-N-10X-1 IC-NO3-N-10X-1 IC-BR-10X-1 IC-PO4-P-10X-1 IC-SO4-S-10X-1 Recommended product for EPA Method 300.0 “Determination of Inorganic Anions by Ion Chromatography” and ASTM D-4327-91, “Test Method for Anions in Water by Chemically Suppressed Ion Chromatography.” $ 235 / 7 x 100 mL Fluoride Chloride Nitrite-Nitrogen Nitrate-Nitrogen Bromide Phosphate-Phosphorous Sulfate-Sulfur IC-AN-KIT-R-10X-5 Each at 1000 µg/mL IC-F-10X-5 IC-Cl-10X-5 IC-NO2-N-10X-5 IC-NO3-N-10X-5 IC-BR-10X-5 IC-PO4-P-10X-5 IC-SO4-S-10X-5 $ 365 / 7 x 500 mL Fluoride Chloride Nitrite-Nitrogen Nitrate-Nitrogen Bromide Phosphate-Phosphorous Sulfate-Sulfur IC-MAN-14-R2-SET IC-MAN-14-R2-1 Water Matrix $ 115 / 2 x 100 mL 100 mL 6 comps. F (Fluoride) Cl (Chloride) Br (Bromide) N-NO3 (Nitrogen-Nitrate) P-PO4 (Phosphorus-Phosphate) SO4 (Sulfate) 20 30 100 100 150 150 µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL IC-NO2-N-1X-1 N-NO2 (Nitrogen-Nitrite) 100 mL 100 µg/mL Organic Acid Salt Standards 100 µg/mL 100 mL 500 mL IC-FORM-1X-1 IC-FORM-1X-5 Price $ 15 55 IC-FORM-10X-1 IC-FORM-10X-5 1000 µg/mL Price $ 45 70 Acetate Water Matrix 100 mL 500 mL IC-ACET-1X-1 IC-ACET-1X-5 $ 15 55 IC-ACET-10X-1 IC-ACET-10X-5 $ 45 70 Oxalate Water Matrix 100 mL 500 mL IC-OXAL-1X-1 IC-OXAL-1X-5 $ 15 55 IC-OXAL-10X-1 IC-OXAL-10X-5 $ 45 70 Chlorate Water Matrix 100 mL 500 mL IC-CHLR-1X-1 IC-CHLR-1X-5 $ 15 55 IC-CHLR-10X-1 IC-CHLR-10X-5 $ 45 70 Chromate Water Matrix 100 mL 500 mL IC-CHRM-1X-1 IC-CHRM-1X-5 $ 15 55 IC-CHRM-10X-1 $ 45 IC-CHRM-10X-5 70 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com IC Unit Formate Water Matrix 79 On-Line Ordering There is an easier way to get Chemical Reference Standards ® e-Standards from AccuStandard.com 5 Ways to Search “e-Standards” is the Fastest, Most Comprehensive Search Engine available and contains over 30,000 products. Search by: Catalog Number Single or Multiple Components, Method (EPA, ASTM, etc.) Chemical Category (Organic, Inorganic, Petroleum, etc.) Other Companys’ Part Number Log on to www.accustandard.com and see how easy it is. Easy Ordering 24/7 Find It Fast...simply search for a product, select it for purchase & click - it's that easy! Discounts may apply to online orders, see details on website. On-Line Custom Services AccuStandard specializes in synthesizing chemicals of high purity to be used as reference standards, and offers custom synthesis capability for milligram to kilogram batches. If you can't find the specific standard you need, we can prepare Custom Formulations and Custom Packaging for both Organic and Inorganic needs. See our Website for more info. Over 30,000 Standards just a click away IC Custom Formulations AccuStandard offers over 30,000 different standards, and if you can't find the specific standard you need, we will prepare a custom formulation. Our custom organic and inorganic standards are a fast, economical way to address your unique requirements. To make an inquiry for Custom Quotes visit our website. You can also Email your requirements to [email protected] or Fax us at 203-786-5287. Please include the following information: List of analytes and concentrations, Solvent or matrix, Quantity required (milliliters), Packaging unit size (milliliters per ampule, bottle, or vial). Quality Control Options 1. Gravimetric/Volumetric Certification: Each standard is measured gravimetrically and then QC’ed instrumentally (where available). Every component in the standard is guaranteed to be within ±0.5% of the requested value unless otherwise stated. The solutions are made up to volume using class A glassware. A certificate comes with each standard and documents the gravimetric values used. 2. Quantitative Validation: Full QA/QC method includes extended GC analysis using both internal and calibration standards plus statistical analysis. A data package is provided containing analytical and gravimetric data (Organic customs only). Also available: OEM Standards - Privately labeled standards manufactured and tested to your specifications. 80 LUFT/LUST Standards State Methods Alaska GRO Hydrocarbons DRO Hydrocarbons RRO Hydrocarbons Arizona Diesel Range California Gasoline Connecticut Extractable TPH Florida FTRPH 82-84 Massachusetts 87-88 EPH VPH Mississippi 86 DRO Multi-State 86 Hydrocarbon Window Defining Pensylvania 89 Storage Tank Monitoring Standards Tennessee 86 DRO Texas 89 Method 1005 (PST) Washington 90-91 VPH EPH Wisconsin 91 Gasoline Range Hydrocarbons 85 85 85 86 LUFT/LUST TPH Pattern Recognition Standards 92-93 93 Gasoline Range HC Analysis (CA, PA, WI) 94 Diesel Range HC Analysis 95 ASTM Method D-2887 95 Complete Hydrocarbon Analysis 95 Proficiency Test Samples 96 Method 1664, Oil, Grease & TPH Analysis 97 Methods 413.2, 418.1 & TPH Analysis 97 Method 8440 TPH Analysis 97 Method 1004 Alcohol Oxidation Products in Engine Exhaust 98 ASTM E-1387 and E-1618 for Fire Debris Analysis 98 Skinner List Refinery Waste (ASTM#E1387) 98 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 81 LUFT/LUST Weathered LUFT/LUST Fuel Standards LUFT/LUST LUFT/LUST Standards Alaska State Methods Alaska Method Determination of Gasoline Range Organic (GRO) Hydrocarbons Normal Alkane Standard - GRO Defining Mixture AK-101.0-NAS-10X AK-101.0-NAS-10X-PAK 2.0 mg/mL each in MeOH $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 5 comps. n-Hexane n-Heptane n-Octane n-Nonane n-Decane Laboratory Control Standard AK-101.0-LCS AK-101.0-LCS-PAK 5.0 mg/mL in MeOH $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL Gasoline - Regular, unleaded Certified BTEX in Unleaded Gasoline (Single Source) GA-001-20X-BTEX 10.0 mg/mL in MeOH $ 55 / 1 x 1 mL Technical Notes Laboratory Control Standard The Gasoline Laboratory Control Standard was taken from an ASTM selected fuel set and a source independent of what is being used in the Gasoline Composite Mix. Simultaneous BTEX / Gasoline QA/QC AccuStandard's QA/QC Department has certified the benzene, toluene, ethyl benzene and xylene concentrations in our unleaded gasoline standard (GA-001-20X-BTEX & in AK-101.0-GCS-BTEX). Use of either standard allows the analytical chemist in a single injection to verify that the QA/QC requirements are being met for the BTEX analytes as well as for the gasoline. Since formulating the standards for the Alaskan method, and because of numerous laboratory requests, we have added a new multi source certified BTEX in gasoline composite mix (AK-101.0GCS-BTEX). The BTEX values for this multi-source calibration standard have been determined through in-house analysis against a BTEX multi level calibration curve, and are listed in the Certificate. AccuStandard continues to look for innovative approaches to save the analytical laboratory time and money. Gasoline - Regular, unleaded Certified BTEX in Gasoline Composite Mix (Multi Source) see Technical Note AK-101.0-GCS-BTEX 5 mg/mL total in MeOH Gasoline Calibration Composite Mixture $ 55 / 1 x 1 mL 3 comps. $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 3 comps. Gasoline - Premium (1.66 mg/mL) Gasoline - Regular, leaded (1.67 mg/mL) Gasoline - Regular, unleaded (1.67 mg/mL) Gasoline - Premium (1.66 mg/mL) Gasoline - Regular, leaded (1.67 mg/mL) Gasoline - Regular, unleaded (1.67 mg/mL) Gasoline Calibration Mix Version 4/02 Surrogate Control Standard AK-101.0-SS AK-101.0-SS-PAK 50 µg/mL each in MeOH $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL AK-101.0-SS-10X AK-101.0-SS-10X-PAK 500 µg/mL each in MeOH $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL AK-101.0-SS-100X AK-101.0-SS-100X-PAK 5,000 µg/mL each in MeOH $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 2 comps. p-Bromofluorobenzene AK-101.0-GCS AK-101.0-GCS-PAK Total 5.0 mg/mL in MeOH a,a,a-Trifluorotoluene AK-101-GSC-R1 AK-101-GSC-R1-PAK Equal parts by weight of each $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL Gasoline - Regular, unleaded Gasoline - Plus, unleaded Gasoline - Premium, unleaded Internal Standard AK-101.0-IS-10X AK-101.0-IS-10X-PAK 2.0 mg/mL in MeOH $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 1-Chloro-4-fluorobenzene LUFT/LUST Alaska Method Determination of Aromatic & Aliphatic Hydrocarbons in Gasoline Range Organics AK101AA Aromatics Mix AK-101AA-ARO AK-101AA-ARO-PAK 2000 µg/mL each in MeOH Benzene Toluene Ethylbenzene m-Xylene 82 $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 14 comps. p-Xylene o-Xylene 1,2,3-Trimethylbenzene 1,2,4-Trimethylbenzene NEW 1,3,5-Trimethylbenzene Isopropylbenzene m-Ethyltoluene p-Ethyltoluene o-Ethyltoluene n-Propylbenzene Quality System is Certified to comply with the International ISO 9001 Quality Standard LUFT/LUST LUFT/LUST Standards Alaska State Methods Alaska Method Determination of Diesel Range Organic (DRO) Hydrocarbons Diesel Calibration Composite Mixture (low sulfur) AK-102.0-DCS AK-102.0-DCS-PAK Total 5.0 mg/mL in CH2Cl2 Diesel Fuel, Arctic (1.66 mg/mL) #1 Diesel - Low Sulfur (1.67 mg/mL) AK-102.0-DCS-10X AK-102.0-DCS-10X-PAK Total 50.0 mg/mL in CH2Cl2 Diesel Fuel, Arctic (16.6 mg/mL) #1 Diesel - Low Sulfur (16.7 mg/mL) $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 3 comps. #2 Diesel - extra Low Sulfur (1.67 mg/mL) $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 3 comps. #2 Diesel - extra Low Sulfur (16.7 mg/mL) Laboratory Control Standard (low sulfur) Stock Concentrate Diesel Calibration Composite Mixture AK-102.0-DCS-R1-10X $ 40 / 1 x 1 mL AK-102.0-DCS-R1-10X-PAK SAVE 20% $ 160 / 5 x 1 mL Total 50.0 mg/mL in CH2Cl2 3 comps. Diesel Fuel, Arctic (16.6 mg/mL) #1 Diesel - Low Sulfur (16.7 mg/mL) #2 Diesel - Conventional (16.7 mg/mL) Laboratory Control Standard AK-102.0-LCS-R1-10X $ 20 / 1 x 1 mL AK-102.0-LCS-R1-10X-PAK SAVE 20% $ 80 / 5 x 1 mL 50.0 mg/mL in Acetone #2 Diesel - Conventional AK-102.0-LCS AK-102.0-LCS-PAK 5.0 mg/mL in Acetone $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL AK102.0-LCS-10X AK-102.0-LCS-10X-PAK 50.0 mg/mL in Acetone $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL Technical Note #2 Diesel - extra Low Sulfur The Laboratory Control Standard was prepared from an independent source of material than what was used in the Diesel Calibration Composite mix. Technical Note AccuStandard originally formulated the Diesel Calibration Composite Mix and Laboratory Control Standard using two independent sources of #2 Diesel as required by the Alaskan method. Unfortunately, the chromatographic patterns for the #2 diesel sources (conventional & extra low sulfur) are different. We have actively sought out and obtained independent sources of each type of #2 diesel to insure similar chromatographic patterns . We recommend that when a customer is analyzing the Diesel Calibration Composite and Laboratory Control standard that the client orders AK-102.0-DCS & AK-102.0-LCS products together to obtain similar chromatographic patterns for #2 diesel extra low sulfur patterns and AK-102.0-DCS-R1-10X & AK-102.0-LCS-R1-10X products to obtain similar chromatographic patterns for #2 Diesel conventional patterns. We believe most laboratories performing the Alaskan DRO analysis will find the #2 Diesel conventional chromatographic pattern more closely resembles typical Diesel samples drawn from environmental sites. Normal Alkane Standard - DRO Defining Mixture Surrogate Standards AK-102.0-NAS-10X AK-102.0-NAS-10X-PAK 2.0 mg/mL each in CH2Cl2 AK-102.0-SS AK-102.0-SS-PAK 200 µg/mL in Acetone $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL AK102.0-SS-10X AK102.0-SS-10X-PAK 2.0 mg/mL in Acetone $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL n-Decane n-Undecane n-Dodecane n-Tridecane n-Tetradecane n-Pentadecane n-Hexadecane n-Heptadecane $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 16 comps. n-Octadecane n-Nonadecane n-Eicosane n-Heneicosane n-Docosane n-Tricosane n-Tetracosane n-Pentacosane o-Terphenyl Internal Standard AK-102.0-IS AK-102.0-IS-PAK 1.0 mg/mL in CH2Cl2 $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL 5-alpha Androstane LUFT/LUST Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 83 LUFT/LUST Standards LUFT/LUST Alaska State Methods Alaska Method Determination of Aromatic & Aliphatic Hydrocarbons in Diesel Range Organics AK102AA DRO Standard AK-102AA-DRO $ 40 / 1 x 1 mL AK-102AA-DRO-PAK SAVE 20% $ 160 / 5 x 1 mL 10 comps. 2000 µg/mL each in CH2Cl2 n-Undecane n-Pentadecane n-Heptadecane n-Octadecane n-Tetracosane Naphthalene Acenaphthene Fluorene Pyrene Anthracene Alaska Method AK102/103AA Retention Time Marker Standard AK-102/103AA-RT AK-102/103AA-RT-PAK 50 µg/mL each in CH2Cl2 $ 25 / 1 x 1 mL $ 100 / 5 x 1 mL 3 comps. n-Decane n-Pentacosane n-Hexatriacontane AK102/103AA Surrogate Standard AK-102/103AA-SS $ 35 / 1 x 1 mL AK-102/103AA-SS-PAK SAVE 20% $ 140 / 5 x 1 mL 3 comps. 1000 µg/mL each in CH2Cl2 Squalane o-Terphenyl 5,6,7,8-Tetrahydro-1-naphthol Determination of Residual Range Organics (RRO) Hydrocarbon Residual Composite Mixtures AK-103.0-RCS AK-103.0-RCS-PAK Total 5.0 mg/mL in CH2Cl2 Laboratory Control Standard $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 3 comps. SAE 30W Motor Oil SAE 40W Motor Oil SAE 50W Motor Oil (1.66 mg) (1.67 mg) (1.67 mg) AK-103.0-LCS AK-103.0-LCS-PAK 5.0 mg/mL in Acetone $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL AK-103.0-LCS-5X AK-103.0-LCS-5X-PAK 25.0 mg/mL in Acetone: CH2Cl2 (1:1) $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL SAE 40W Motor Oil AK-103.0-RCS-10X AK-103.0-RCS-10X-PAK Total 50.0 mg/mL in CH2Cl2 $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 3 comps. SAE 30W Motor Oil SAE 40W Motor Oil SAE 50W Motor Oil (16.6 mg) (16.7 mg) (16.7 mg) Surrogate Control Standard AK-103.0-SS AK-103.0-SS-PAK 500 µg/mL in Acetone $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL AK-103.0-SS-10X AK-103.0-SS-10X-PAK 5.0 mg/mL in THF : Acetone (1:3) $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL n-Triacontane-d62 Alaska Method Determination of Aromatic and Aliphatic Hydrocarbons in Residual Range Organics AK103AA RRO Standard AK-103AA-RRO $ 35 / 1 x 1 mL AK-103AA-RRO-PAKSAVE 20% $ 140 / 5 x 1 mL 9 comps. 50 µg/mL each in CH2Cl2 Benzo[b]fluoranthene Benzo[a]pyrene Benzo[g,h,i]perylene Dibenz[a,h]anthracene AK-102/103AA-RT $ 25 / 1 x 1 mL AK-102/103AA-RT-PAK SAVE 20% $ 100 / 5 x 1 mL 50 µg/mL each in CH2Cl2 3 comps. n-Decane n-Pentacosane n-Hexatriacontane AK102/103AA Surrogate Standard AK-102/103AA-SS $ 35 / 1 x 1 mL AK-102/103AA-SS-PAK SAVE 20% $ 140 / 5 x 1 mL 3 comps. 1000 µg/mL each in CH2Cl2 Squalane o-Terphenyl 5,6,7,8-Tetrahydro-1-naphthol LUFT/LUST n-Hexacosane n-Octacosane n-Triacontane n-Dotriacontane n-Tetratriacontane AK102/103AA Retention Time Marker Standard 84 Quality System is Certified to comply with the International ISO 9001 Quality Standard LUFT/LUST Standards LUFT/LUST Arizona California Connecticut State Methods Arizona Method Determination of Diesel Range and Oil Range Organic Hydrocarbons Retention Time Verification Standard Diesel & Oil Range Standard AZ-8015-DRO/ORO AZ-8015-DRO/ORO-PAK 2000 µg/mL each in CH2Cl2 n-Decane n-Dodecane n-Docosane n-Dotriacontane $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 12 comps. n-Octadecane n-Tetracosane n-Tetradecane n-Triacontane n-Eicosane n-Hexacosane n-Hexadecane n-Octacosane AZ-8015-RTV AZ-8015-RTV-PAK 2000 µg/mL each in CH2Cl2 n-Decane n-Docosane $ 25 / 1 x 1 mL SAVE 20% $ 100 / 1 x 1 mL 3 comps. n-Dotriacontane Stock Calibration Standard Surrogate Standards AK-102.0-SS-10X AK-102.0-SS-10X-PAK 2.0 mg/mL in Acetone $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL AZ-8015-SCS AZ-8015-SCS-PAK 10000 µg/mL each in CH2Cl2 #2 Diesel $ 40 / 1 x 1 mL SAVE 20% $ 160 / 1 x 1 mL 2 comps. 10W 30 Motor Oil o-Terphenyl California Method California - Gasoline Range Hydrocarbons Oxygenate Gasoline Additive Standard S-603A-10X S-603A-10X-PAK 2.0 mg/mL each in MeOH OGAD-001 OGAD-001-PAK At stated conc. in MeOH $ 25 / 1 x 1 mL SAVE 25% $ 90 / 5 x 1 mL 7 comps. Benzene Ethylbenzene Methyl t-butyl ether m-Xylene p-Xylene Toluene o-Xylene LA County Well Investigation & Monitoring Program Purgeable Aromatics - Gasoline ID M-602-GAS-10X 2.0 mg/mL each in MeOH Benzene Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene $ 30 / 1 x 1 mL 11 comps. 1,4-Dichlorobenzene Ethylbenzene Toluene o-Xylene Connecticut Method p-Xylene m-Xylene MtBE (2000 µg/mL) (2000 µg/mL) (2000 µg/mL) TAME t-Butanol (2000 µg/mL) (10000 µg/mL) Ethanol M-8015B/5031-11 10 mg/mL in Water $ 25 / 1 x 1 mL Methanol M-8015B/5031-17 10 mg/mL in Water $ 20 / 1 x 1 mL Extractable Total Petroleum Hydrocarbon CT ETPH Alkane Standard DRH-009S DRH-009S-PAK 1000 µg/mL in CH2Cl2 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane MtBE ETBE Isopropyl ether $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 5 comps. Surrogate Standard $ 35 / 1 x 1 mL SAVE 20% $ 140 / 5 x 1 mL 15 comps. n-Octadecane n-Eicosane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Dotriacontane n-Tetratriacontane n-Hexatriacontane Proficiency Test Samples required for the ETPH method and individual fuels are available as standard products. Custom formulations can be quoted and manufactured to meet your specific application. $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL o-Terphenyl (OTP) Internal Standard GRH-IS GRH-IS-PAK 1.0 mg/mL in CH2Cl2 LUFT/LUST Technical Note GRH-SS GRH-SS-PAK 2.0 mg/mL in Acetone $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL 5-alpha Androstane Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 85 LUFT/LUST Standards LUFT/LUST Florida Miss/Tenn Mult-State Florida Method State Methods Total Recoverable Petroleum Hydrocarbon (FTRPH) Standard & Surrogates Calibration/Window Defining Hydrocarbon Standard FTRPH Surrogate Standard DRH-004S-5X DRH-004S-5X-PAK 1.0 mg/mL each in CH2Cl2 : CS2 (1:1) Octane C8 Eicosane Decane C10 Docosane Dodecane C12 Tetracosane Tetradecane C14 Hexacosane Hexadecane C16 Octacosane Octadecane C18 Triacontane DRH-FL-SS-3X DRH-FL-SS-3X-PAK 3.0 mg/mL in Carbon disulfide $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL DRH-FL-SS DRH-FL-SS-PAK 1.0 mg/mL in Carbon disulfide $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL $ 50 / 1 x 1 mL SAVE 20% $ 200 / 5 x 1 mL 17 comps. C20 Dotriacontane C32 C22 Tetratriacontane C34 C24 Hexatricontane C36 C26 Octatriacontane C38 C28 Tetracontane C40 C30 Nonatriacontane FTRPH Calibration / Window Defining Standard FTRPH Combined Surrogate Standard DRH-FTRPH DRH-FTRPH-PAK 500 µg/mL each in Hexane DRH/GRH-FL-SS DRH/GRH-FL-SS-PAK 5.0 mg/mL in Carbon disulfide n-Octane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane $ 35 / 1 x 1 mL SAVE $ 150 / 5 x 1 mL 17 comps. n-Dotriacontane n-Tetratriacontane n-Hexatriacontane n-Octatriacontane n-Tetracontane n-Eicosane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane Technical Note The above FTRPH Calibration/Window Defining Standard was formulated at a lower concentration to insure solubility of the analytes & eliminate the odor caused by the introduction of Carbon disulfide as a cosolvent. Nonatriacontane $ 50 / 1 x 1 mL SAVE 20% $ 200 / 5 x 1 mL 2 comps. o-Terphenyl (OTP) Technical Note The above FTRPH Surrogate Standard was formulated at a higher concentration for combined DRH & GRH analysis. This standard has proven useful for those laboratories performing gasoline & diesel analysis simultaneously. DRH/GRH-FL-SS-R2 NEW DRH/GRH-FL-SS-R2-PAK At stated conc. in Carbon disulfide Nonatriacontane (6000 µg/mL) Internal Standard $ 50 / 1 x 1 mL SAVE 20% $ 200 / 5 x 1 mL 2 comps. o-Terphenyl (OTP) (1500 µg/mL) Technical Note GRH-IS GRH-IS-PAK 1.0 mg/mL in CH2Cl2 $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL 5-alpha Androstane Items in Carbon disulfide cannot ship by Air. Whenever possible we try to find an alternate solvent, however some long chain hydrocarbon will not go in solution or any other solvent. Surrogate Standards DRH-SS DRH-SS-PAK 5.0 mg/mL in THF $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL GRH-SS GRH-SS-PAK 2.0 mg/mL in Acetone $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL o-Terphenyl (OTP) n-Triacontane-d62 Mississippi / Tennessee Method Multi-State Method DRO Defining Mix DRH-008S-R2 DRH-008S-R2-PAK 500 µg/mL each in Chloroform Octane Heptadecane Nonane Pristane Decane Octadecane Undecane Phytane Dodecane Nonadecane Tridecane Eicosane Tetradecane Heneicosane Pentadecane Docosane Hexadecane Tricosane AK-102.0-NAS-10X AK-102.0-NAS-10X-PAK 2.0 mg/mL each in CH2Cl2 LUFT/LUST n-Decane n-Undecane n-Dodecane n-Tridecane n-Tetradecane n-Pentadecane $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 16 comps. n-Hexadecane n-Heptadecane n-Octadecane n-Nonadecane n-Eicosane n-Heneicosane n-Docosane n-Tricosane n-Tetracosane n-Pentacosane Hydrocarbon Window Defining $ 65 / 1 x 1 mL SAVE 20% $ 260 / 5 x 1 mL 35 comps. Tetracosane Tritriacontane Pentacosane Tetratriacontane Hexacosane Pentatriacontane Heptacosane Hexatriacontane Octacosane Heptatriacontane Nonacosane Octatriacontane Triacontane Nonatriacontane n-Hentriacontane Tetracontane Dotriacontane Technical Note AccuStandard offers a hydrocarbon window defining standard with the C8 to C40 odd and even alkanes. Use of this one standard should meet the numerous state-to-state variations for hydrocarbon validation and reporting. As an added benefit, AccuStandard has included Pristane and Phytane in the formulation. Again, use of this one standard can meet numerous LUFT/LUST programs requiring that the C17 (Pristane) and C18 (Phytane) ratio be used to estimate subsurface degradation of fuel oil spills. 86 Quality System is Certified to comply with the International ISO 9001 Quality Standard LUFT/LUST Massachusetts LUFT/LUST Standards State Methods - Ready-to-Inject Working Level EPH Standards Massachusetts Method Determination of Extractable Petroleum Hydrocarbons (EPH) Aromatic Hydrocarbons Calibration Set DEP (MA) - Aromatic Hydrocarbons DRH-006-CAL-SET At stated conc. in CH2Cl2 DRH-006S DRH-006S-PAK 1.0 mg/mL each in CH2Cl2 $ 125 / 5 x 1 mL 18 comps. DRH DRH DRH DRH DRH -006 -006 -006 -006 -006 -CA -CA -CA -CA -CA L-2 L L-4 L L -1X -10X -4X Cat. No. 0X 0X Components (units in µg/mL) Level 1 ( 1X ) Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene Dibenz[a,h]anthracene Fluoranthene Fluorene Indeno[1,2,3-cd]pyrene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene o-Terphenyl (Surrogate) Level 2 ( 4X ) 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 Level 3 ( 10X ) 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Level 4 ( 20X ) 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 Level 5 ( 40X ) 200 200 200 200 200 200 200 200 200 200 200 200 200 200 200 200 200 200 Aliphatic Hydrocarbons Calibration Set DRH-007-CAL-SET At stated conc. in CH2Cl2 $ 125 / 5 x 1 mL 15 comps. DRH DRH DRH DRH DRH -007 -007 -007 -007 -007 -CA -CA -CA -CA -CA L-4 L-1 L-4 L-2 L-1 0X 0X X 0X X Cat. No. Components (units in µg/mL) Level 1 ( 1X ) n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane n-Eicosane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane 1-Chlorooctadecane (Surrogate) Level 2 ( 4X ) 5 5 5 5 5 5 5 5 5 5 5 5 5 5 5 20 20 20 20 20 20 20 20 20 20 20 20 20 20 20 Level 3 ( 10X ) Level 4 ( 20X ) 50 50 50 50 50 50 50 50 50 50 50 50 50 50 50 100 100 100 100 100 100 100 100 100 100 100 100 100 100 100 Aliphatic Surrogate High Concentrates AccuStandard formulated two high concentration EPH stocks for laboratories that prepare in-house working level solutions. CCC Working Level In addition, AccuStandard received numerous requests to formulate Ready-to-Use working level aromatic and aliphatic calibration sets. AccuStandard's Product Development Team designed the two listed Calibration sets to meet those requests. Custom/Bulk Packaging Larger volumes of Daily Continuing Calibration solution can be purchased by contacting our Technical Service Department. DEP (MA) - Aliphatic Hydrocarbons Level 5 ( 40X ) 200 200 200 200 200 200 200 200 200 200 200 200 200 200 200 DRH-007S $ 40 / 1 x 1 mL DRH-007S-PAK SAVE 20% $ 160 / 5 x 1 mL 14 comps. 1.0 mg/mL each in CH2Cl2 : Hexane (1:1) n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane DRH-MA-MS DRH-MA-MS-PAK DRH-MA-MS-10X DRH-MA-MS-10X-PAK 1-Chlorooctadecane n-Eicosane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane 25 µg/mL in Acetone $ 20 / 1 x 1 mL 25 µg/mL in Acetone SAVE 20% $ 80 / 5 x 1 mL 250 µg/mL in Acetone $ 30 / 1 x 1 mL 250 µg/mL in AcetoneSAVE 20% $ 120 / 5 x 1 mL DRH-MA-MS-40X 1,000 µg/mL in Acetone $ 30 / 1 x 1 mL DRH-MA-MS-40X-PAK 1,000 µg/mL in AcetoneSAVE 20% $ 120 / 5 x 1 mL 10 comps. EPH Surrogate Spike 1-Chlorooctadecane Technical Notes LUFT/LUST $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL 20 200 2,000 2,000 Dibenz[a,h]anthracene Fluoranthene Fluorene Indeno[1,2,3-cd]pyrene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene EPH Matrix Spike DRH-007-SS DRH-007-SS-PAK 1.0 mg/mL in Hexane DRH-MA-SS DRH-MA-SS-10X DRH-MA-SS-100X DRH-MA-SS-100X-PAK Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene $ 65 / 1 x 1 mL SAVE 20% $ 260 / 5 x 1 mL 17 comps. µg/mL each µg/mL each µg/mL each µg/mL each in Acetone $ 10 in Acetone $ 20 in Acetone $ 20 in Acetone $ 100 / / / / 1 1 1 5 2 x 1 mL x 1 mL x 1 mL x 1 mL comps. Acenaphthene Anthracene Chrysene n-Eicosane Naphthalene n-Nonadecane n-Nonane n-Octacosane Pyrene n-Tetradecane o-Terphenyl Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 87 LUFT/LUST Standards LUFT/LUST Massachusetts State Methods Massachusetts Method Determination of Extractable Petroleum Hydrocarbons (EPH) (Continued) DEP (MA) - Fractionation Surrogate Spike DRH-MA-FSS-10ML 40 µg/mL in Hexane $ 25 / 1 x 10 mL DRH-MA-FSS-50X 2.0 mg/mL in Hexane $ 25 / 1 x 1 mL DRH-MA-FSS-50X-PAK 2.0 mg/mL in HexaneSAVE 20% $ 100 / 5 x 1 mL 2 comps. 2-Fluorobiphenyl 2-Bromonaphthalene Aromatic Surrogate DRH-006-SS DRH-006-SS-PAK 1.0 mg/mL in CH2Cl2 $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL o-Terphenyl Internal Standard GRH-IS 1,000 µg/mL in CH2Cl2 $ 15 / 1 x 1 mL GRH-IS-PAK 1,000 µg/mL in CH2Cl2 SAVE 20% $ 60 / 5 x 1 mL GRH-IS-10X 10.0 mg/mL in CH2Cl2 $ 30 / 1 x 1 mL Combined Aromatic/Aliphatic Matrix Spike Standard DRH-MS-ASL DRH-MS-ASL-PAK 25 µg/mL each in Hexane $ 45 / 1 x 1 mL SAVE 20% $ 180 / 5 x 1 mL 31 comps. n-Hexacosane n-Hexadecane n-Hexatriacontane Indeno[1,2,3-cd]pyrene 2-Methylnaphthalene Naphthalene n-Nonadecane n-Nonane n-Octacosane n-Octadecane Phenanthrene Pyrene n-Tetracosane n-Tetradecane n-Triacontane Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene n-Decane Dibenz[a,h]anthracene n-Docosane n-Dodecane n-Eicosane Fluoranthene Fluorene 5-alpha Androstane Massachusetts Method Determination of Volatile Petroleum Hydrocarbons (VPH) Stock Concentrate Volatile Petroleum Hydrocarbon Mix Volatile Petroleum Hydrocarbons with Surrogate Standard GRH-004S-10X GRH-004S-10X-PAK At stated conc. in MeOH GRH-004S/SS GRH-004S/SS-PAK At stated conc. in MeOH Benzene Ethylbenzene Isooctane 2-Methylpentane MtBE Naphthalene n-Nonane (5.0 (5.0 (15.0 (15.0 (15.0 (10.0 (10.0 mg/mL) mg/mL) mg/mL) mg/mL) mg/mL) mg/mL) mg/mL) $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 13 comps. n-Pentane (10.0 Toluene (15.0 1,2,4-Trimethylbenzene (10.0 o-Xylene (10.0 m-Xylene (10.0 p-Xylene (10.0 mg/mL) mg/mL) mg/mL) mg/mL) mg/mL) mg/mL) LUFT/LUST DEP (MA)-VPH Surrogate Standard GRH-004-SS GRH-004-SS-PAK 50 µg/mL in MeOH $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL GRH-004-SS-10X GRH-004-SS-10X-PAK 500 µg/mL in MeOH $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL GRH-004-SS-100X GRH-004-SS-100X-PAK 5,000 µg/mL in MeOH $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 2,5-Dibromotoluene VPH Matrix Spike GRH-004-MS GRH-004-MS-PAK 50 µg/mL each in MeOH $ 15 / 1 x 1 mL $ 60 / 5 x 1 mL 8 comps. GRH-004-MS-10X GRH-004-MS-10X-PAK 500 µg/mL each in MeOH $ 25 / 1 x 1 mL $ 100 / 5 x 1 mL 8 comps. GRH-004-MS-100X GRH-004-MS-100X-PAK 5,000 µg/mL each in MeOH Benzene Naphthalene Ethylbenzene Toluene MtBE o-Xylene 88 $ 25 / 1 x 1 mL $ 100 / 5 x 1 mL 8 comps. m-Xylene p-Xylene $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 14 comps. Benzene (500 2,5-Dibromotoluene(Surrogate) (1,000 Ethylbenzene (500 Isooctane (1,500 2-Methylpentane (1,500 MtBE (1,500 Naphthalene (1,000 µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) n-Nonane n-Pentane Toluene 1,2,4-Trimethylbenzene o-Xylene m-Xylene p-Xylene (1,000 (1,000 (1,500 (1,000 (1,000 (1,000 (1,000 µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) Certified BTEX in Unleaded Gasoline GA-001-20X-BTEX 10.0 mg/mL in MeOH $ 55 / 1 x 1 mL Gasoline - Regular, unleaded Technical Notes Calibration Curve Analytical chemists can easily develop the VPH Calibration Curve using one AccuStandard primary dilution standard that includes the surrogate. Simultaneous BTEX / Gasoline QA/QC AccuStandard's QA/QC department has certified the benzene, toluene, ethyl benzene and xylene concentrations in our unleaded gasoline standard (GA-001-20X-BTEX). Use of this standard allows the analytical chemist in a single injection to verify that the QA/QC requirements are being met for the BTEX analytes as well as the gasoline. AccuStandard's Product Development Team continues to look for innovative approaches to save the analytical laboratory time and money. Quality System is Certified to comply with the International ISO 9001 Quality Standard LUFT/LUST Standards LUFT/LUST Penn Texas State Methods Pennsylvania Method Storage Tank Site Closure & Monitoring Petroleum Standards PA Extractable PAH Standard PA Volatile Petroleum Standard DRH-PA-001 DRH-PA-001-PAK 2000 µg/mL each in CH2Cl2 GRH-PA-001 GRH-PA-001-PAK At stated conc. in MeOH Benz[a]anthracene Benzo[a]pyrene Fluorene Texas Method $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 5 comps. Benzene Ethylbenzene MtBE Naphthalene Toluene Naphthalene Phenanthrene (1000 (1000 (2000 (1000 (1000 $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 9 comps. µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) o-Xylene m-Xylene p-Xylene Isopropylbenzene (1000 (1000 (1000 (1000 µg/mL) µg/mL) µg/mL) µg/mL) Storage Tank (PST) Division - TX Method 1005 Standards Gasoline & Diesel Calibration Set Stock Hydrocarbon Calibration Standard DRH-TX-002-D-SET $ 75 / 8 x 1 mL Each mix contains: Regular, Unleaded Gasoline & #2 Diesel Fuel DRH-TX-001-10X DRH-TX-001-10X-PAK 2000 µg/mL each in n-Pentane Cat. No. DRH-TX-002-D-0.01X DRH-TX-002-D-0.04X DRH-TX-002-D-0.1X DRH-TX-002-D-0.2X DRH-TX-002-D-0.4X DRH-TX-002-D-1X DRH-TX-002-D-2X DRH-TX-002-D-10X 5 20 50 100 200 500 1000 5000 Conc. µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL Solvent CH2Cl2 CH2Cl2 CH2Cl2 CH2Cl2 CH2Cl2 CH2Cl2 CH2Cl2 CH2Cl2 n-Hexane n-Octane n-Decane n-Dodecane $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 12 comps. n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Tetradecane n-Hexadecane n-Octadecane n-Eicosane Gasoline/Diesel Calibration/Matrix Spike Solution DRH-TX-002-10X DRH-TX-002-10X-PAK 5000 µg/mL each in MeOH Gasoline - Regular, unleaded $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 2 comps. #2 Diesel Fuel Gasoline/Diesel Continuing Calibration Solution DRH-TX-002-D-0.4X-10ML 200 µg/mL each in CH2Cl2 $ 50 / 1 x 10 mL 2 comps. Gasoline - Regular, unleaded #2 Diesel Fuel Stock Gasoline/Diesel Calibration Solution DRH-TX-002-D-40X DRH-TX-002-D-40X-PAK 20,000 µg/mL each in CH2Cl2 Gasoline - Regular, unleaded $ 25 / 1 x 1 mL SAVE 20% $ 100 / 5 x 1 mL 2 comps. #2 Diesel Fuel Technical Notes Texas Method 1005 Rev. 03 and 1006 Over 22,000 notifications of leaking petroleum storage tanks have been received by the Texas Natural Resource Conservation Commission. At least 8000 of these leaks have affected groundwater resulting in the testing and monitoring of the site. The capability to test for TPH concentration and identify the petrochemical product offers analytical laboratories additional sources of revenue. New State specific methods have been proposed and promulgated to determine the Total concentration of Petroleum Hydrocarbons (TPH). AccuStandard continues to support the analytical community by developing these new formulations to meet both TNRCC method 1005 Rev. 3.0 and 1006. Additionally, QA/QC and Proficiency Testing samples are now available to monitor sample handling/testing procedures or to receive certification to perform TPH analysis. These new standards are in ready to use calibration curves, cost effective bulk quantities, and convenient concentrations to simplify the instrument calibration procedures. Aromatic Fractionation Check Standard Gasoline & Diesel Calibration Curve DRH-TX-003-SET Each mix contains: Regular, Unleaded Gasoline & #2 Diesel Fuel 20 100 250 500 750 1000 5000 10000 Conc. µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL µg/mL Solvent Pentane Pentane Pentane Pentane Pentane Pentane Pentane Pentane DRH-TX-003-FCS DRH-TX-003-FCS-PAK 20 µg/mL each in Pentane Acenaphthene Acenaphthylene Anthracene Benzene Benz[a]anthracene Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[a]pyrene $ 55 / 1 x 10 mL SAVE 20% $ 220 / 5 x 10 mL 24 comps. Benzo[e]pyrene Benzo[g,h,i]perylene Chrysene Dibenz[a,h]anthracene Ethylbenzene Fluoranthene Fluorene Indeno[1,2,3-cd]pyrene Naphthalene Phenanthrene Pyrene Toluene 1,2,3-Trimethylbenzene m-Xylene p-Xylene o-Xylene Carbon Number Distribution Maker Surrogate Standard DRH-TX-003-SS1 DRH-TX-003-SS1-PAK 10 mg/mL each in Pentane 1-Chlorooctadecane $ 35 / 1 x 5 mL SAVE 20% $ 175 / 5 x 5 mL 2 comps. 1-Chlorooctane DRH-TX-003-CNM DRH-TX-003-CNM-PAK 2000 µg/mL each in Pentane n-Decane n-Dodecane n-Heneicosane $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 9 comps. n-Heptane n-Hexadecane n-Hexane Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com n-Octacosane n-Octane n-Pentatriacontane 89 LUFT/LUST Cat. No. DRH-TX-003-0.04X DRH-TX-003-0.2X DRH-TX-003-0.5X DRH-TX-003-1X DRH-TX-003-1.5X DRH-TX-003-2X DRH-TX-003-10X DRH-TX-003-20X $ 125 / 8 x 1 mL LUFT/LUST Standards LUFT/LUST Washington State Methods Washington Method Determination of Volatile Petroleum Hydrocarbons (VPH) VPH Solution WA-VPH $ 30 / 1 x 1 mL WA-VPH-PAK SAVE 20% $ 120 / 5 x 1 mL 200 µg/mL each in MeOH 15 comps. Benzene Ethylbenzene Toluene o-Xylene m-Xylene p-Xylene MtBE n-Pentane n-Hexane n-Octane n-Decane n-Dodecane 1-Methylnaphthalene Naphthalene 1,2,3-Trimethylbenzene VPH Primary Dilution Standard with Surrogate Benzene Ethylbenzene Toluene o-Xylene m-Xylene p-Xylene MtBE n-Pentane n-Hexane VPH Surrogate Standard GRH-004-SS GRH-004-SS-PAK 50 µg/mL in MeOH µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) WA-VPH-100X $ 35 / 1 x 1 mL WA-VPH-100X-PAK SAVE 20% $ 140 / 5 x 1 mL 20.0 mg/mL each in MeOH 15 comps. n-Octane n-Decane n-Dodecane 1-Methylnaphthalene Naphthalene 1,2,3-Trimethylbenzene 2,5-Dibromotoluene (surrogate) WA-VPH-MS $ 25 / 1 x 1 mL WA-VPH-MS-PAK SAVE 20% $ 100 / 5 x 1 mL Varied conc. in MeOH 11 comps. (60 (60 (180 (360 (200 (600 (60 (60 (60 (60 (60 WA-VPH-10X $ 30 / 1 x 1 mL WA-VPH-10X-PAK SAVE 20% $ 120 / 5 x 1 mL 2,000 µg/mL each in MeOH 15 comps. WA-VPH-10X-SS $ 35 / 1 x 1 mL WA-VPH-10X-SS-PAKSAVE 20% $ 140 / 5 x 1 mL 2,000 µg/mL each in MeOH 16 comps. VPH Matrix Spike Benzene Ethylbenzene MTBE Naphthalene n-Nonane n-Pentane Toluene 1,2,3-Trimethylbenzene m-Xylene p-Xylene o-Xylene Stock Concentrate VPH Solutions Benzene Ethylbenzene Toluene o-Xylene m-Xylene p-Xylene MtBE n-Pentane VPH Retention Time Marker WA-VPH-RT $ 20 / 1 x 1 mL WA-VPH-RT-PAK SAVE 20% $ 80 / 5 x 1 mL 2,000 µg/mL each in MeOH 6 comps. $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL n-Pentane n-Hexane n-Octane GRH-004-SS-10X $ 20 / 1 x 1 mL GRH-004-SS-10X-PAK SAVE 20% $ 80 / 5 x 1 mL 500 µg/mL in MeOH GRH-004-SS-100X $ 20 / 1 x 1 mL GRH-004-SS-100X-PAKSAVE 20% $ 80 / 5 x 1 mL 5,000 µg/mL in MeOH 2,5-Dibromotoluene n-Hexane n-Octane n-Decane n-Dodecane 1-Methylnaphthalene Naphthalene 1,2,3-Trimethylbenzene n-Decane n-Dodecane n-Tridecane 1,2,3-Trimethylbenzene Standard V-028S-D-10X $ 20 / 1 x 1 mL V-028S-D-10X-PAK SAVE 20% $ 80 / 5 x 1 mL 1000 µg/mL each in CH2Cl2 1,2,3-Trimethylbenzene Certified BTEX in Unleaded Gasoline (Single Source) GA-001-20X-BTEX 10.0 mg/mL in MeOH $ 55 / 1 x 1 mL Gasoline - Regular, unleaded Certified BTEX in Gasoline Composite Mix (Multi Source) AK-101.0-GCS-BTEX 5 mg/mL each in MeOH $ 55 / 1 x 1 mL 3 comps. LUFT/LUST Gasoline - Premium (1.66 mg/mL Gasoline - Regular, leaded (1.67 mg/mL) Gasoline - Regular, unleaded (1.67 mg/mL) Technical Notes Simultaneous BTEX / Gasoline QA/QC AccuStandard's QA/QC department has certified the benzene, toluene, ethyl benzene and xylene concentrations in our unleaded gasoline Standard. (GA-001-20X-BTEX and in AK-101.0-GCS-BTEX). Use of either standard allows the analytical chemist in a single injection to verify that the QA/QC requirements are being met for the BTEX analytes as well as for the gasoline. Since formulating the Standards for the TPH methods and because of numerous laboratory requests, we have added a new multi source certified BTEX in gasoline composite mix (AK-101.0-GCS-BTEX). The BTEX values for this multi source calibration standard have been determined through in-house analysis against a BTEX multi level calibration curve. AccuStandard's Product Development Team continues to look for innovative approaches to save the analytical laboratory time and money. Washington EPH Standards on Next Page 90 Quality System is Certified to comply with the International ISO 9001 Quality Standard LUFT/LUST Standards LUFT/LUST Washington Wisconsin State Methods Washington Method Determination of Extractable Petroleum Hydrocarbons (EPH) EPH Aromatic/PAH Standard EPH Aliphatic Check Mix EPH Fractionation Check Solution WA-EPH-10X $ 75 / 1 x 1 mL WA-EPH-10X-PAK SAVE 20% $ 300 / 5 x 1 mL 18 comps. 1.0 mg/mL each in CH2Cl2 WA-EPH-ALI $ 20 / 1 x 1 mL WA-EPH-ALI-PAK SAVE 20% $ 80 / 5 x 1 mL 5 comps. 1.0 mg/mL each in CH2Cl2 WA-EPH-FCS $ 45 / 1 x 1 mL WA-EPH-FCS-PAK SAVE 20% $ 180 / 5 x 1 mL 25 µg/mL each in Hexane 24 comps. Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene Dibenz[a,h]anthracene Fluoranthene Fluorene Indeno[1,2,3-cd]pyrene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene 1,2,3-Trimethylbenzene Internal Standard GRH-IS $ 15 / 1 x 1 mL 1,000 µg/mL in CH2Cl2 GRH-IS-PAK SAVE 20% $ 60 / 5 x 1 mL 1,000 µg/mL in CH2Cl2 GRH-IS-10X $ 30 / 1 x 1 mL 10.0 mg/mL in CH2Cl2 5-alpha Androstane EPH Surrogate Spike DRH-MA-SS 20 µg/mL each in Acetone DRH-MA-SS-10X 200 µg/mL each in Acetone $ 10 / 1 2 $ 20 / 1 2 x 1 mL comps. x 1 mL comps. DRH-MA-SS-100X $ 20 / 1 x 1 mL DRH-MA-SS-100X-PAK SAVE 20% $ 80 / 5 x 1 mL 2,000 µg/mL each in Acetone 2 comps. 1-Chlorooctadecane o-Terphenyl n-Octane n-Decane n-Dodecane n-Hexadecane n-Heneicosane EPH Aromatic Check Mix WA-EPH-ARO $ 30 / 1 x 1 mL WA-EPH-ARO-PAKSAVE 20% $ 120 / 5 x 1 mL 5 comps. 1.0 mg/mL each in CH2Cl2 Acenaphthene Benzo[g,h,i]perylene Naphthalene Revised EPH Aliphatic Check Mix WA-EPH-ALI-R1 $ 20 / 1 x 1 mL WA-EPH-ALI-R1-PAK SAVE 20% $ 80 / 5 x 1 mL 1.0 mg/mL each in CH2Cl2 6 comps. n-Octane n-Decane n-Dodecane WA-EPH-MS2-20ML WA-EPH-MS2-20ML-PAK 25 µg/mL each in Acetone Acenaphthene Anthracene Benzo[g,h,i]perylene Benzo[a]pyrene n-Decane n-Dodecane n-Hexadecane n-Heneicosane Naphthalene Pyrene $ 30 / 1 x 20 mL 10 comps. n-Hexadecane n-Heneicosane n-Tetratriacontane Revised EPH Aromatic Check Mix WA-EPH-ARO-R1 WA-EPH-ARO-R1-PAK 1.0 mg/mL each in CH2Cl2 Acenaphthene Benzo[g,h,i]perylene Naphthalene EPH Matrix Spike Pyrene 1,2,3-Trimethylbenzene $ 30 / 1 x 1 mL $ 120 / 5 x 1 mL 6 comps. Pyrene 1,2,3-Trimethylbenzene Toluene Aliphatic Surrogate DRH-007-SS $ 15 / 1 x 1 mL DRH-007-SS-PAK SAVE 20% $ 60 / 5 x 1 mL 1.0 mg/mL in Hexane Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene Dibenz[a,h]anthracene Fluoranthene Fluorene Indeno[1,2,3-cd]pyrene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Eicosane n-Heneicosane Revised EPH Fractionation Check Solution WA-EPH-FCS-R1 $ 45 / 1 x 1 mL WA-EPH-FCS-R1-PAKSAVE 20% $ 180 / 5 x 1 mL 25 µg/mL each in Hexane 23 comps Acenaphthene Acenaphthylene Anthracene Benz[a]anthracene Benzo[a]pyrene Benzo[b]fluoranthene Benzo[g,h,i]perylene Benzo[k]fluoranthene Chrysene Dibenz[a,h]anthracene Fluoranthene Fluorene Indeno[1,2,3-cd]pyrene 2-Methylnaphthalene Naphthalene Phenanthrene Pyrene n-Octane n-Decane n-Dodecane n-Hexadecane n-Heneicosane n-Tetratriacontane 1,2,3-Trimethylbenzene Standard V-028S-D-10X $ 20 / 1 x 1 mL V-028S-D-10X-PAK SAVE 20% $ 80 / 5 x 1 mL 1000 µg/mL each in CH2Cl2 1,2,3-Trimethylbenzene 1-Chlorooctadecane Aromatic Surrogate DRH-006-SS $ 15 / 1 x 1 mL DRH-006-SS-PAK SAVE 20% $ 60 / 5 x 1 mL 1.0 mg/mL in CH2Cl2 o-Terphenyl LUFT/LUST Wisconsin Method Wisconsin DNR - Gasoline Range Hydrocarbons GRH-003S GRH-003S-PAK 2.0 mg/mL each in MeOH Benzene Ethylbenzene MtBE Naphthalene Toluene $ 35 / 1 x 1 mL SAVE 20% $ 140 / 5 x 1 mL 10 comps. 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m-Xylene p-Xylene Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 91 LUFT/LUST LUFT/LUST Standards TPH Complete Set of Total Petroleum Hydrocarbon (TPH) Pattern Recognition Standards AccuStandard has assembled the following sets to identify specific petroleum product types found during LUFT/LUST investigations. The sets can be purchased using one convenient Cat. No. or as individuals. TPH-SET $ 535 / 33 x 1 mL (includes TPH-001-SET, TPH-002-SET, TPH-003-SET, TPH-004-SET) Motor Fuels & Lubricating Oils Set Aviation Fuels & Oils Set TPH-001-SET TPH-003-SET $ 180 / 11 x 1 mL (Set includes Cat. No.'s listed in Bold) Conc. (mg/mL) Description Regular unleaded Regular leaded Premium RFA Gasoline (oxygenate free) #2 Diesel (conventional) #1 Diesel (low sulfur) #2 Diesel (extra low sulfur) Arctic Diesel SAE 30 W motor oil SAE 40 W motor oil SAE 50 W motor oil 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 Solv. MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 Hexane Hexane CH2Cl2 Hexane Hexane CH2Cl2 Hexane Hexane CH2Cl2 Cat. No. GA-001 GA-001-40X GA-001-D-40X GA-002 GA-002-40X GA-002-D-40X GA-003 GA-003-40X GA-003-D-40X GA-005 GA-005-40X GA-005-D-40X FU-009 FU-009-40X FU-009-D-40X FU-013 FU-013-40X FU-013-D-40X FU-017 FU-017-40X FU-017-D-40X FU-023 FU-023-40X FU-023-D-40X FU-018-H FU-018-H-40X FU-018-D-40X FU-019-H FU-019-H-40X FU-019-D-40X FU-021-H FU-021-H-40X FU-021-D-40X 1 mL Price $ 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 Description Aviation (gas) Grade 100 LL JP-4 Fuel JP-5 Fuel JP-7 Fuel JP-8 Fuel JP-10 Fuel (Cruise Missile) JP-TS Jet Fuel (type 1) Turbine (Jet A) Fuel Hydraulic oil TPH-004-SET Description #1 Fuel Oil LUFT/LUST #2 Fuel Oil #3 Fuel Oil #4 Fuel Oil #5 Fuel Oil #6 Fuel Oil Kerosene 92 $ 115 / 7 x 1 mL (Set includes Cat. No.'s listed in Bold) Conc. (mg/mL) 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 Solv. MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 Hexane Hexane CH2Cl2 Hexane Hexane CH2Cl2 Hexane Hexane CH2Cl2 Hexane Hexane CH2Cl2 MeOH MeOH CH2Cl2 Cat. No. FU-001 FU-001-40X FU-001-D-40X FU-002 FU-002-40X FU-002-D-40X FU-003 FU-003-40X FU-003-D-40X FU-004 FU-004-40X FU-004-D-40X FU-007 FU-007-40X FU-007-D-40X FU-008 FU-008-40X FU-008-D-40X FU-005 FU-005-40X FU-005-D-40X 1 mL Price $ 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 Conc. (mg/mL) 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 0.5 20 20 Solv. MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 MeOH MeOH CH2Cl2 Hexane Hexane CH2Cl2 Cat. No. GA-004 GA-004-40X GA-004-D-40X FU-010 FU-010-40X FU-010-D-40X FU-012 FU-012-40X FU-012-D-40X FU-014 FU-014-40X FU-014-D-40X FU-015 FU-015-40X FU-015-D-40X FU-022 FU-022-40X FU-022-D-40X FU-016 FU-016-40X FU-016-D-40X FU-011 FU-011-40X FU-011-D-40X FU-006 FU-006-40X FU-006-D-40X FU-020-H FU-020-H-40X FU-020-D-40X 1 mL Price $ 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 10 20 20 Household & Industrial Solvent Set Heating Fuel Oils Set TPH-002-SET $ 160 / 10 x 1 mL (Set includes Cat. No.'s listed in Bold) Description Lacquer thinner Mineral spirits Naphtha Turpentine Stoddard $ 80 / 5 x 1 mL (Set includes Cat. No.'s listed in Bold) Conc. (mg/mL) 1 gram 0.5 20.0 20.0 1 gram 0.5 20.0 20.0 1 gram 0.5 20.0 20.0 1 gram 0.5 20.0 20.0 1 gram 0.5 20.0 20.0 Solv. Neat MeOH MeOH CH2Cl2 Neat MeOH MeOH CH2Cl2 Neat MeOH MeOH CH2Cl2 Neat MeOH MeOH CH2Cl2 Neat MeOH MeOH CH2Cl2 Cat. No. HS-001N HS-001S HS-001S-40X HS-001S-D-40X HS-002N HS-002S HS-002S-40X HS-002S-D-40X HS-003N HS-003S HS-003S-40X HS-003S-D-40X HS-004N HS-004S HS-004S-40X HS-004S-D-40X HS-005N HS-005S HS-005S-40X HS-005S-D-40X 1 mL Price $ 10 10 20 20 10 10 20 20 10 10 20 20 10 10 20 20 10 10 20 20 Motor Oil & Weathered Fuels Standards on Next Page Quality System is Certified to comply with the International ISO 9001 Quality Standard LUFT/LUST Standards LUFT/LUST TPH Weathered Fuels Motor Oil Standards Description Conc. (mg/mL) Solv. 0.5 20.0 20.0 0.5 20.0 20.0 Hexane Hexane CH2Cl2 Hexane Hexane CH2Cl2 SAE 5W 30 Motor Oil SAE 10W 30 Motor Oil 1 mL Price Cat. No. FU-025-H FU-025-H-40X FU-025-D-40X FU-026-H FU-026-H-40X FU-026-D-40X $ 10 20 20 10 20 20 Description SAE 10W 40 Motor Oil SAE 20W 50 Motor Oil Conc. (mg/mL) Solv. 0.5 20.0 20.0 0.5 20.0 20.0 Hexane Hexane CH2Cl2 Hexane Hexane CH2Cl2 1 mL Price Cat. No. FU-027-H FU-027-H-40X FU-027-D-40X FU-028-H FU-028-H-40X FU-028-D-40X $ 10 20 20 10 20 20 Weathered LUFT/LUST Fuels Petroleum Products contain many different chemicals, plus synthetic product additives. Typically, these petroleum products are subdivided into two groups based on their volatility: [a] gasoline related products (more volatile) and [b] fuel related products (less volatile such as kerosene, aviation fuels, diesel fuels and heating oils). Most analytical methods for petroleum products focus on several items: the level of BTEX, the total petroleum hydrocarbon number (TPH), and the fingerprint of the petroleum product. Depending on the volatility of the petroleum product spilled, the nature of the contaminated soil, and the age of the spill, analysis becomes even more difficult. Weathering, evaporation, and the migration of the lighter volatiles at the contamination site can affect the fingerprint identification portion of the fuel products analysis. AccuStandard designed the weathered fuel line to artificially mimic the weathering, evaporation, and migration process. Use of these standards can help in the identification of the fuel type if it has been present in the ground for some time, in a sandy type soil with possible evaporation loss, or has migrated from the plume point of origin. Weathered Fuels Motor Oil Composite Standard Weathered Gasoline Set WGU-SET Gasoline - Regular, Gasoline - Regular, Gasoline - Regular, Gasoline - Regular, unleaded unleaded (25% Weathered) unleaded (50% Weathered) unleaded (75% Weathered) 5.0 5.0 5.0 5.0 $ 85 / 4 x 1 mL mg/mL in MeOH mg/mL in MeOH mg/mL in MeOH mg/mL in MeOH GA-001-10X GA-W25-10X GA-W50-10X GA-W75-10X $ $ $ $ 20 25 25 25 / / / / 1 1 1 1 x x x x 1 1 1 1 mL mL mL mL 5.0 5.0 5.0 5.0 $ 85 / 4 x 1 mL mg/mL in CH2Cl2 mg/mL in CH2Cl2 mg/mL in CH2Cl2 mg/mL in CH2Cl2 FU-005-D-10X FK-W25-10X FK-W50-10X FK-W75-10X $ $ $ $ 20 25 25 25 / / / / 1 1 1 1 x x x x 1 1 1 1 mL mL mL mL FU-017-D-10X FD2-W25-10X FD2-W50-10X FD2-W75-10X $ $ $ $ 20 25 25 25 / / / / 1 1 1 1 x x x x 1 1 1 1 mL mL mL mL FU-009-D-10X FD2-W25-R1-10X FD2-W50-R1-10X FD2-W75-R1-10X $ $ $ $ 20 25 25 25 / / / / 1 1 1 1 x x x x 1 1 1 1 mL mL mL mL MO-COMP-D-40X $ 30 / 1 x 1 mL 5000 µg/mL each in CH2Cl2 4 comps. 5w30 Motor oil 10w30 Motor oil 10w40 Motor oil 20w50 Motor oil Weathered Kerosene Set WFK-SET Kerosene Kerosene (25% Weathered) Kerosene (50% Weathered) Kerosene (75% Weathered) Weathered #2 Diesel (extra Low Sulfur Content) Set WFD2-SET #2 Diesel fuel #2 Diesel fuel #2 Diesel fuel #2 Diesel fuel (extra (extra (extra (extra Low Low Low Low Sulfur) Sulfur) (25% Weathered) Sulfur) (50% Weathered) Sulfur) (75% Weathered) 5.0 5.0 5.0 5.0 $ 85 / 4 x 1 mL mg/mL in CH2Cl2 mg/mL in CH2Cl2 mg/mL in CH2Cl2 mg/mL in CH2Cl2 Weathered #2 Diesel (Conventional) Set WFD2-R1-SET #2 Diesel fuel (Conventional) #2 Diesel fuel (Conventional) (25% Weathered) #2 Diesel fuel (Conventional) (50% Weathered) #2 Diesel fuel (Conventional) (75% Weathered) 5.0 5.0 5.0 5.0 $ 85 / 4 x 1 mL mg/mL in CH2Cl2 mg/mL in CH2Cl2 mg/mL in CH2Cl2 mg/mL in CH2Cl2 Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com LUFT/LUST Total Petroleum Hydrocarbon Pattern Recognition Standards This book contains chromatography for the various petroleum products typically found during LUFT/LUST site investigations. The chromatography shows each fuel pattern in a 25 minute analytical run for early eluting petroleum products like gasoline to late eluting products like motor oil. In addition, an n-alkane standard (DRH-008S) analyzed under identical conditions has been overlaid on each petroleum product chromatogram. Use of the book will assist the chemist’s identification of the fuel for pattern recognition. The n-alkane standard (DRH-008S) overlay provides n-alkane reference points between the standard and the unknown sample. These beginning and ending n-alkane reference points can be used to establish gross hydrocarbon concentrations. By comparing the specific n-alkane range of the closest identified petroleum standard to that of the unknown sample, a reproducible gross hydrocarbon number can be achieved. To Order: TPH Book BOOK-TPH $ 35 93 LUFT/LUST GRH LUFT/LUST Standards Gasoline Range Gasoline Range Hydrocarbon Analysis California - Gasoline Range Hydrocarbons EPA Method - Gasoline Range Hydrocarbons Gasoline Standard GRH-002S At stated conc. in MeOH 2-Methylpentane 2,2,4-Trimethylpentane Heptane Benzene Toluene $ 25 / 1 x 1 mL 10 comps. (1.5 (1.5 (0.5 (0.5 (1.5 mg/mL) mg/mL) mg/mL) mg/mL) mg/mL) Ethylbenzene m-Xylene p-Xylene o-Xylene 1,2,4-Trimethylbenzene (0.5 (1.0 (1.0 (1.0 (1.0 mg/mL) mg/mL) mg/mL) mg/mL) mg/mL) Internal Standard GARH-IS 1.0 mg/mL in CH2Cl2 $15 / 1 x 1 mL S-603A-10X S-603A-10X-PAK 2.0 mg/mL each in MeOH Benzene Ethylbenzene Methyl t-butyl ether Toluene $ 25 / 1 x 1 mL SAVE 25% $ 90 / 5 x 1 mL 7 comps. o-Xylene m-Xylene p-Xylene Los Angeles County Well Investigation and Monitoring Program Purgeable Aromatics - Gasoline ID M-602-GAS-10X 2.0 mg/mL each in MeOH Chloro-4-fluorobenzene Surrogate Standard GARH-SS 2.5 mg/mL in Acetone $ 20 / 1 x 1 mL 4-Bromofluorobenzene Benzene Chlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene Ethylbenzene $ 30 / 1 x 1 mL 11 comps. Toluene o-Xylene p-Xylene m-Xylene MtBE Oxygenate Gasoline Additive Standard Gasoline Additives GAD-001 GAD-001-PAK 0.2 mg/mL each in MeOH $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 4 comps. Dibromomethane 1,2-Dibromoethane 1,2-Dichloroethane Methyl t-butyl ether OGAD-001 OGAD-001-PAK At stated conc. in MeOH MtBE ETBE Isopropyl ether (2000 µg/mL) (2000 µg/mL) (2000 µg/mL) $ 30 / 1 x 1 mL $ 120 / 1 x 1 mL 5 comps. TAME t-Butanol (2000 µg/mL) (10000 µg/mL) Ethanol M-8015B/5031-11 10 mg/mL in Water Technical Note Simultaneous BTEX/Gasoline QA/QC AccuStandard's QA/QC department has certified the benzene, toluene, ethyl benzene and xylene concentrations in our unleaded gasoline standard. Use of GA-001-20X-BTEX allows the analytical chemist in a single injection to verify that QA/QC requirements are being met for the BTEX analytes as well as the gasoline. AccuStandard's Product Development Team continues to look for innovative approaches to save the analytical laboratory time and money. Certified BTEX in Unleaded Gasoline GA-001-20X-BTEX 10.0 mg/mL in MeOH $ 55 / 1 x 1 mL $ 25 / 1 x 1 mL Methanol M-8015B/5031-17 10 mg/mL in Water $ 20 / 1 x 1 mL Pennsylvania DER - Gasoline Range Hydrocarbons GRH-001S GRH-001S-PAK 1.0 mg/mL each in MeOH Benzene Ethylbenzene Heptane 2-Methyl pentane Toluene $ 25 / 1 x 1 mL SAVE 20% $ 100 / 1 x 1 mL 10 comps. 1,2,4-Trimethylbenzene 2,2,4-Trimethylpentane o-Xylene m-Xylene p-Xylene LUFT/LUST Regular unleaded gasoline Hexadecane Extraction Volatiles CLP-BTEX CLP-BTEX-PAK 0.2 mg/mL each in MeOH $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 6 comps. CLP-BTEX-10X CLP-BTEX-10X-PAK 2.0 mg/mL each in MeOH $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 6 comps. Benzene Ethyl benzene Toluene 94 o-Xylene m-Xylene p-Xylene Wisconsin DNR - Gasoline Range Hydrocarbons GRH-003S GRH-003S-PAK 2.0 mg/mL each in MeOH Benzene Ethylbenzene MtBE Naphthalene Toluene $ 35 / 1 x 1 mL SAVE 20% $ 140 / 5 x 1 mL 10 comps. 1,2,4-Trimethylbenzene 1,3,5-Trimethylbenzene o-Xylene m-Xylene p-Xylene Quality System is Certified to comply with the International ISO 9001 Quality Standard LUFT/LUST Standards LUFT/LUST DRH Diesel Range Diesel Range Hydrocarbon Analysis Complete Hydrocarbon Analysis EPA Method - Diesel Range Hydrocarbons Multi-State Hydrocarbon Window Defining Standard DRH-001S 0.2 mg/mL each in CH2Cl2 : Hexane (1:1) $ 20 / 1 x 1 mL 10 comps. DRH-001S-10X 2.0 mg/mL each in CH2Cl2 : Hexane (1:1) $ 30 / 1 x 1 mL 10 comps. DRH-008S-R2 DRH-008S-R2-PAK 500 µg/mL each in Chloroform n-Decane C10 n-Hexadecane C16 n-Docosane C22 n-Hexacosane C26 n-Dodecane C12 n-Octadecane C18 n-Tetracosane C24 n-Octacosane C28 n-Tetradecane C14 n-Eicosane C20 Surrogate Standard GRH-SS GRH-SS-PAK 2.0 mg/mL in Acetone $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL Octane Nonane Decane Undecane Dodecane Tridecane Tetradecane Pentadecane Hexadecane Heptadecane Pristane Octadecane Phytane Nonadecane Eicosane Heneicosane Docosane Tricosane Internal Standard GRH-IS GRH-IS-PAK 1.0 mg/mL in CH2Cl2 $ 15 / 1 x 1 mL SAVE 20% $ 60 / 5 x 1 mL 5-alpha Androstane Calibration/Window Defining Hydrocarbon Standard DRH-004S-5X 1.0 mg/mL each in CH2Cl2 : CS2 (1:1) C8 C10 C12 C14 Hexadecane Octadecane Eicosane Docosane C16 C18 C20 C22 Tetracosane Hexacosane Octacosane Triacontane C24 C26 C28 C30 $ 50 / 1 x 1 mL 17 comps. Dotriacontane C32 Tetratriacontane C34 Hexatriacontane C36 Octatriacontane C38 Tetracontane C40 Surrogate Standard DRH-SS DRH-SS-PAK 5.0 mg/mL in THF $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL n-Triacontane-d62 D-2887 Tritriacontane Tetratriacontane Pentatriacontane Hexatriacontane Heptatriacontane Octatriacontane Nonatriacontane Tetracontane AccuStandard offers a hydrocarbon window defining standard with the C8 to C40 odd and even Alkanes. Use of this one standard should meet the numerous State to State variations for hydrocarbon validation and reporting. As an added benefit AccuStandard included pristane and phytane in the formulation. Again, use of this one standard can meet numerous LUFT/LUST programs requiring that the C17/ pristane and C18/ phytane ratio be used to estimate subsurface degradation of fuel oil spills. If you prefer, AccuStandard has also developed a fuel oil degradation mixture containing just the four required analytes to determine the C17/pristane and C18/ phytane ratio. Cat. No. DRH-005S-10X Fuel Oil Degradation/Retention Time Mixture for quantification of C17/Pristane and C18/Phytane ratios DRH-005S-10X 2.0 mg/mL each in CH2Cl2 : CS2 (1:1) Heptadecane Octadecane $ 20 / 1 x 1 mL 4 comps. Phytane (2,6,10,14-Tetramethylhexadecane) Pristane (2,6,10,14-Tetramethylpentadecane) Hydrocarbon Window Defining Standard Set DRH-FTRPH-SET DRH-FTRPH-SET-PAK 500 µg/mL each in Hexane Calibration Solution Calibration Solution DRH-002S At stated conc. in CS2 Hexane (600 µg/mL) Heptane (600 µg/mL) Octane (800 µg/mL) Nonane (800 µg/mL) Decane (1,200 µg/mL) Undecane (1,200 µg/mL) Tetracosane Pentacosane Hexacosane Heptacosane Octacosane Nonacosane Triacontane n-Hentriacontane Dotriacontane Technical Note o-Terphenyl (OTP) Octane Decane Dodecane Tetradecane $ 65 / 1 x 1 mL SAVE 20% $ 260 / 5 x 1 mL 35 comps. $ 45 / 1 x 1 mL 17 comps. Dodecane (1,200 µg/mL) Tetradecane (1,200 µg/mL) Hexadecane (1,000 µg/mL) Octadecane (500 µg/mL) Eicosane (200 µg/mL) Tetracosane (200 µg/mL) Octacosane Dotriacontane Hexatriacontane Tetracontane Tetratetracontane (100 µg/mL) (100 µg/mL) (100 µg/mL) (100 µg/mL) (100 µg/mL) ASTM-D2887 1% v/v in n-Octane $ 10 / 1 x 1 mL 2 comps. n-Hexadecane n-Octadecane Wisconsin Diesel Range Hydrocarbons DRH-003S 0.2 mg/mL each in Hexane n-Decane C10 n-Tetradecane n-Undecane C11 n-Pentadecane n-Dodecane C12 n-Hexadecane n-Tridecane C13 n-Heptadecane C14 C15 C16 C17 $ 20 / 1 x 1 mL 11 comps. n-Octadecane C18 n-Nonadecane C19 n-Eicosane C20 FTRPH Calibration/Window Defining Standard DRH-FTRPH DRH-FTRPH-PAK 500 µg/mL each in Hexane n-Octane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Eicosane n-Docosane n-Tetracosane n-Hexacosane $ 35 / 1 x 1 mL SAVE 15% $ 150 / 5 x 1 mL 17 comps. n-Octacosane n-Hexatriacontane n-Triacontane n-Octatriacontane n-Dotriacontane n-Tetracontane n-Tetratriacontane Hydrocarbon Window Defining Standard DRH-FTRPH2 DRH-FTRPH2-PAK 500 µg/mL each in Hexane n-Nonane n-Undecane n-Tridecane n-Pentadecane n-Heptadecane Pristane Phytane n-Nonadecane n-Heneicosane n-Tricosane $ 45 / 1 x 1 mL SAVE 20% $ 180 / 5 x 1 mL 18 comps. n-Pentacosane n-Heptacosane n-Nonacosane n-Hentriacontane Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com n-Tritriacontane n-Pentatriacontane n-Heptatriacontane n-Nonatriacontane 95 LUFT/LUST Column Test Mixture $ 80 / 2 x 1 mL SAVE 20% $ 320 / 5 (2 x 1 mL) LUFT/LUST PT LUFT/LUST Proficiency Test Samples QC Suffix Key "AS" = Formal PT Study "AT" = Pre-Test, Quick TAT "AV" = Values Included Petro PT Samples New PT Samples Gasoline & Diesel The new Gasoline PT sample allows laboratories to test for gasoline TPH. This sample can also be used to test for the BTEX concentrations so the lab can use this product for method 602, 8020, 8021 and 8015 modified. The sample can also be used to reduce analytical bias by using the recommended calibration standard listed with the PT sample when conducting PT studies. AccuStandard is the one ISO 9001 standard manufacturer capable of supplying not only the PT sample(s), but also a wide variety of calibration standards to meet your specific TPH Method requirement. Oxygenate PT Sample With MtBE contamination problems in drinking water, numerous states are now requiring certification for Oxygenate monitoring. Join AccuStandard’s next study for Oxygenate analysis. Our timely PT schedule easily allows your lab to be proactive in new regulatory requirements. The analytes in the standard and the PT sample have been drawn from the California list of known prevalent oxygenates in gasoline. These new Oxygenate PT samples and standards allow your Lab to: • • • • Expand testing capabilities Generate new testing revenue Eliminate standard preparation Easily combine with other AccuStandard Volatile standards. * * * ETBE Diisopropylether * * * IPE-OILG-001-AS IPE-OILG-001-AT IPE-OILG-001-AV Sample conc. after prep Contains 2 analytes listed below Analyte List Total Oil & Grease † TPH $ 32 / 5 mL $ 32 / 5 mL $ 32 / 5 mL Sample range 5-100 mg/L 5-100 mg/L Technical Note WS-PT Oxygenates OPE-OXY-001-AS OPE-OXY-001-AT OPE-OXY-001-AV Sample conc. after prep 5.0-50 µg/L Contains 4 analytes listed below WP-PT Oil, Grease & TPH $ 47 / 2 mL $ 47 / 2 mL $ 47 / 2 mL This PT sample can be used by gravimetric oil and grease methods. In addition, it can also be used for TPH analysis by gravimetric methods including the EPA method 1664. The sample contains real world material commonly found at petroleum containment sites. Suggested Calibration Standard Oil and Grease MTBE TAME WC-OILG-10X-1 1000 µg/mL Total Oil and Grease in n-Propanol $ 45 / 100 mL Contains 500 µg/mL vegetable oil and 500 µg/mL of petroleum oil. Shake well before use. Suggested Calibration Standard Oxygenate Gasoline Additive Standard OGAD-001 OGAD-001-PAK At stated conc. in MeOH MtBE ETBE Isopropyl ether NEW $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 5 comps. TAME t-Butanol (2000 µg/mL) (2000 µg/mL) (2000 µg/mL) (2000 µg/mL) (10000 µg/mL) * Designed for NELAC/CA † indicates these are included in the NVLAP Scope of Accreditation †† indicates kits. See individual Cat. No.s for Accreditation status of analytes LUFT/LUST Lab Code 200389-0 96 Quality System is Certified to comply with the International ISO 9001 Quality Standard Method LUFT/LUST Standards 1664 413 & 418 8440 Oil, Grease & TPH Method 1664 Oil, Grease & Total Petroleum Hydrocarbon Determination Precision and Recovery (PAR) Spiking Solution M-1664-5ML M-1664-5ML-PAK 4.0 mg/mL each in Acetone $ 15 / 1 x 5 mL SAVE 20% $ 60 / 5 x 5 mL 2 comps. M-1664-20ML M-1664-20ML-PAK 4.0 mg/mL each in Acetone $ 25 / 1 x 20 mL SAVE 20% $ 100 / 5 x 20 mL 2 comps. Hexadecane Stearic acid Method 413.2 & 418.1 M-418-CON % by volume Oil, Grease and Petroleum Hydrocarbon Total Recoverable (IR Method) $ 35 / 1 x 1 mL 3 comps. Method 8440 (25.0) (37.5) AccuStandard's Precison and Recovery (PAR) Spiking Solution was developed for the new Method 1664. This performance based method was developed to replace previous gravimetric procedures which incorporated Freon-113 as the extraction solvent for the determination of Oil and Grease and Total Petroleum Hydrocarbons. Each standard is packaged in a flame sealed ampule conveniently sized for quality control of the analytical batch. Total Petroleum Hydrocarbon Analysis by IR Oil, Grease & Petroleum Hydrocarbon Concentrates Mix Chlorobenzene Isooctane Technical Note Hexadecane (37.5) M-418 $ 30 / 1 x 1 mL M-418-PAK SAVE 20% $ 120 / 5 x 1 mL Total 4.15 mg/mL in Freon 113, (Parts by volume) 3 comps. Chlorobenzene n-Hexadecane (10.0) (15.0) Isooctane (15.0) Total Petroleum Hydrocarbon Analysis Total Recoverable Petroleum Hydrocarbon Mix Total Petroleum Hydrocarbon Concentrate Mix M-8440 M-8440-PAK At stated conc. in Tetrachloroethene M-8440-CON M-8440-CON-PAK Chlorobenzene n-Hexadecane (0.10 w/w %) (0.15 w/w %) $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 3 comps. Isooctane (0.15 w/w %) Chlorobenzene n-Hexadecane $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 3 comps. (25.0 vol %) (37.5 vol %) Isooctane (37.5 vol %) Silica Gel Cleanup Calibration Solution M-8440-SGC M-8440-SGC-PAK 10.0 mg/mL in Tetrachloroethene $ 10 / 1 x 1 mL SAVE 20% $ 40 / 5 x 1 mL Corn Oil Total Petroleum Hydrocarbon Pattern Recognition Standards Leaking Underground Storage Tank Retention Time Standard This product can be used to screen a sample to determine what type of petroleum spill that may have caused the contamination. NEW Retention Time Standard n-Hexane n-Decane n-Dodecane $ 20 / 1 x 1 mL SAVE 20% $ 80 / 5 x 1 mL 7 comps. n-Tetracosane n-Octacosane n-Triacontane n-Tetracontane Technical Note A sample showing peaks in the C6-C10 range generally indicates a gasoline spill. Samples with the peaks in the C24C12 range are indicative of a diesel spill while samples with the higher carbon numbers above C24 are typically oils or lubricants. Once the initial screen is complete, more detailed work can be done to further identify the contaminant. Fax 203-786-5287 • Toll Free 800-442-5290 / 203-786-5290 • Website www.accustandard.com 97 LUFT/LUST DRH-010S DRH-010S-PAK 25 µg/mL each in CH2Cl2 This book contains chromatography for the various petroleum products typically found during LUFT/LUST site investigations. The chromatography shows each fuel pattern in a 25 minute analytical run for early eluting petroleum products like gasoline to late eluting products like motor oil. In addition, an n-alkane standard (DRH-008S) analyzed under identical conditions has been overlaid on each petroleum product chromatogram. Use of the book will assist the chemist’s identification of the fuel for pattern recognition. The n-alkane standard (DRH-008S) overlay provides n-alkane reference points between the standard and the unknown sample. These beginning and ending n-alkane reference points can be used to establish gross hydrocarbon concentrations. By comparing the specific n-alkane range of the closest identified petroleum standard to that of the unknown sample a reproducible gross hydrocarbon number can be achieved. To Order, BOOK-TPH $ 35 LUFT/LUST Standards Automotive Engine Exhaust, Refinery Waste (Skinner List) Alcohol Oxidation Products in Automotive Engine Exhaust by HPLC of DNPH derivatives The California Air Resources Board, in conjunction with some of the larger automobile manufacturers, has developed an HPLC method in which the 2,4-Dinitrophenylhydrazine derivatives of the by-products are quantitated. Method 1004 Carbonyl Compounds as DNPH deriv. by HPLC Skinner List for Refinery Waste Carbonyl Compounds as DNPH deriv. by HPLC California Air Resources Board Method 1004 Base/Neutral Extractables M-1004 At stated conc. in AcCN $ 25 / 1 x 1 mL 13 comps. M-005B M-005B-PAK M-1004-10X At 10 times the stated conc. in AcCN $ 35 / 1 x 1 mL 13 comps. $ 200 / 1 x 1 mL M-005B-10X 2.0 mg/mL each in CH2Cl2 M-005B-10X-PAK 2.0 mg/mL each in CH2Cl2 SAVE 20% $ 1,000 / 5 x 1 mL 27 comps. Carbonyl Compound Acetaldehyde Acetone Acrolein Benzaldehyde 2-Butanone (MEK) n-Butyraldehyde Crotonaldehyde Formaldehyde Hexanal Methacrolein Propionaldehyde m-Tolualdehyde Valeraldehyde (3.0 (3.0 (3.0 (3.0 (3.0 (3.0 (3.0 (3.0 (3.0 (3.0 (3.0 (3.0 (3.0 µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) CAR-DNPH At stated conc. in AcCN as DNPH derivatives Acetaldehyde Acetone Acrolein Benzaldehyde (1000 (500 (500 (500 µg/mL) µg/mL) µg/mL) µg/mL) 0.2 mg/mL each in CH2Cl2 0.2 mg/mL each in CH2Cl2 (15.3 (12.3 (12.7 (8.1 (10.5 (10.5 (10.7 (21.0 (8.4 (10.7 (12.3 (7.5 (9.3 µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) µg/mL) $ 20 / 1 x 1 mL 7 comps. Reference Gas Oil Sample $ 20 / 1 x 1 mL Anthracene Benzo[a]anthracene Benzo[b]fluoranthene Benzo[k]fluoranthene Benzo[a]pyrene bis(2-Ethylhexyl)phthalate Butyl benzyl phthalate Chrysene Dibenz[a,h]acridine Dibenz[a,h]anthracene o-Dichlorobenzene m-Dichlorobenzene p-Dichlorobenzene Diethyl phthalate M-005A M-005A-PAK 0.2 mg/mL each in CH2Cl2 0.2 mg/mL each in CH2Cl2 o-Cresol m-Cresol p-Cresol 2,4-Dimethylphenol 2,4-Dinitrophenol LUFT/LUST $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 8 comps. 4-Nitrophenol Phenol Thiophenol Volatiles Resolution Check Mix for Fire Debris Analysis ASTM-E1387 ASTM-E1387-PAK 2.0 mg/mL each in CH2Cl2 ASTM E-1618 $ 35 / 1 x 1 mL SAVE 20% $ 140 / 5 x 1 mL M-005A-10X 2.0 mg/mL each in CH2Cl2 M-005A-10X-PAK 2.0 mg/mL each in CH2Cl2 M-005V M-005V-PAK 0.2 mg/mL each in MeOH 0.2 mg/mL each in MeOH $ 35 / 1 x 1 mL SAVE 20% $ 140 / 5 x 1 mL M-005V-10X M-005V-10X-PAK 2.0 mg/mL each in MeOH 2.0 mg/mL each in MeOH $ 40 / 1 x 1 mL SAVE 20% $ 160 / 5 x 1 mL 14 comps. Resolution Check Mix Decane Dodecane Eicosane 2-Ethyltoluene 3-Ethyltoluene 7,12-Dimethylbenz[a]anthracene Dimethyl phthalate Di-n-butyl phthalate Di-n-octyl phthalate Indene Fluoranthene 6-Methylchrysene 1-Methylnaphthalene Naphthalene Phenanthrene Pyrene Pyridine Quinoline Acid Extractables Hydrocarbon Mixture (boiling point range 250-850 °F) ASTM E-1387 $ 150 / 1 x 1 mL SAVE 20% $ 600 / 5 x 1 mL DNPH Derivative Butyraldehyde (500 µg/mL) Formaldehyde (1500 µg/mL) Propionaldehyde (500µg/mL) RGS-001 Semi-Volatiles $ 30 / 1 x 1 mL SAVE 20% $ 120 / 5 x 1 mL 13 comps. Hexadecane Hexane Octadecane Octane Tetradecane Toluene 1,2,4-Trimethylbenzene p-Xylene Benzene Carbon disulfide Chlorobenzene Chloroform 1,2-Dichloroethane 1,4-Dioxane Ethyl benzene Ethylene dibromide Methyl ethyl ketone Styrene Toluene o-Xylene m-Xylene p-Xylene Resolution Check Mix for Fire Debris Analysis Test Mix for Fire Debris Analysis ASTM-E1618 ASTM-E1618-PAK 0.05% v/v (0.50 µL/mL) each in CH2Cl2 n-Decane n-Dodecane n-Eicosane o-Ethyltoluene m-Ethyltoluene 98 n-Hexadecane n-Hexane n-Octadecane n-Octane $ 35 / 1 x 1 mL SAVE 20% $ 140 / 5 x 1 mL 13 comps. n-Tetradecane Toluene 1,2,4-Trimethylbenzene p-Xylene Quality System is Certified to comply with the International ISO 9001 Quality Standard Catalog Number Index 73 73 26 73 73 26 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 26 73 73 26 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 73 AA22H-1 AA22H-10X-20ML AA22H-25X-20ML AA22H-5 AA23N-1 AA23N-10X-20ML AA23N-25X-20ML AA23N-5 AA24N-1 AA24N-10X-20ML AA24N-25X-20ML AA24N-5 AA25N-1 AA25N-10X-20ML AA25N-25X-20ML AA25N-5 AA26H-1 AA26H-10X-20ML AA26H-5 AA27N-1 AA27N-5 AA27N-1 AA27N-10X-20ML AA27N-25X-20ML AA27N-5 AA28N-1 AA28N-10X-20ML AA28N-25X-20ML AA28N-5 AA29N-1 AA29N-10X-20ML AA29N-25X-20ML AA29N-5 AA30N-1 AA30N-5 AA30N-10X-20ML AA30N-25X-20ML AA31N-1 AA31N-10X-20ML AA31N-25X-20ML AA31N-5 AA32N-1 AA32N-5 AA32N-10X-20ML AA32N-25X-20ML AA33N-1 AA33N-5 AA33N-10X-20ML AA33N-25X-20ML AA34N-1 AA34N-10X-20ML AA34N-25X-20ML AA34N-5 AA35W-1 AA35W-10X-20ML AA35W-25X-20ML AA35W-5 AA36N-1 AA36N-10X-20ML AA36N-25X-20ML AA36N-5 AA37N-1 AA37N-1 AA37N-10X-20ML AA37N-25X-20ML AA37N-5 AA37N-5 AA38W-1 AA38W-10X-20ML AA38W-25X-20ML AA38W-5 AA40H-1 AA40H-10X-20ML AA40H-25X-20ML AA40H-5 AA41W-1 AA41W-10X-20ML AA41W-5 73 73 73 73 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 26 74 74 26 74 74 74 74 74 74 74 74 17, 74 17, 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 26 74 74 74 26 74 74 74 74 74 74 74 74 74 74 74 74 AA42H-1 AA42H-10X-20ML AA42H-25X-20ML AA42H-5 AA43N-1 AA43N-5 AA43N-10X-20ML AA43N-25X-20ML AA44N-1 AA44N-10X-20ML AA44N-25X-20ML AA44N-5 AA45W-1 AA45W-10X-20ML AA45W-25X-20ML AA45W-5 AA46H-1 AA46H-10X-20ML AA46H-25X-20ML AA46H-5 AA47N-1 AA47N-10X-20ML AA47N-25X-20ML AA47N-5 AA48H-1 AA48H-10X-20ML AA48H-25X-20ML AA48H-5 AA49N-1 AA49N-10X-20ML AA49N-25X-20ML AA49N-5 AA50N-1 AA50N-10X-20ML AA50N-25X-20ML AA50N-5 AA51N-1 AA51N-10X-20ML AA51N-25X-20ML AA51N-5 AA52W-1 AA-52W-10X-20ML AA52W-5 AA53N-1 AA53N-10X-20ML AA53N-25X-20ML AA53N-5 AA54N-1 AA54N-5 AA54N-1 AA54N-10X-20ML AA54N-25X-20ML AA54N-5 AA55N-1 AA55N-10X-20ML AA55N-25X-20ML AA55N-5 AA56W-1 AA56W-10X-20ML AA56W-25X-20ML AA56W-5 AA57W-1 AA57W-10X-20ML AA57W-25X-20ML AA57W-5 AA58H-1 AA58H-10X-20ML AA59N-1 AA59N-10X-20ML AA59N-25X-20ML AA59N-5 AA60N-1 AA60N-10X-20ML AA60N-25X-20ML AA60N-5 AA61N-1 AA61N-5 AA62N-1 26, 26, 17, 17, 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 74 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 26 75 75 26 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 AA62N-10X-20ML AA62N-25X-20ML AA62N-5 AA63H-1 AA63H-5 AA63N-10X-20ML AA63N-25X-20ML AA64W-1 AA64W-10X-20ML AA64W-5 AA65W-1 AA65W-10X-20ML AA65W-5 AA66N-1 AA66N-5 AA67N-1 26, AA67N-10X-20ML AA67N-25X-20ML AA67N-5 26, AA68N-1 AA68N-10X-20ML AA68N-25X-20ML AA68N-5 AA69N-1 AA69N-10X-20ML AA69N-25X-20ML AA69N-5 AA70N-1 AA70N-10X-20ML AA70N-25X-20ML AA70N-5 AA71N-1 AA71N-10X-20ML AA71N-25X-20ML AA71N-5 AK-101.0-GCS AK-101.0-GCS-BTEX 82, AK-101.0-GCS-PAK AK-101.0-IS-10X AK-101.0-IS-10X-PAK AK-101.0-LCS AK-101.0-LCS-PAK AK-101.0-NAS-10X AK-101.0-NAS-10X-PAK AK-101.0-SS AK-101.0-SS-100X AK-101.0-SS-100X-PAK AK-101.0-SS-10X AK-101.0-SS-10X-PAK AK-101.0-SS-PAK AK-101AA-ARO AK-101AA-ARO-PAK AK-101-GSC-R1 AK-101-GSC-R1-PAK AK-102.0-DCS AK-102.0-DCS-10X AK-102.0-DCS-10X-PAK AK-102.0-DCS-PAK AK-102.0-DCS-R1-10X AK-102.0-DCS-R1-10X-PAK AK-102.0-IS AK-102.0-IS-PAK AK-102.0-LCS AK-102.0-LCS-10X AK-102.0-LCS-10X-PAK AK-102.0-LCS-PAK AK-102.0-LCS-R1-10X AK-102.0-LCS-R1-10X-PAK AK-102.0-NAS-10X 83, AK-102.0-NAS-10X-PAK 83, AK-102.0-SS AK-102.0-SS-10X 83, AK-102.0-SS-10X-PAK 83, AK-102.0-SS-PAK AK-102/103AA-RT AK-102/103AA-RT-PAK AK-102/103AA-SS AK-102/103AA-SS-PAK 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 75 82 90 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 82 83 83 83 83 83 83 83 83 83 83 83 83 83 83 86 86 83 85 85 83 84 84 84 84 AK-102AA-DRO 84 AK-102AA-DRO-PAK 84 AK-103.0-LCS 84 AK-103.0-LCS-5X 84 AK-103.0-LCS-5X-PAK 84 AK-103.0-LCS-PAK 84 AK-103.0-RCS 84 AK-103.0-RCS-PAK 84 AK-103.0-SS-PAK 84 AK-103AA-RRO 84 AK-103AA-RRO-PAK 84 ASTM-D2887 14 ASTM-D2887 95 ASTM-D3710 20 ASTM-D3710-PAK 20 ASTM-E1387 98 ASTM-E1387-PAK 98 ASTM-E1618 98 ASTM-E1618-PAK 98 ASTM-FUEL-QCS-01-PAK 1,40 ASTM-FUEL-QCS-02-PAK 1,40 ASTM-P-0010-PAK 11 ASTM-P-0020-PAK 11 ASTM-P-0030 12,13 ASTM-P-0031 13 ASTM-P-0032 13 ASTM-P-0033 13 ASTM-P-0034 13 ASTM-P-0035 13 ASTM-P-0036 12 ASTM-P-0037 12 ASTM-P-0038 14 ASTM-P-0050 15 ASTM-P-0051N-2G 56 ASTM-P-0051N-2G 15 ASTM-P-0052 15 ASTM-P-0052-PAK 15 ASTM-P-0053N-2G 56 ASTM-P-0053N-2G 15 ASTM-P-0061-SET 37 ASTM-P-0062-SET 37 ASTM-P-0063-SET 37 ASTM-P-0064-SET 37 ASTM-P-0065-SET 37 ASTM-P-0066-SET 37 ASTM-P-0067-SET 37 ASTM-P-0068-SET 37 ASTM-P-0069-SET 37 ASTM-P-0070-10X 23, 40 ASTM-P-0070-1X 23, 40 ASTM-P-0070-20X 23, 40 ASTM-P-0070-2X 23, 40 ASTM-P-0070-4X 23, 40 ASTM-P-0070-BL 23, 40 ASTM-P-0070-SET 23, 40 ASTM-P-0071-01 23, 40 ASTM-P-0071-02 23, 40 ASTM-P-0071-03 23, 40 ASTM-P-0071-BL 23, 40 ASTM-P-0071-SET 23, 40 ASTM-P-0080 55 ASTM-P-0080-PAK 55 ASTM-P-0081 55 ASTM-P-0081-PAK 55 ASTM-P-0082 55 ASTM-P-0082-PAK 55 ASTM-P-0082-R1 55 ASTM-P-0082-R1-PAK 55 ASTM-P-0090-01 66 ASTM-P-0090-02 66 ASTM-P-0090-03 66 ASTM-P-0090-04 66 ASTM-P-0090-05 66 ASTM-P-0090-06 66 ASTM-P-0090-07 66 ASTM-P-0090-08 66 ASTM-P-0090-09 66 ASTM-P-0090-10 66 INDEX AA01N-1 AA01N-5 AA01N-1 AA01N-10X-20ML AA01N-25X-20ML AA01N-5 AA02N-1 AA02N-5 AA02W-10X-20ML AA03N-10X-20ML AA03N-25X-20ML AA03N-1 AA03N-5 AA04N-1 AA04N-5 AA04N-10X-20ML AA04N-25X-20ML AA05N-1 AA05N-10X-20ML AA05N-5 AA06N-1 AA06N-10X-20ML AA06N-25X-20ML AA06N-5 AA07W-1 AA07W-10X-20ML AA07W-5 AA08N-1 AA08N-5 AA08N-10X-20ML AA08N-25X-20ML AA09N-1 AA09N-5 AA09N-1 AA09N-10X-20ML AA09N-25X-20ML AA09N-5 AA11N-1 AA11N-10X-20ML AA11N-25X-20ML AA11N-5 AA12N-1 AA12N-10X-20ML AA12N-25X-20ML AA12N-5 AA13N-1 AA13N-5 AA13N-10X-20ML AA13N-25X-20ML AA14N-1 AA14N-5 AA14N-10X-20ML AA14N-25X-20ML AA15N-1 AA15N-10X-20ML AA15N-25X-20ML AA15N-5 AA16N-1 AA16N-10X-20ML AA16N-25X-20ML AA16N-5 AA17N-1 AA17N-10X-20ML AA17N-25X-20ML AA18N-1 AA18N-10X-20ML AA18N-25X-20ML AA18N-5 AA19N-1 AA19N-10X-20ML AA19N-25X-20ML AA19N-5 AA20N-1 AA20N-10X-20ML AA20N-5 AA21W-1 AA21W-10X-20ML AA21W-5 i INDEX ii ASTM-P-0090-11 ASTM-P-0090-12 ASTM-P-0090-13 ASTM-P-0090-14 ASTM-P-0090-15 ASTM-P-0090-16 ASTM-P-0090-SET ASTM-P-0091-01-10X ASTM-P-0091-02-10X ASTM-P-0091-03-10X ASTM-P-0091-04-10X ASTM-P-0091-05-10X ASTM-P-0091-06-10X ASTM-P-0091-07-10X ASTM-P-0091-08-10X ASTM-P-0091-09-10X ASTM-P-0091-10-10X ASTM-P-0091-10X-SET ASTM-P-0091-11-10X ASTM-P-0091-12-10X ASTM-P-0091-13-10X ASTM-P-0091-14-10X ASTM-P-0091-15-10X ASTM-P-0091-16-10X ASTM-P-0091-17-10X ASTM-P-0091-18-10X ASTM-P-0091-19-10X ASTM-P-0091-20-10X ASTM-P-0091-21-10X ASTM-P-0091-22-10X ASTM-P-0092-0.1X ASTM-P-0092-100X ASTM-P-0092-10X ASTM-P-0092-1X ASTM-P-0092-500X ASTM-P-0092-5X ASTM-P-0092-BL ASTM-P-0092-SET ASTM-P-0100-01 ASTM-P-0100-02 ASTM-P-0100-03 ASTM-P-0100-04 ASTM-P-0100-05 ASTM-P-0100-06 ASTM-P-0100-07 ASTM-P-0100-08 ASTM-P-0100-09 ASTM-P-0100-10 ASTM-P-0100-11 ASTM-P-0100-12 ASTM-P-0100-SET ASTM-P-0101-01 ASTM-P-0101-02 ASTM-P-0101-03 ASTM-P-0101-04 ASTM-P-0101-05 ASTM-P-0101-06 ASTM-P-0101-07 ASTM-P-0101-08 ASTM-P-0101-09 ASTM-P-0101-10 ASTM-P-0101-11 ASTM-P-0101-12 ASTM-P-0102-01 ASTM-P-0102-02 ASTM-P-0102-03 ASTM-P-0102-04 ASTM-P-0102-05 ASTM-P-0102-06 ASTM-P-0102-07 ASTM-P-0102-08 ASTM-P-0102-09 ASTM-P-0102-10 ASTM-P-0102-11 ASTM-P-0102-12 ASTM-P-0102-SET ASTM-P-0102-SET ASTM-P-0103-01 ASTM-P-0103-01 ASTM-P-0103-02 ASTM-P-0103-02 ASTM-P-0103-03 ASTM-P-0103-03 ASTM-P-0103-04 ASTM-P-0103-04 ASTM-P-0103-05 ASTM-P-0103-05 ASTM-P-0103-06 ASTM-P-0103-06 ASTM-P-0103-07 66 66 66 66 66 66 66 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 38 66 66 66 66 66 66 66 66 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 39 62 39 62 39 62 39 62 39 62 39 62 39 62 39 ASTM-P-0103-07 ASTM-P-0103-08 ASTM-P-0103-08 ASTM-P-0103-09 ASTM-P-0103-09 ASTM-P-0103-10 ASTM-P-0103-10 ASTM-P-0103-11 ASTM-P-0103-11 ASTM-P-0103-12 ASTM-P-0103-12 ASTM-P-0103-SET ASTM-P-0103-SET ASTM-P-0104-01 ASTM-P-0104-02 ASTM-P-0104-03 ASTM-P-0104-04 ASTM-P-0104-05 ASTM-P-0104-06 ASTM-P-0104-07 ASTM-P-0104-08 ASTM-P-0104-09 ASTM-P-0105-01 ASTM-P-0105-02 ASTM-P-0105-03 ASTM-P-0105-04 ASTM-P-0105-05 ASTM-P-0105-06 ASTM-P-0105-07 ASTM-P-0106-01 ASTM-P-0106-02 ASTM-P-0106-03 ASTM-P-0106-04 ASTM-P-0106-05 ASTM-P-0106-06 ASTM-P-0106-07 ASTM-P-0107-5 ASTM-P-0108-01 ASTM-P-0108-02 ASTM-P-0108-03 ASTM-P-0108-04 ASTM-P-0108-05 ASTM-P-0108-06 ASTM-P-0108-07 ASTM-P-0108-08 ASTM-P-0108-09 ASTM-P-0108-10 ASTM-P-0108-11 ASTM-P-0108-12 ASTM-P-0108-13 ASTM-P-0108-14 ASTM-P-0108-15 ASTM-P-0108-16 ASTM-P-0108-17 ASTM-P-0108-SET ASTM-P-0109-01 ASTM-P-0109-02 ASTM-P-0109-03 ASTM-P-0109-04 ASTM-P-0109-05 ASTM-P-0109-06 ASTM-P-0109-07 ASTM-P-0109-08 ASTM-P-0109-09 ASTM-P-0109-10 ASTM-P-0109-11 ASTM-P-0109-12 ASTM-P-0109-13 ASTM-P-0109-14 ASTM-P-0109-15 ASTM-P-0109-16 ASTM-P-0109-17 ASTM-P-0109-SET ASTM-P-0110-01 ASTM-P-0110-02 ASTM-P-0110-03 ASTM-P-0110-04 ASTM-P-0110-05 ASTM-P-0110-06 ASTM-P-0110-07 ASTM-P-0110-08 ASTM-P-0110-09 ASTM-P-0110-10 ASTM-P-0110-11 ASTM-P-0110-12 ASTM-P-0110-13 ASTM-P-0110-14 ASTM-P-0110-15 ASTM-P-0110-16 ASTM-P-0110-17 62 39 62 39 62 39 62 39 62 39 62 39 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 62 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 ASTM-P-0110-SET ASTM-P-0110-SET ASTM-P-0111-01 ASTM-P-0111-02 ASTM-P-0111-03 ASTM-P-0111-04 ASTM-P-0111-05 ASTM-P-0111-06 ASTM-P-0111-07 ASTM-P-0111-08 ASTM-P-0111-09 ASTM-P-0111-10 ASTM-P-0111-11 ASTM-P-0111-12 ASTM-P-0111-13 ASTM-P-0111-14 ASTM-P-0111-15 ASTM-P-0111-16 ASTM-P-0111-17 ASTM-P-0111-SET ASTM-P-0112-01 ASTM-P-0112-02 ASTM-P-0112-03 ASTM-P-0112-04 ASTM-P-0112-05 ASTM-P-0112-06 ASTM-P-0112-07 ASTM-P-0112-08 ASTM-P-0112-09 ASTM-P-0112-10 ASTM-P-0112-11 ASTM-P-0112-12 ASTM-P-0112-13 ASTM-P-0112-14 ASTM-P-0112-15 ASTM-P-0112-16 ASTM-P-0112-17 ASTM-P-0112-SET ASTM-P-0113-01 ASTM-P-0113-02 ASTM-P-0113-03 ASTM-P-0113-04 ASTM-P-0113-05 ASTM-P-0113-06 ASTM-P-0113-07 ASTM-P-0113-08 ASTM-P-0113-09 ASTM-P-0113-10 ASTM-P-0113-11 ASTM-P-0113-12 ASTM-P-0113-13 ASTM-P-0113-14 ASTM-P-0113-15 ASTM-P-0113-16 ASTM-P-0113-17 ASTM-P-0113-SET ASTM-P-0114-01 ASTM-P-0114-02 ASTM-P-0114-03 ASTM-P-0114-04 ASTM-P-0114-05 ASTM-P-0114-06 ASTM-P-0114-07 ASTM-P-0114-08 ASTM-P-0114-09 ASTM-P-0114-10 ASTM-P-0114-11 ASTM-P-0114-12 ASTM-P-0114-13 ASTM-P-0114-14 ASTM-P-0114-15 ASTM-P-0114-16 ASTM-P-0114-17 ASTM-P-0114-SET ASTM-P-0115-01 ASTM-P-0115-02 ASTM-P-0115-03 ASTM-P-0115-04 ASTM-P-0115-05 ASTM-P-0115-06 ASTM-P-0115-07 ASTM-P-0115-08 ASTM-P-0115-09 ASTM-P-0115-10 ASTM-P-0115-11 ASTM-P-0115-12 ASTM-P-0115-13 ASTM-P-0115-14 ASTM-P-0115-15 ASTM-P-0115-16 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 22, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 58, 25 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 63 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 64 ASTM-P-0115-17 ASTM-P-0115-SET ASTM-P-0116-01 ASTM-P-0116-02 ASTM-P-0116-03 ASTM-P-0116-04 ASTM-P-0116-05 ASTM-P-0116-06 ASTM-P-0116-07 ASTM-P-0116-08 ASTM-P-0116-09 ASTM-P-0116-10 ASTM-P-0116-11 ASTM-P-0116-SET ASTM-P-0117-01 ASTM-P-0117-01 ASTM-P-0117-02 ASTM-P-0117-02 ASTM-P-0117-03 ASTM-P-0117-03 ASTM-P-0117-04 ASTM-P-0117-04 ASTM-P-0117-05 ASTM-P-0117-05 ASTM-P-0117-06 ASTM-P-0117-06 ASTM-P-0117-07 ASTM-P-0117-07 ASTM-P-0117-08 ASTM-P-0117-08 ASTM-P-0117-09 ASTM-P-0117-09 ASTM-P-0117-10 ASTM-P-0117-10 ASTM-P-0117-SET ASTM-P-0117-SET ASTM-P-0118-01 ASTM-P-0118-02 ASTM-P-0118-03 ASTM-P-0118-04 ASTM-P-0118-05 ASTM-P-0118-06 ASTM-P-0118-07 ASTM-P-0118-08 ASTM-P-0118-09 ASTM-P-0118-10 ASTM-P-0119-01 ASTM-P-0119-02 ASTM-P-0119-03 ASTM-P-0119-04 ASTM-P-0119-05 ASTM-P-0119-06 ASTM-P-0119-07 ASTM-P-0119-08 ASTM-P-0119-09 ASTM-P-0119-10 ASTM-P-0119-11 ASTM-P-0119-12 ASTM-P-0119-13 ASTM-P-0119-14 ASTM-P-0119-15 ASTM-P-0119-16 ASTM-P-0119-17 ASTM-P-0119-18 ASTM-P-0119-19 ASTM-P-0119-20 ASTM-P-0119-21 ASTM-P-0119-22 ASTM-P-0119-SET ASTM-P-0120-01 ASTM-P-0120-02 ASTM-P-0120-03 ASTM-P-0120-04 ASTM-P-0120-05 ASTM-P-0120-06 ASTM-P-0120-07 ASTM-P-0120-08 ASTM-P-0120-09 ASTM-P-0120-10 ASTM-P-0120-11 ASTM-P-0120-12 ASTM-P-0120-13 ASTM-P-0120-14 ASTM-P-0120-15 ASTM-P-0120-16 ASTM-P-0120-17 ASTM-P-0120-18 ASTM-P-0120-19 ASTM-P-0120-20 ASTM-P-0120-21 64 64 64 64 64 64 64 64 64 64 64 64 64 64 58 64 58 64 58 64 58 64 58 64 58 64 58 64 58 64 58 64 58 64 58 64 64 64 64 64 64 64 64 64 64 64 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 ASTM-P-0120-22 ASTM-P-0120-23 ASTM-P-0120-SET ASTM-P-0121-01 ASTM-P-0121-02 ASTM-P-0121-03 ASTM-P-0121-04 ASTM-P-0121-05 ASTM-P-0121-06 ASTM-P-0121-07 ASTM-P-0121-08 ASTM-P-0121-09 ASTM-P-0121-10 ASTM-P-0121-11 ASTM-P-0121-12 ASTM-P-0121-13 ASTM-P-0121-SET ASTM-P-0122-0.5 ASTM-P-0122-1 ASTM-P-0123-0.5 ASTM-P-0123-1 ASTM-P-0135 ASTM-P-0135-PAK ASTM-P-0136-SET ASTM-P-0137N-2G ASTM-P-0137N-2G ASTM-P-0138N-2G ASTM-P-0138N-2G ASTM-P-0139 ASTM-P-0140-01 ASTM-P-0140-02 ASTM-P-0140-03 ASTM-P-0140-04 ASTM-P-0140-05 ASTM-P-0140-IS ASTM-P-0140-IS2 ASTM-P-0140-IS2-PAK ASTM-P-0140-IS-PAK ASTM-P-0140-PES ASTM-P-0140-PES-PAK ASTM-P-0140-QC ASTM-P-0140-QC-PAK ASTM-P-124-01 ASTM-P-124-01-VAP ASTM-P-124-02 ASTM-P-124-02-VAP ASTM-P-124-03 ASTM-P-124-03-VAP ASTM-P-124-04 ASTM-P-124-04-VAP ASTM-P-124-05 ASTM-P-124-05-VAP ASTM-P-124-06 ASTM-P-124-06-VAP ASTM-P-124-07-VAP ASTM-P-125-01-VAP ASTM-P-125-02-VAP ASTM-P-126-01 ASTM-P-126-SET ASTM-P-127-01 ASTM-P-127-02 ASTM-P-128-01 ASTM-P-128-02 ASTM-P-128-03 ASTM-P-128-04 ASTM-P-128-05 ASTM-P-128-06 ASTM-P-129-01 ASTM-P-129-02 ASTM-P-131-01 ASTM-P-131-02 ASTM-P-131-03 ASTM-P-131-04 ASTM-P-131-05 ASTM-P-132-01 ASTM-P-132-02 ASTM-P-132-03 ASTM-P-132-04 ASTM-P-133-01 ASTM-P-133-02 ASTM-P-133-03 ASTM-P-133-04 ASTM-P-134-PAK ASTM-PIANO-SET ASTM-SSTD-A/B-SET ASTM-SSTDA-01 ASTM-SSTDA-02 ASTM-SSTDA-03 ASTM-SSTDA-04 ASTM-SSTDA-BL 60, 60, 60, 60, 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 65 57 57 57 56 15 56 15 14 51 51 51 51 51 51 51 51 51 51 51 51 51 32 29 32 29 32 29 32 29 32 29 32 29 29 29 29 3 3 3 3 3 3 3 3 3 3 5 5 5 5 5 5 5 3 3 3 3 3 3 3 3 4 13 11 11 11 11 11 11 11 11 11 11 11 85 85 85 85 85 85 12 93 21 54 54 54 21 21 21 21 21 54 54 54 21 21 21 21 21 54 54 54 21 21 21 21 21 54 54 54 21 21 21 21 21 54 54 54 21 21 21 21 21 54 54 54 21 21 21 21 21 54 54 54 21 21 21 21 21 54 54 54 21 21 21 21 21 54 54 54 21 21 21 21 98 71 71 71 71 CLP-BLN-5 39, CLP-BLN-5 CLP-BLN-L 39, CLP-BLN-L CLP-BLW-5 CLP-BTEX CLP-BTEX-10X CLP-BTEX-10X-PAK CLP-BTEX-PAK D-2622-LL-1000X-4 D-2622-LL-100X-4 D-2622-LL-10X-4 D-2622-LL-1100X-4 D-2622-LL-1200X-4 D-2622-LL-200X-4 D-2622-LL-300X-4 D-2622-LL-30X-4 D-2622-LL-400X-4 D-2622-LL-500X-4 D-2622-LL-50X-4 D-2622-LL-5X-4 D-2622-LL-600X-4 D-2622-LL-700X-4 D-2622-LL-75X-4 D-2622-LL-800X-4 D-2622-LL-900X-4 D-2622-LL-BL-4 D-2622-LL-CAL-SET D-2789-CTM D-2789-CTM-PAK D-2887-REFOIL D-3120-92-100X 10, D-3120-92-10X 10, D-3120-92-1X 10, D-3120-92-30X 10, D-3120-92-3X 10, D-3120-92-50X 10, D-3120-92-75X 10, D-3120-92-BL D-3120-92-CAL-SET 10, D-3120-BL D-3230-89-1 D-3230-89-5 D-3237-01 D-3237-02 D-3237-03 D-3237-04 D-3237-CAL-SET D-3524-CAL-SET-10ML D-3524-CAL-SET-5ML D-3524-CR D-3524-CR-PAK D-3524-IS-10ML D-3524-IS-10ML-PAK D-3524-QC-10ML D-3605-91-1 D-3606/IS2-SET D-3606/IS2-SET-PAK D-3606/IS-SET D-3606/IS-SET-2ML D-3606/IS-SET-2ML-PAK D-3606-QC/IS-10ML D-3606-QC/IS-10ML-PAK D-3606-QC-25ML D-3606-QC-25ML-PAK D-3606-QC-IS2-25ML D-3606-QC-IS2-25ML-PAK D-3606-SET-25ML D-3610-93-1 D-3710-QUAL D-3710-QUAL-PAK D-3798-10ML D-3798-10ML-PAK D-3798-IS D-3798-IS-PAK D-3831 D-4291-93 D-4291-93-PAK D-4420-94 D-4420-94-PAK D-4420-CAL-SET D-4629-91-HB-0.3X D-4629-91-HB-100X D-4629-91-HB-10X D-4629-91-HB-1X D-4629-91-HB-25X D-4629-91-HB-50X D-4629-91-HB-75X D-4629-91-HB-CAL-SET D-4629-91-HB-CON 52 71 52 71 71 94 94 94 94 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 10 11 11 14 16 16 16 16 16 16 16 10 16 16 16 16 16 16 16 16 16 17 17 17 17 17 17 17 17 18 18 18 18 18 18 18 18 18 18 18 18 18 20 20 20 20 20 20 20 21 21 22 22 22 23 23 23 23 23 23 23 23 23 D-4629-91-HB-CON-PAK D-4629-91-LB-0.3X D-4629-91-LB-100X D-4629-91-LB-10X D-4629-91-LB-1X D-4629-91-LB-25X D-4629-91-LB-50X D-4629-91-LB-75X D-4629-91-LB-CAL-SET D-4629-91-LB-CON D-4629-91-LB-CON-PAK D-4815/IS-SET D-4815/IS-SET-PAK D-4815-RT D-4815-RT-PAK D-4815-SET-10ML D-4815-VT D-4815-VT-PAK D-4929-94 D-4929-94-100X D-4929-94-100X-PAK D-4929-94-PAK D-5059-A-01 D-5059-A-02 D-5059-A-03 D-5059-A-04 D-5059-A-05 D-5059-A-06 D-5059-A-07 D-5059-A-CAL-SET D-5059-C-01 D-5059-C-02 D-5059-C-03 D-5059-C-04 D-5059-C-05 D-5059-C-06 D-5059-C-07 D-5059-C-CAL-SET D-5059-IS-10ML-PAK D-5059-IS-4 D-5134-92-ALK D-5134-92-CEM D-5134-92-LCM D-5134-92-NAP D-5134-92-REF D-5134-92-SET D-5184-91-AL-1 D-5184-91-AL-5 D-5184-91-SI-1 D-5184-91-SI-5 D-5184-91-TA-5 D-5186-96-DLC-25X D-5186-96-DLC-50X D-5186-96-DLC-SET D-5186-96-PM D-5186-96-PM-PAK D-5307-CR D-5307-CR-PAK D-5307-IS-10ML D-5307-IS-10ML-PAK D-5307-QUAL D-5307-QUAL-PAK D-5307-QUANT D-5307-QUANT-PAK D-5441 D-5441-10X D-5441-10X-5ML D-5441-10X-5ML-PAK D-5441-10X-PAK D-5441-5ML D-5441-5ML-PAK D-5441-PAK D-5441-QUAL D-5441-QUANT D-5441-RES D-5441-RES-5ML D-5441-RES-5ML-PAK D-5441-RES-PAK D-5442-CR-PAK D-5442-PAK D-5442-RT1 D-5442-RT2 D-5443-93-HTM D-5453-HL-01 D-5453-HL-02 D-5453-HL-03 D-5453-HL-04 D-5453-HL-BL D-5453-HL-SET D-5453-LL-01 23 23 23 23 23 23 23 23 23 23 23 24 24 24 24 24 24 24 25 25 25 25 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 27 28 28 28 28 28 28 28 28 28 28 29 29 29 29 29 29 29 29 30 30 30 30 30 30 30 30 30 30 30 30 30 30 31 31 31 31 31 31 31 31 31 31 31 31 D-5453-LL-02 D-5453-LL-03 D-5453-LL-04 D-5453-LL-BL D-5453-LL-SET D-5453-ML-01 D-5453-ML-02 D-5453-ML-03 D-5453-ML-04 D-5453-ML-05 D-5453-ML-BL D-5453-ML-SET D-5480-CR-100X-PAK D-5480-CR-PAK D-5480-IS-5ML D-5480-IS-5ML-PAK D-5501-94-01 D-5501-94-02 D-5501-94-03 D-5501-94-04 D-5501-94-05 D-5501-94-06 D-5501-94-07 D-5580-95-CAL-IS-SET D-5580-95-CAL-SET-10ML D-5580-QC D-5580-QC-PAK D-5580-QC-R1 D-5580-QC-R1-PAK D-5600-01-1 D-5600-BLH-5 D-5600-BLH-L D-5600-LIB-1 D-5600-LIB-5 D-5708-A-10X D-5708-B-10X-1 D-5708-B-10X-5 D-5708-B-5 D-5762-95-100X D-5762-95-10X D-5762-95-1X D-5762-95-500X-PAK D-5762-95-50X D-5762-95-5X D-5762-95-BL D-5762-95-CAL-SET D-5769-ADD/IS D-5769-ADD/IS-R D-5769-ADD/IS-R2 D-5769-ADD-10ML D-5769-ADD-5ML D-5769-CAL/IS-R2-SET D-5769-CAL/IS-R-SET D-5769-CAL/IS-SET D-5769-CAL-SET-10ML D-5769-CAL-SET-5ML D-5769-QC/IS-5ML D-5769-QC/IS-5ML-PAK D-5769-QC/IS-R2-5ML D-5769-QC/IS-R2-5ML-PAK D-5769-QC/IS-R-5ML D-5769-QC/IS-R-5ML-PAK D-5769-QC-10ML D-5769-QC-10ML-PAK D-5863-95A-10X-1 D-5863-95B-10X D-611-01 D-611-02 D-611-03 D-611-04 D-611-05 D-611E-01 D-611E-02 D-611E-03 D-611E-SET D-611-SET D-6258-01 D-6258-02 D-6258-03 D-6258-04 D-6258-05 D-6258-BL D-6258-CAL-SET-5ML D-6258-CONC-5ML D-6296-BL D-6296-CAL1 D-6296-CAL1-PAK D-6296-CAL2 D-6296-CAL2-PAK D-6296-VER1 31 31 31 31 31 31 31 31 31 31 31 31 32 32 32 32 32 32 32 32 32 32 32 32 32 33 33 33 33 37 37 37 37 37 39 39 39 39 40 40 40 40 40 40 40 40 47 48 49 46 46 49 48 47 46 46 47 47 49 49 48 48 46 46 52 52 4 4 4 4 4 4 4 4 4 4 54 54 54 54 54 54 54 54 55 55 55 55 55 55 D-6296-VER2 55 D-6296-VER-SET 55 D-6296-VER-SET-PAK 55 D-6379-SET 57 D-6379-SET-PAK 57 D-6379-SRS 57 D-6379-SRS-PAK 57 D-6428-0.1X 57 D-6428-0.1X-4 57 D-6428-0.5X 57 D-6428-0.5X-4 57 D-6428-100X 57 D-6428-100X-4 57 D-6428-10X 57 D-6428-10X-4 57 D-6428-1X 57 D-6428-1X-4 57 D-6428-2.5X 57 D-6428-2.5X-4 57 D-6428-25X 57 D-6428-25X-4 57 D-6428-50X 57 D-6428-50X-4 57 D-6428-5X 57 D-6428-5X-4 57 D-6428-75X 57 D-6428-75X-4 57 D-6428-BL 57 D-6428-BL-4 57 D-6428-R1-4-SET 57 D-6428-R1-SET 57 D-6428-R2-4-SET 57 D-6428-R2-SET 57 D-6550-CONC 58 D-6550-CONC-5ML 58 DRH/GRH-FL-SS 86 DRH/GRH-FL-SS-PAK 86 DRH/GRH-FL-SS-R2 86 DRH/GRH-FL-SS-R2-PAK 86 DRH-001S 95 DRH-001S-10X 95 DRH-002N 56 DRH-002N 14 DRH-002N-10X 56 DRH-002N-10X 14 DRH-002S 95 DRH-002S-R1 14, 20 DRH-002S-R1-PAK 14, 20 DRH-002S-R2 14 DRH-002S-R2-PAK 14 DRH-003S 95 DRH-004S-5X 86, 95 DRH-004S-5X-PAK 86 DRH-005S-10X 14 DRH-005S-10X 95 DRH-006-CAL-10X 87 DRH-006-CAL-1X 87 DRH-006-CAL-20X 87 DRH-006-CAL-40X 87 DRH-006-CAL-4X 87 DRH-006-CAL-SET 87 DRH-006S 87 DRH-006S-PAK 87 DRH-006-SS 88, 91 DRH-006-SS-PAK 88, 91 DRH-007-CAL-10X 87 DRH-007-CAL-1X 87 DRH-007-CAL-20X 87 DRH-007-CAL-40X 87 DRH-007-CAL-4X 87 DRH-007-CAL-SET 87 DRH-007S 87 DRH-007S-PAK 87 DRH-007-SS 87, 91 DRH-007-SS-PAK 87, 91 DRH-008S-R1 14, 56, 86, 95 DRH-008S-R1-PAK 14, 56, 86, 95 DRH-009S 85 DRH-009S-PAK 85 DRH-010S 97 DRH-010S-PAK 97 DRH-FL-SS 86 DRH-FL-SS-3X 86 DRH-FL-SS-3X-PAK 86 DRH-FL-SS-PAK 86 DRH-FTRPH 86, 95 DRH-FTRPH2 95 DRH-FTRPH2-PAK 95 DRH-FTRPH-PAK 86, 95 INDEX ASTM-SSTDB-04 ASTM-SSTDB-05 ASTM-SSTDB-06 ASTM-SSTDB-07 ASTM-SSTDB-BL AZ-8015-DRO/ORO AZ-8015-DRO/ORO-PAK AZ-8015-RTV AZ-8015-RTV-PAK AZ-8015-SCS AZ-8015-SCS-PAK BOOK-TPH BOOK-TPH C-216N C-216S C-216S-H-10X C-216S-M C-216-ST-1 C-216-ST-1-PAK C-216-ST-2 C-216-ST-2-PAK C-221N C-221S C-221S-H-10X C-221S-M C-221-ST-1 C-221-ST-1-PAK C-221-ST-2 C-221-ST-2-PAK C-232N C-232S C-232S-H-10X C-232S-M C-232-ST-1 C-232-ST-1-PAK C-232-ST-2 C-232-ST-2-PAK C-242N C-242S C-242S-H-10X C-242S-M C-242-ST-1 C-242-ST-1-PAK C-242-ST-2 C-242-ST-2-PAK C-248N C-248S C-248S-H-10X C-248S-M C-248-ST-1 C-248-ST-1-PAK C-248-ST-2 C-248-ST-2-PAK C-254N C-254S C-254S-H-10X C-254S-M C-254-ST-1 C-254-ST-1-PAK C-254-ST-2 C-254-ST-2-PAK C-260N C-260S C-260S-H-10X C-260S-M C-260-ST-1 C-260-ST-1-PAK C-260-ST-2 C-260-ST-2-PAK C-262N C-262S C-262S-H-10X C-262S-M C-262-ST-1 C-262-ST-1-PAK C-262-ST-2 C-262-ST-2-PAK C-268N C-268S C-268S-H-10X C-268S-M C-268-ST-1 C-268-ST-1-PAK C-268-ST-2 C-268-ST-2-PAK CAR-DNPH CLP-BLH-5 CLP-BLH-L CLP-BLMA-5 CLP-BLMA-L iii INDEX iv DRH-FTRPH-SET DRH-FTRPH-SET-PAK DRH-MA-FSS-10ML DRH-MA-FSS-50X DRH-MA-FSS-50X-PAK DRH-MA-MS DRH-MA-MS-10X DRH-MA-MS-10X-PAK DRH-MA-MS-40X DRH-MA-MS-40X-PAK DRH-MA-MS-PAK DRH-MA-SS 87, DRH-MA-SS-100X 87, DRH-MA-SS-100X-PAK 87, DRH-MA-SS-10X 87, DRH-MS-ASL DRH-MS-ASL-PAK DRH-PA-001 DRH-PA-001-PAK DRH-SS DRH-SS-PAK DRH-TX-001-10X DRH-TX-001-10X-PAK DRH-TX-002-10X DRH-TX-002-10X-PAK DRH-TX-002-D-0.4X-10ML DRH-TX-002-D-40X DRH-TX-002-D-40X-PAK DRH-TX-002-D-SET DRH-TX-003-CNM DRH-TX-003-CNM-PAK DRH-TX-003-FCS DRH-TX-003-FCS-PAK DRH-TX-003-SET DRH-TX-003-SS1 DRH-TX-003-SS1-PAK FD2-W25-10X FD2-W25-R1-10X FD2-W50-10X FD2-W50-R1-10X FD2-W75-10X FD2-W75-R1-10X FIA-ARO FIA-ARO-5ML FIA-CAL-SET FIA-OLE FIA-OLE-5ML FIA-PAR FIA-PAR-5ML FK-W25-10X FK-W50-10X FK-W75-10X FU-001 FU-001-40X FU-001-D-40X FU-002 FU-002-40X FU-002-D-40X FU-003 FU-003-40X FU-003-D-40X FU-004 FU-004-40X FU-004-D-40X FU-005 FU-005-40X FU-005-D-10X FU-005-D-40X FU-006 FU-006-40X FU-006-D-40X FU-007 FU-007-40X FU-007-D-40X FU-008 FU-008-40X FU-008-D-40X FU-009 FU-009-40X FU-009-D-10X FU-009-D-40X FU-010 FU-010-40X FU-010-D-40X FU-011 FU-011-40X FU-011-D-40X FU-012 FU-012-40X FU-012-D-40X 95 95 88 88 88 87 87 87 87 87 87 91 91 91 91 88 88 89 89 86 86 89 89 89 89 89 89 89 89 89 89 89 89 89 89 89 93 93 93 93 93 93 4 4 4 4 4 4 4 93 93 93 92 92 92 92 92 92 92 92 92 92 92 92 92 92 93 92 92 92 92 92 92 92 92 92 92 92 92 93 92 92 92 92 92 92 92 92 92 92 FU-013 92 FU-013-40X 92 FU-013-D-40X 92 FU-014 92 FU-014-40X 92 FU-014-D-40X 92 FU-015 92 FU-015-40X 92 FU-015-D-40X 92 FU-016 92 FU-016-40X 92 FU-016-D-40X 92 FU-017 92 FU-017-40X 92 FU-017-D-10X 93 FU-017-D-40X 92 FU-018-D-40X 92 FU-018-H 92 FU-018-H-40X 92 FU-019-D-40X 92 FU-019-H 92 FU-019-H-40X 92 FU-020-D-40X 92 FU-020-H 92 FU-020-H-40X 92 FU-021-D-40X 92 FU-021-H 92 FU-021-H-40X 92 FU-022 92 FU-022-40X 92 FU-022-D-40X 92 FU-023 92 FU-023-40X 92 FU-023-D-40X 92 FU-025-D-40X 93 FU-025-H 93 FU-025-H-40X 93 FU-026-D-40X 93 FU-026-H 93 FU-026-H-40X 93 FU-027-D-40X 93 FU-027-H 93 FU-027-H-40X 93 FU-028-D-40X 93 FU-028-H 93 FU-028-H-40X 93 GA-001 92 GA-001-10X 93 GA-001-20X-BTEX 82, 88, 90, 94 GA-001-40X 92 GA-001-D-40X 92 GA-002 92 GA-002-40X 92 GA-002-D-40X 92 GA-003 92 GA-003-40X 92 GA-003-D-40X 92 GA-004 92 GA-004-40X 92 GA-004-D-40X 92 GA-005 92 GA-005-40X 92 GA-005-D-40X 92 GAD-001 94 GAD-001-PAK 94 GARH-IS 94 GARH-SS 94 GA-W25-10X 93 GA-W50-10X 93 GA-W75-10X 93 GRH-001S 94 GRH-001S-PAK 94 GRH-002S 94 GRH-003S 91, 94 GRH-003S-PAK 91, 94 GRH-004-MS 88 GRH-004-MS-100X 88 GRH-004-MS-100X-PAK 88 GRH-004-MS-10X 88 GRH-004-MS-10X-PAK 88 GRH-004-MS-PAK 88 GRH-004S/SS 88 GRH-004S/SS-PAK 88 GRH-004S-10X 88 GRH-004S-10X-PAK 88 GRH-004-SS 88, 90 GRH-004-SS-100X 88, 90 GRH-004-SS-100X-PAK 88, 90 GRH-004-SS-10X 88, 90 GRH-004-SS-10X-PAK 88, GRH-004-SS-PAK 88, GRH-IS 85-86, 88, 91, GRH-IS-10X 88, GRH-IS-PAK 85-86, 88, 91, GRH-PA-001 GRH-PA-001-PAK GRH-SS 85-86, GRH-SS-PAK 85-86, HS-001N HS-001S HS-001S-40X HS-001S-D-40X HS-002N HS-002S HS-002S-40X HS-002S-D-40X HS-003N HS-003S HS-003S-40X HS-003S-D-40X HS-004N HS-004S HS-004S-40X HS-004S-D-40X HS-005N HS-005S HS-005S-40X HS-005S-D-40X IC-ACET-10X-1 IC-ACET-10X-5 IC-ACET-1X-1 IC-ACET-1X-5 IC-AN-KIT-10X-1 IC-AN-KIT-10X-5 IC-AN-KIT-1X-1 IC-AN-KIT-1X-5 IC-AN-KIT-2X-1 IC-AN-KIT-2X-5 IC-AN-KIT-R-10X-1 IC-AN-KIT-R-10X-5 IC-BA-10X-1 IC-BA-10X-5 IC-BA-1X-1 IC-BA-1X-5 IC-BA-2X-1 IC-BA-2X-5 IC-BR-10X-1 IC-BR-1X-1 IC-BR-1X-5 IC-BR-2X-1 IC-BR-2X-5 IC-CA-10X-1 IC-CA-10X-5 IC-CA-1X-1 IC-CA-1X-5 IC-CA-2X-1 IC-CA-2X-5 IC-CAT-KIT-10X-1 IC-CAT-KIT-10X-5 IC-CAT-KIT-1X-1 IC-CAT-KIT-1X-5 IC-CAT-KIT-2X-1 IC-CAT-KIT-2X-5 IC-CHLR-10X-1 IC-CHLR-10X-5 IC-CHLR-1X-1 IC-CHLR-1X-5 IC-CHRM-10X-1 IC-CHRM-10X-5 IC-CHRM-1X-1 IC-CHRM-1X-5 IC-Cl-10X-1 IC-Cl-10X-5 IC-Cl-1X-1 IC-Cl-1X-5 IC-Cl-2X-1 IC-Cl-2X-5 IC-ELU-01-0.5 IC-ELU-01-0.5-PAK IC-ELU-01-1 IC-ELU-01-1-PAK IC-ELU-02-0.5 IC-ELU-02-0.5-PAK IC-ELU-02-1 IC-ELU-02-1-PAK IC-ELU-03-0.5 IC-ELU-03-0.5-PAK IC-ELU-03-1 IC-ELU-03-1-PAK 90 90 95 91 95 89 89 95 95 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 92 79 79 79 79 76 76 76 76 76 76 79 79 78 78 78 78 78 78 76 76 76 76 76 78 78 78 78 78 78 78 78 78 78 78 78 79 79 79 79 79 79 79 79 76 76 76 76 76 76 79 79 79 79 79 79 79 79 79 79 79 79 IC-F-10X-1 IC-F-10X-5 IC-F-1X-1 IC-F-1X-5 IC-F-2X-1 IC-FORM-10X-1 IC-FORM-10X-5 IC-FORM-1X-1 IC-FORM-1X-5 IC-K-10X-1 IC-K-10X-5 IC-K-1X-1 IC-K-1X-5 IC-K-2X-1 IC-K-2X-5 IC-LI-10X-1 IC-LI-10X-5 IC-LI-1X-1 IC-LI-1X-5 IC-LI-2X-1 IC-LI-2X-5 IC-MAN-01-1 IC-MAN-02-1 IC-MAN-03-1 IC-MAN-04-1 IC-MAN-05-R1-1 IC-MAN-05-SET IC-MAN-06-R1-1 IC-MAN-06-SET IC-MAN-07-R1-1 IC-MAN-07-SET IC-MAN-08-R1-1 IC-MAN-08-SET IC-MAN-09-R1-1 IC-MAN-09-SET IC-MAN-10-R1-1 IC-MAN-10-SET IC-MAN-11-1 IC-MAN-12-1 IC-MAN-13-1 IC-MAN-14-R2-1 IC-MAN-14-R2-SET IC-MAN-14-R3-1 IC-MAN-14-SET IC-MAN-15-R2-1 IC-MAN-15R-SET IC-MAN-16-R1-1 IC-MAN-16-SET IC-MAN-17-R1-1 IC-MAN-17-SET IC-MAN-18-R1-1 IC-MAN-18-SET IC-MAN-CAL-SET IC-MCA-01-1 IC-MCA-02-1 IC-MCA-03-1 IC-MCA-04-1 IC-MCA-05-1 IC-MCA-06-1 IC-MG-10X-1 IC-MG-10X-5 IC-MG-1X-1 IC-MG-1X-5 IC-MG-2X-1 IC-MG-2X-5 IC-NA-10X-1 IC-NA-10X-5 IC-NA-1X-1 IC-NA-1X-5 IC-NA-2X-1 IC-NA-2X-5 IC-NH4-10X-1 IC-NH4-10X-5 IC-NH4-1X-1 IC-NH4-1X-5 IC-NH4-2X-1 IC-NH4-2X-5 IC-NH4-N-10X-1 IC-NH4-N-10X-5 IC-NH4-N-1X-1 IC-NH4-N-1X-5 IC-NO2-0.05X-1 IC-NO2-0.12X-1 IC-NO2-0.1X-1 IC-NO2-0.2X-1 IC-NO2-0.4X-1 IC-NO2-0.5X-1 IC-NO2-10X-1 IC-NO2-10X-5 IC-NO2-1X-1 76 76 76 76 76 79 79 79 79 78 78 78 78 78 78 78 78 78 78 78 78 77 77 77 77 77 77 77 77 77 77 77 77 77 77 77 77 77 77 77 77, 79 77, 79 77 77 77 77 77 77 77 77 77 77 77 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 78 79 79 79 79 77 77 77 77 77 77 76 76 76-77 IC-NO2-1X-5 IC-NO2-2X-1 IC-NO2-2X-5 IC-NO2-N-10X-1 IC-NO2-N-10X-5 IC-NO2-N-1X-1 IC-NO2-N-1X-5 IC-NO3-10X-1 IC-NO3-10X-5 IC-NO3-1X-1 IC-NO3-1X-5 IC-NO3-2X-1 IC-NO3-2X-5 IC-NO3-N-10X-1 IC-NO3-N-10X-5 IC-NO3-N-1X-1 IC-NO3-N-1X-5 IC-OXAL-10X-1 IC-OXAL-10X-5 IC-OXAL-1X-1 IC-OXAL-1X-5 ICP-01N-0.5-10X ICP-01N-1 ICP-01N-10X-20ML ICP-01N-1-10X ICP-01N-25X-20ML ICP-01N-5 ICP-01N-5-10X ICP-02N-0.5-10X ICP-02N-1 ICP-02N-10X-20ML ICP-02N-1-10X ICP-02N-5 ICP-02N-5-10X ICP-03N-0.5-10X ICP-03N-1 ICP-03N-10X-20ML ICP-03N-1-10X ICP-03N-25X-20ML ICP-03N-5 ICP-03N-5-10X ICP-04N-0.5-10X ICP-04N-1 ICP-04N-10X-20ML ICP-04N-1-10X ICP-04N-25X-20ML ICP-04N-5 ICP-04N-5-10X ICP-05N-0.5-10X ICP-05N-1 ICP-05N-10X-20ML ICP-05N-1-10X ICP-05N-5 ICP-05N-5-10X ICP-06N-0.5-10X ICP-06N-1 ICP-06N-10X-20ML ICP-06N-1-10X ICP-06N-25X-20ML ICP-06N-5 ICP-06N-5-10X ICP-07W-0.5-10X ICP-07W-1 ICP-07W-10X-20ML ICP-07W-1-10X ICP-07W-5 ICP-07W-5-10X ICP-08N-0.5-10X ICP-08N-1 ICP-08N-10X-20ML ICP-08N-1-10X ICP-08N-25X-20ML ICP-08N-5 ICP-08N-5-10X ICP-09N-0.5-10X ICP-09N-1 ICP-09N-10X-20ML ICP-09N-1-10X ICP-09N-25X-20ML ICP-09N-5 ICP-09N-5-10X ICP-11N-0.5-10X ICP-11N-1 ICP-11N-10X-20ML ICP-11N-1-10X ICP-11N-25X-20ML ICP-11N-5 ICP-11N-5-10X ICP-12N-0.5-10X 76 76 76 79 79 77, 79 79 76 76 76 76 76 76 79 79 79 79 79 79 79 79 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 68 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 ICP-24N-5 ICP-24N-5-10X ICP-25N-1 ICP-25N-10X-20ML ICP-25N-25X-20ML ICP-25N-5 ICP-26H-0.5-10X ICP-26H-1 ICP-26H-10X-20ML ICP-26H-1-10X ICP-26H-25X-20ML ICP-26H-5 ICP-26H-5-10X ICP-27N-0.5-10X ICP-27N-1 ICP-27N-10X-20ML ICP-27N-1-10X ICP-27N-25X-20ML ICP-27N-5 ICP-27N-5 ICP-27N-5-10X ICP-28N-0.5-10X ICP-28N-1 ICP-28N-10X-20ML ICP-28N-1-10X ICP-28N-25X-20ML ICP-28N-5 ICP-28N-5-10X ICP-29N-0.5-10X ICP-29N-1 ICP-29N-10X-20ML ICP-29N-1-10X ICP-29N-25X-20ML ICP-29N-5 ICP-29N-5-10X ICP-30N-0.5-10X ICP-30N-1 ICP-30N-10X-20ML ICP-30N-1-10X ICP-30N-25X-20ML ICP-30N-5 ICP-30N-5-10X ICP-31N-0.5-10X ICP-31N-1 ICP-31N-10X-20ML ICP-31N-1-10X ICP-31N-25X-20ML ICP-31N-5 ICP-31N-5-10X ICP-32N-0.5-10X ICP-32N-1 ICP-32N-10X-20ML ICP-32N-1-10X ICP-32N-25X-20ML ICP-32N-5 ICP-32N-5-10X ICP-33N-0.5-10X ICP-33N-1 ICP-33N-10X-20ML ICP-33N-1-10X ICP-33N-25X-20ML ICP-33N-5 ICP-33N-5-10X ICP-34N-0.5-10X ICP-34N-1 ICP-34N-10X-20ML ICP-34N-1-10X ICP-34N-25X-20ML ICP-34N-5 ICP-34N-5-10X ICP-35W-0.5-10X ICP-35W-1 ICP-35W-10X-20ML ICP-35W-1-10X ICP-35W-25X-20ML ICP-35W-5 ICP-35W-5-10 ICP-36N-0.5-10X ICP-36N-1 ICP-36N-10X-20ML ICP-36N-1-10X ICP-36N-25X-20ML ICP-36N-5 ICP-36N-5-10X ICP-37N-0.5-10X ICP-37N-1 ICP-37N-10X-20ML ICP-37N-1-10X ICP-37N-25X-20ML ICP-37N-5 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 52 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 69 52 ICP-37N-5 ICP-37N-5-10X ICP-38W-0.5-10X ICP-38W-1 ICP-38W-10X-20ML ICP-38W-1-10X ICP-38W-25X-20ML ICP-38W-5 ICP-38W-5-10X ICP-40H-0.5-10X ICP-40H-1 ICP-40H-10X-20ML ICP-40H-1-10X ICP-40H-25X-20ML ICP-40H-5 ICP-40H-5-10X ICP-41W-0.5-10X ICP-41W-1 ICP-41W-1 ICP-41W-10X-20ML ICP-41W-1-10X ICP-41W-5 ICP-41W-5 ICP-41W-5-10X ICP-42H-0.5-10X ICP-42H-1 ICP-42H-10X-20ML ICP-42H-1-10X ICP-42H-25X-20ML ICP-42H-5 ICP-42H-5-10X ICP-43N-0.5-10X ICP-43N-1 ICP-43N-10X-20ML ICP-43N-1-10X ICP-43N-25X-20ML ICP-43N-5 ICP-43N-5-10X ICP-44N-0.5-10X ICP-44N-10X-20ML ICP-44N-1-10X ICP-44N-25X-20ML ICP-44N-5-10X ICP-45W-0.5-10X ICP-45W-10X-20ML ICP-45W-1-10X ICP-45W-25X-20ML ICP-45W-5-10X ICP-46H-0.5-10X ICP-46H-10X-20ML ICP-46H-1-10X ICP-46H-25X-20ML ICP-46H-5-10X ICP-47N-0.5-10X ICP-47N-10X-20ML ICP-47N-1-10X ICP-47N-25X-20ML ICP-47N-5-10X ICP-48H-0.5-10X ICP-48H-10X-20ML ICP-48H-1-10X ICP-48H-25X-20ML ICP-48H-5-10X ICP-49N-0.5-10X ICP-49N-10X-20ML ICP-49N-1-10X ICP-49N-25X-20ML ICP-49N-5-10X ICP-50N-0.5-10X ICP-50N-10X-20ML ICP-50N-1-10X ICP-50N-25X-20ML ICP-50N-5-10X ICP-51N-0.5-10X ICP-51N-1 ICP-51N-10X-20ML ICP-51N-1-10X ICP-51N-25X-20ML ICP-51N-5 ICP-51N-5-10X ICP-52W-0.5-10X ICP-52W-1 ICP-52W-10X-20ML ICP-52W-1-10X ICP-52W-5 ICP-52W-5-10X ICP-53N-0.5-10X ICP-53N-1 ICP-53N-10X-20ML ICP-53N-1-10X 69 69 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 16 70 70 70 16 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 ICP-53N-25X-20ML ICP-53N-5 ICP-53N-5-10X ICP-54N-0.5-10X ICP-54N-1 ICP-54N-10X-20ML ICP-54N-1-10X ICP-54N-25X-20ML ICP-54N-5 ICP-54N-5-10X ICP-55N-0.5-10X ICP-55N-1 ICP-55N-10X-20ML ICP-55N-1-10X ICP-55N-25X-20ML ICP-55N-5 ICP-55N-5-10X ICP-56W-0.5-10X ICP-56W-1 ICP-56W-10X-20ML ICP-56W-1-10X ICP-56W-25X-20ML ICP-56W-5 ICP-56W-5-10X ICP-57W-0.5-10X ICP-57W-1 ICP-57W-10X-20ML ICP-57W-1-10X ICP-57W-25X-20ML ICP-57W-5 ICP-57W-5-10X ICP-58H-0.5-10X ICP-58H-1 ICP-58H-10X-20ML ICP-58H-1-10X ICP-58H-5 ICP-58H-5-10X ICP-59N-0.5-10X ICP-59N-1 ICP-59N-10X-20ML ICP-59N-1-10X ICP-59N-25X-20ML ICP-59N-5 ICP-59N-5-10X ICP-60N-0.5-10X ICP-60N-1 ICP-60N-10X-20ML ICP-60N-1-10X ICP-60N-25X-20ML ICP-60N-5 ICP-60N-5-10X ICP-61N-1 ICP-61N-5 ICP-62N-0.5-10X ICP-62N-1 ICP-62N-10X-20ML ICP-62N-1-10X ICP-62N-25X-20ML ICP-62N-5 ICP-62N-5-10X ICP-63H-0.5-10X ICP-63H-1 ICP-63H-1-10X ICP-63H-5 ICP-63H-5-10X ICP-63N-0.5-10X ICP-63N-1 ICP-63N-10X-20ML ICP-63N-1-10X ICP-63N-25X-20ML ICP-63N-5 ICP-63N-5-10X ICP-64W-0.5-10X ICP-64W-1 ICP-64W-10X-20ML ICP-64W-1-10X ICP-65W-0.5-10X ICP-65W-1 ICP-65W-10X-20ML ICP-65W-1-10X ICP-65W-5 ICP-65W-5-10X ICP-66N-1 ICP-66N-5 ICP-67N-0.5-10X ICP-67N-1 ICP-67N-10X-20ML ICP-67N-1-10X ICP-67N-25X-20ML ICP-67N-5 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 70 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 52 ICP-67N-5 ICP-67N-5-10X ICP-68N-0.5-10X ICP-68N-1 ICP-68N-10X-20ML ICP-68N-1-10X ICP-68N-25X-20ML ICP-68N-5 ICP-68N-5-10X ICP-69N-0.5-10X ICP-69N-1 ICP-69N-10X-20ML ICP-69N-1-10X ICP-69N-25X-20ML ICP-69N-5 ICP-69N-5-10X ICP-70N-0.5-10X ICP-70N-1 ICP-70N-10X-20ML ICP-70N-1-10X ICP-70N-25X-20ML ICP-70N-5 ICP-70N-5-10X ICP-71N-0.5-10X ICP-71N-1 ICP-71N-10X-20ML ICP-71N-1-10X ICP-71N-25X-20ML ICP-71N-5 ICP-71N-5-10X ICP-MS-01N-0.01X-1 ICP-MS-01N-0.1X-1 ICP-MS-01N-1 ICP-MS-02N-0.01X-1 ICP-MS-02N-0.1X-1 ICP-MS-02N-1 ICP-MS-03N-0.01X-1 ICP-MS-03N-0.1X-1 ICP-MS-03N-1 ICP-MS-04N-0.01X-1 ICP-MS-04N-0.1X-1 ICP-MS-04N-1 ICP-MS-05N-0.01X-1 ICP-MS-05N-0.1X-1 ICP-MS-05N-1 ICP-MS-06N-0.01X-1 ICP-MS-06N-0.1X-1 ICP-MS-06N-1 ICP-MS-08N-0.01X-1 ICP-MS-08N-0.1X-1 ICP-MS-08N-1 ICP-MS-09N-0.01X-1 ICP-MS-09N-0.1X-1 ICP-MS-09N-1 ICP-MS-13N-0.01X-1 ICP-MS-13N-0.1X-1 ICP-MS-13N-1 ICP-MS-14N-0.01X-1 ICP-MS-14N-0.1X-1 ICP-MS-14N-1 ICP-MS-15N-0.01X-1 ICP-MS-15N-1 ICP-MS-21W-0.01X-1 ICP-MS-21W-0.1X-1 ICP-MS-21W-1 ICP-MS-22H-0.01X-1 ICP-MS-22H-0.1X-1 ICP-MS-22H-1 ICP-MS-25N-0.01X-1 ICP-MS-25N-0.1X-1 ICP-MS-25N-1 ICP-MS-27N-0.01X-1 ICP-MS-27N-0.1X-1 ICP-MS-27N-1 ICP-MS-29N-0.01X-1 ICP-MS-29N-0.1X-1 ICP-MS-29N-1 ICP-MS-30N-0.01X-1 ICP-MS-30N-0.1X-1 ICP-MS-30N-1 ICP-MS-32N-0.01X-1 ICP-MS-32N-0.1X-1 ICP-MS-32N-1 ICP-MS-33N-0.01X-1 ICP-MS-33N-0.1X-1 ICP-MS-33N-1 ICP-MS-34N-0.01X-1 ICP-MS-34N-0.1X-1 ICP-MS-34N-1 ICP-MS-35W-0.01X-1 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 71 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 INDEX ICP-12N-1 ICP-12N-10X-20ML ICP-12N-1-10X ICP-12N-25X-20ML ICP-12N-5 ICP-12N-5-10X ICP-13H-0.5-10X ICP-13H-1 ICP-13H-1-10X ICP-13H-5 ICP-13H-5-10X ICP-13N-0.5-10X ICP-13N-1 ICP-13N-10X-20ML ICP-13N-1-10X ICP-13N-25X-20ML ICP-13N-5 ICP-13N-5-10X ICP-14N-0.5-10X ICP-14N-1 ICP-14N-10X-20ML ICP-14N-1-10X ICP-14N-25X-20ML ICP-14N-5 ICP-14N-5-10X ICP-15N-0.5-10X ICP-15N-1 ICP-15N-10X-20ML ICP-15N-1-10X ICP-15N-25X-20ML ICP-15N-5 ICP-15N-5-10X ICP-16N-0.5-10X ICP-16N-1 ICP-16N-10X-20ML ICP-16N-1-10X ICP-16N-25X-20ML ICP-16N-5 ICP-16N-5-10X ICP-17N-0.5-10X ICP-17N-1 ICP-17N-10X-20ML ICP-17N-1-10X ICP-17N-25X-20ML ICP-17N-5 ICP-17N-5-10X ICP-18N-0.5-10X ICP-18N-1 ICP-18N-10X-20ML ICP-18N-1-10X ICP-18N-25X-20ML ICP-18N-5 ICP-18N-5-10X ICP-19N-0.5-10X ICP-19N-1 ICP-19N-10X-20ML ICP-19N-1-10X ICP-19N-25X-20ML ICP-19N-5 ICP-19N-5-10X ICP-20N-0.5-10X ICP-20N-1 ICP-20N-10X-20ML ICP-20N-1-10X ICP-20N-5 ICP-20N-5-10X ICP-21W-0.5-10X ICP-21W-1 ICP-21W-10X-20ML ICP-21W-1-10X ICP-21W-5-10X ICP-22H-0.5-10X ICP-22H-1 ICP-22H-10X-20ML ICP-22H-1-10X ICP-22H-25X-20ML ICP-22H-5 ICP-22H-5-10X ICP-23N-0.5-10X ICP-23N-1 ICP-23N-10X-20ML ICP-23N-1-10X ICP-23N-25X-20ML ICP-23N-5 ICP-23N-5-10X ICP-24N-0.5-10X ICP-24N-1 ICP-24N-10X-20ML ICP-24N-1-10X ICP-24N-25X-20ML v INDEX vi ICP-MS-35W-0.1X-1 ICP-MS-35W-1 ICP-MS-37N-0.01X-1 ICP-MS-37N-0.1X-1 ICP-MS-37N-1 ICP-MS-41W-0.01X-1 ICP-MS-41W-0.1X-1 ICP-MS-41W-1 ICP-MS-43N-0.01X-1 ICP-MS-43N-0.1X-1 ICP-MS-43N-1 ICP-MS-46H-0.01X-1 ICP-MS-46H-0.1X-1 ICP-MS-46H-1 ICP-MS-50N-0.01X-1 ICP-MS-50N-0.1X-1 ICP-MS-50N-1 ICP-MS-51N-0.01X-1 ICP-MS-51N-0.1X-1 ICP-MS-51N-1 ICP-MS-53N-0.01X-1 ICP-MS-53N-0.1X-1 ICP-MS-53N-1 ICP-MS-54N-0.01X-1 ICP-MS-54N-0.1X-1 ICP-MS-54N-1 ICP-MS-55N-0.01X-1 ICP-MS-55N-0.1X-1 ICP-MS-55N-1 ICP-MS-56W-0.01X-1 ICP-MS-56W-0.1X-1 ICP-MS-56W-1 ICP-MS-59N-0.01X-1 ICP-MS-59N-0.1X-1 ICP-MS-59N-1 ICP-MS-60N-0.01X-1 ICP-MS-60N-0.1X-1 ICP-MS-60N-1 ICP-MS-61N-0.01X-1 ICP-MS-61N-0.1X-1 ICP-MS-63N-0.01X-1 ICP-MS-63N-0.1X-1 ICP-MS-63N-1 ICP-MS-64W-0.01X-1 ICP-MS-64W-0.1X-1 ICP-MS-64W-1 ICP-MS-66N-0.01X-1 ICP-MS-66N-0.1X-1 ICP-MS-67N-0.01X-1 ICP-MS-67N-0.1X-1 ICP-MS-67N-1 ICP-MS-69N-0.01X-1 ICP-MS-69N-0.1X-1 ICP-MS-69N-1 ICP-MS-70N-0.01X-1 ICP-MS-70N-0.1X-1 ICP-MS-70N-1 IC-PO4-10X-1 IC-PO4-10X-5 IC-PO4-1X-1 IC-PO4-1X-5 IC-PO4-2X-1 IC-PO4-2X-5 IC-PO4-P-10X-1 IC-PO4-P-10X-5 IC-PO4-P-1X-1 IC-PO4-P-1X-5 IC-SO4-10X-1 IC-SO4-10X-5 IC-SO4-1X-1 IC-SO4-1X-5 IC-SO4-2X-1 IC-SO4-2X-5 IC-SO4-S-10X-1 IC-SO4-S-10X-5 IC-SO4-S-1X-1 IC-SO4-S-1X-5 IC-SR-10X-1 IC-SR-10X-5 IC-SR-1X-1 IC-SR-1X-5 IC-SR-2X-1 IC-SR-2X-5 IPE-OILG-001-AS IPE-OILG-001-AS IPE-OILG-001-AT IPE-OILG-001-AT IPE-OILG-001-AV IPE-OILG-001-AV IS-7281-2OZ 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 72 76 76 76 76 76 76 79 79 79 79 76 76 76 76 76 76 79 79 79 79 78 78 78 78 78 78 2 96 2 96 2 96 59 KF-0.6X-5ML-VAP 5 KF-10X-20ML-PAK 5 KF-10X-2ML-VAP 5 KF-10X-5ML-VAP 5 KF-1X-20ML-PAK 5 KF-1X-2ML-VAP 5 KF-1X-5ML-VAP 5 KF-50X-20ML-PAK 5 KF-50X-2ML-VAP 5 KF-50X-5ML-VAP 5 M-005A 98 M-005A-10X 98 M-005A-10X-PAK 98 M-005A-PAK 98 M-005B 98 M-005B-10X 98 M-005B-10X-PAK 98 M-005B-PAK 98 M-005V 98 M-005V-10X 98 M-005V-10X-PAK 98 M-005V-PAK 98 M-1004 98 M-1004-10X 98 M-1664-20ML 97 M-1664-20ML-PAK 97 M-1664-5ML 97 M-1664-5ML-PAK 97 M-418 97 M-418-CON 97 M-418-PAK 97 M-602-GAS-10X 85, 94 M-8015B/5031-11 85, 94 M-8015B/5031-17 85, 94 M-8440 97 M-8440-CON 97 M-8440-CON-PAK 97 M-8440-PAK 97 M-8440-SGC 97 M-8440-SGC-PAK 97 MA-900-4 59 MA-900-8 59 M-GRA-ADD/IS 44 M-GRA-ADD/IS-R 45 M-GRA-CAL/IS-SET 44 M-GRA-CAL-R/IS-R-SET 45 M-GRA-FP 47-49 M-GRA-FP-PAK 47-49 M-GRA-IS 44, 47, 50 M-GRA-IS-5ML 44, 46-47, 50 M-GRA-IS-5ML-PAK 44, 46-47, 50 M-GRA-IS-AS-5ML 33 M-GRA-IS-AS-5ML-PAK 33 M-GRA-IS-R 45, 48 M-GRA-IS-R-10ML 45-46, 48, 50 M-GRA-IS-R-10ML-PAK 45-46, 48, 50 M-GRA-IS-R2 49 M-GRA-IS-R2-25ML 49 M-GRA-IS-R2-SET 49 M-GRA-K1 43 M-GRA-K2 43 M-GRA-K4 43 M-GRA-MSR 47 M-GRA-MSR-PAK 47 M-GRA-QC/IS-5ML 44 M-GRA-QC/IS-5ML-PAK 44 M-GRA-QC/IS-R-5ML 45 M-GRA-QC/IS-R-5ML-PAK 45 M-GRA-QC-10ML 44-45, 53 M-GRA-QC-10ML-PAK 44-45, 53 M-GRA-QC-R/IS-5ML 50 M-GRA-QC-R/IS-5ML-PAK 50 M-GRA-QC-R/IS-R-5ML 50 M-GRA-QC-R/IS-R-5ML-PAK 50 M-GRA-QC-R-10ML 50 M-GRA-QC-R-10ML-PAK 50 M-GRA-RES 47-49 M-GRA-RES-PAK 47-49 M-GRA-SCS-AS 33 M-GRA-SCS-AS-PAK 33 M-GRA-ST 44-45, 47-49 M-GRA-ST-PAK 44-45, 47-49 M-GRA-VT/IS-AS 33 M-GRA-VT/IS-AS-PAK 33 M-GRA-VT-AS-10ML 33 M-GRA-VT-AS-10ML-PAK 33 M-GRO-BLNK/IS-10ML 35 M-GRO-BLNK/IS-10ML-PAK 35 M-GRO-BLNK-10ML 35-37 M-GRO-BLNK-10ML 24 M-GRO-BLNK-10ML-PAK 35-36 M-GRO-BLNK-10ML-PAK 24 M-GRO-CAL/IS-SET 34 M-GRO-CAL/IS-SET-PAK 34 M-GRO-CAL-EPA-SET-10ML 36 M-GRO-CAL-IS/EPA-SET 36 M-GRO-CAL-SET 34 M-GRO-EPA-CC/IS-5ML 36 M-GRO-EPA-CC/IS-5MLPAK 36 M-GRO-EPA-CC-10ML 36 M-GRO-EPA-CC-10ML-PAK 36 M-GRO-EPA-SP-5ML 36 M-GRO-EPA-SP-5ML-PAK 36 M-GRO-IS-5ML 35-36 M-GRO-IS-5ML 24 M-GRO-IS-5ML-PAK 35-36 M-GRO-IS-5ML-PAK 24 M-GRO-QC/IS-5ML 35 M-GRO-QC/IS-5ML-PAK 35 M-GRO-QC-10ML 35 M-GRO-QC-10ML-PAK 35 M-GRO-QC-R/IS-5ML 35 M-GRO-QC-R/IS-5ML-PAK 35 M-GRO-QC-R-10ML 35 M-GRO-QC-R-10ML-PAK 35 MO-COMP-D-40X 93 MOSOL-20-16 59 MOSOL-75-16 59 OGAD-001 2 OGAD-001 85, 94, 96 OGAD-001-PAK 2 OGAD-001-PAK 85, 94, 96 OMT-001 66 OMT-001-PAK 66 OMT-002 66 OMT-002-PAK 66 OMT-003 66 OMT-003-PAK 66 OMT-004 66 OMT-004-PAK 66 OMT-005 66 OMT-005-PAK 66 OMT-006 66 OMT-006-PAK 66 OPE-OXY-001-AS 2 OPE-OXY-001-AS 96 OPE-OXY-001-AT 2 OPE-OXY-001-AT 96 OPE-OXY-001-AV 2 OPE-OXY-001-AV 96 RGS-001 98 S-3571 12 S-603A-10X 85, 94 S-603A-10X-PAK 85, 94 SBPT-AROM 2, 41 SBPT-BENZ 2, 41 SBPT-COMP 1, 41 SBPT-LSGAS 1, 31, 41 SBPT-OLEFIN 2, 41 SBPT-OLEFINSFC 1, 41 SBPT-SDF 1, 41 SBPT-SGAS 2, 41 SBPT-SWMO 1, 41 SCO-100X-4 11 SCO-10X-4 11 SCO-200X-4 11 SCO-25X-4 11 SCO-300X-4 11 SCO-400X-4 11 SCO-500X-4 11 SCO-50X-4 11 SCO-CAL-SET-4 11 SDF-100X-4 8 SDF-100X-SHOT 8 SDF-10X-4 8 SDF-10X-SHOT 8 SDF-150X-4 8 SDF-150X-SHOT 8 SDF-15X-4 8 SDF-15X-SHOT 8 SDF-1X-4 8 SDF-1X-SHOT 8 SDF-200X-4 8 SDF-200X-SHOT 8 SDF-2X-4 SDF-2X-SHOT SDF-300X-4 SDF-300X-SHOT SDF-30X-4 SDF-30X-SHOT SDF-3X-4 SDF-3X-SHOT SDF-400X-4 SDF-400X-SHOT SDF-4X-4 SDF-4X-SHOT SDF-500X-4 SDF-500X-SHOT SDF-50X-4 SDF-50X-SHOT SDF-5X-4 SDF-5X-SHOT SDF-600X-4 SDF-600X-SHOT SDF-7.5X-4 SDF-7.5X-SHOT SDF-70X-4 SDF-70X-SHOT SDF-BL-4 SDF-BL-SHOT SDF-CAL-SET-4 SK-100X-4 SK-100X-SHOT SK-10X-4 SK-10X-SHOT SK-1X-4 SK-1X-SHOT SK-200X-4 SK-200X-SHOT SK-20X-4 SK-20X-SHOT SK-30X-4 SK-30X-SHOT SK-3X-4 SK-3X-SHOT SK-40X-4 SK-40X-SHOT SK-50X-4 SK-50X-SHOT SK-5X-4 SK-5X-SHOT SK-7.5X-4 SK-7.5X-SHOT SK-BL-4 SK-BL-SHOT SK-CAL-SET-4 SK-HD-100X-4 SK-HD-10X-4 SK-HD-150X-4 SK-HD-15X-4 SK-HD-1X-4 SK-HD-200X-4 SK-HD-20X-4 SK-HD-2X-4 SK-HD-300X-4 SK-HD-30X-4 SK-HD-3X-4 SK-HD-400X-4 SK-HD-40X-4 SK-HD-4X-4 SK-HD-500X-4 SK-HD-50X-4 SK-HD-5X-4 SK-HD-600X-4 SK-HD-7.5X-4 SK-HD-70X-4 SK-HD-BL-4 SK-HD-CAL-SET-4 SRO-100X-4 SRO-150X-4 SRO-200X-4 SRO-300X-4 SRO-35X-4 SRO-400X-4 SRO-70X-4 SRO-CAL-SET-4 STP-100X-4 STP-10X-4 STP-1X-4 STP-200X-4 STP-20X-4 STP-2X-4 STP-300X-4 STP-30X-4 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 9 11 11 11 11 11 11 11 11 10 10 10 10 10 10 10 10 STP-3X-4 STP-40X-4 STP-5X-4 STP-60X-4 STP-BL-4 STP-CAL-SET SWMO-100X-4 SWMO-100X-SHOT SWMO-10X-4 SWMO-10X-SHOT SWMO-150X-4 SWMO-150X-SHOT SWMO-15X-4 SWMO-15X-SHOT SWMO-1X-4 SWMO-1X-SHOT SWMO-200X-4 SWMO-200X-SHOT SWMO-2X-4 SWMO-2X-SHOT SWMO-300X-4 SWMO-300X-SHOT SWMO-30X-4 SWMO-30X-SHOT SWMO-3X-4 SWMO-3X-SHOT SWMO-400X-4 SWMO-400X-SHOT SWMO-4X-4 SWMO-4X-SHOT SWMO-500X-4 SWMO-500X-SHOT SWMO-50X-4 SWMO-50X-SHOT SWMO-5X-4 SWMO-5X-SHOT SWMO-600X-4 SWMO-600X-SHOT SWMO-7.5X-4 SWMO-7.5X-SHOT SWMO-70X-4 SWMO-70X-SHOT SWMO-BL-4 SWMO-BL-SHOT SWMO-CAL-SET-4 SWMO-LT-100X-4 SWMO-LT-100X-SHOT SWMO-LT-10X-4 SWMO-LT-10X-SHOT SWMO-LT-150X-4 SWMO-LT-150X-SHOT SWMO-LT-15X-4 SWMO-LT-15X-SHOT SWMO-LT-1X-4 SWMO-LT-1X-SHOT SWMO-LT-200X-4 SWMO-LT-200X-SHOT SWMO-LT-2X-4 SWMO-LT-2X-SHOT SWMO-LT-300X-4 SWMO-LT-300X-SHOT SWMO-LT-30X-4 SWMO-LT-30X-SHOT SWMO-LT-3X-4 SWMO-LT-3X-SHOT SWMO-LT-400X-4 SWMO-LT-400X-SHOT SWMO-LT-4X-4 SWMO-LT-4X-SHOT SWMO-LT-500X-4 SWMO-LT-500X-SHOT SWMO-LT-50X-4 SWMO-LT-50X-SHOT SWMO-LT-5X-4 SWMO-LT-5X-SHOT SWMO-LT-600X-4 SWMO-LT-600X-SHOT SWMO-LT-7.5X-4 SWMO-LT-7.5X-SHOT SWMO-LT-70X-4 SWMO-LT-70X-SHOT SWMO-LT-BL-4 SWMO-LT-BL-SHOT SWMO-LT-CAL-SET-4 T-W130 V-028S-D-10X V-028S-D-10X-PAK WA-EPH-10X WA-EPH-10X-PAK WA-EPH-ALI 10 10 10 10 10 10 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 8 21 90-91 90-91 91 91 91 WM-20CST-70 WM-20CST-71 WM-20-NMS-10X-1 WM-20-NMS-1X-1 WM-20-NMS-30X-1 WM-20-NMS-3X-1 WM-20-NMS-50X-1 WM-20-NMS-5X-1 WM-20-NMS-90X-1 WM-20-NMS-SET-1 WM-21-10X-4 WM-21-10X-8 WM-21-1X-4 WM-21-1X-8 WM-21-30X-4 WM-21-30X-8 WM-21-3X-4 WM-21-3X-8 WM-21-50X-4 WM-21-50X-8 WM-21-5X-4 WM-21-5X-8 WM-21-90X-4 WM-21-90X-8 WM-21-NMS-10X-1 WM-21-NMS-10X-1 WM-21-NMS-1X-1 WM-21-NMS-1X-1 WM-21-NMS-30X-1 WM-21-NMS-30X-1 WM-21-NMS-3X-1 WM-21-NMS-3X-1 WM-21-NMS-50X-1 WM-21-NMS-50X-1 WM-21-NMS-5X-1 WM-21-NMS-5X-1 WM-21-NMS-SET-1 WM-21-NMS-SET-1 WM-21-SET-4 WM-21-SET-8 WM-75CST-01-5X WM-75CST-02-5X WM-75CST-04-5X WM-75CST-06-5X WM-75CST-07-5X WM-75CST-08-5X WM-75CST-09-5X WM-75CST-13-5X WM-75CST-15-5X WM-75CST-27-5X WM-75CST-29-5X WM-75CST-30-5X WM-75CST-32-5X WM-75CST-33-5X WM-75CST-35-5X WM-75CST-37-5X WM-NMS-14 WM-NMS-14-5X Z-008 Z-008S Z-008S-H-10X Z-008S-M 26, 26, 26, 26, 26, 26, 26, 26, 26, 26, 59 59 61 61 61 61 61 61 61 61 59 59 59 59 59 59 59 59 59 59 59 59 59 59 28 61 28 61 28 61 28 61 28 61 28 61 28 61 59 59 59 59 59 59 59 59 59 59 59 59 59 59 59 59 59 59 28 28 21 54 54 54 INDEX WA-EPH-ALI-PAK 91 WA-EPH-ALI-R1 91 WA-EPH-ALI-R1-PAK 91 WA-EPH-ARO 91 WA-EPH-ARO-PAK 91 WA-EPH-ARO-R1 91 WA-EPH-ARO-R1-PAK 91 WA-EPH-FCS 91 WA-EPH-FCS-PAK 91 WA-EPH-FCS-R1 91 WA-EPH-FCS-R1-PAK 91 WA-EPH-MS2-20ML 91 WA-EPH-MS2-20ML-PAK 91 WA-VPH 90 WA-VPH-100X 90 WA-VPH-100X-PAK 90 WA-VPH-10X 90 WA-VPH-10X-PAK 90 WA-VPH-10X-SS 90 WA-VPH-10X-SS-PAK 90 WA-VPH-MS 90 WA-VPH-MS-PAK 90 WA-VPH-PAK 90 WA-VPH-RT 90 WA-VPH-RT-PAK 90 WC-OILG-10X-1 2, 96 WFD2-R1-SET 93 WFD2-SET 93 WFK-SET 93 WGU-SET 93 WM-11-NMS-10X-1 61 WM-11-NMS-1X-1 61 WM-11-NMS-30X-1 61 WM-11-NMS-3X-1 61 WM-11-NMS-50X-1 61 WM-11-NMS-5X-1 61 WM-11-NMS-90X-1 61 WM-11-NMS-SET-1 61 WM-12-10X-4 59 WM-12-10X-8 59 WM-12-1X-4 59 WM-12-1X-8 59 WM-12-30X-4 59 WM-12-30X-8 59 WM-12-3X-4 59 WM-12-3X-8 59 WM-12-50X-4 59 WM-12-50X-8 59 WM-12-5X-4 59 WM-12-5X-8 59 WM-12-90X-4 59 WM-12-90X-8 59 WM-12-NMS-10X-1 61 WM-12-NMS-1X-1 61 WM-12-NMS-30X-1 61 WM-12-NMS-3X-1 61 WM-12-NMS-50X-1 61 WM-12-NMS-5X-1 61 WM-12-NMS-SET-1 61 WM-12-SET-4 59 WM-12-SET-8 59 WM-20CST-01 59 WM-20CST-02 59 WM-20CST-03 59 WM-20CST-04 59 WM-20CST-06 59 WM-20CST-07 59 WM-20CST-08 59 WM-20CST-09 59 WM-20CST-13 59 WM-20CST-15 59 WM-20CST-27 59 WM-20CST-29 59 WM-20CST-30 59 WM-20CST-32 59 WM-20CST-33 59 WM-20CST-34 59 WM-20CST-35 59 WM-20CST-37 59 WM-20CST-41 59 WM-20CST-43 59 WM-20CST-50 59 WM-20CST-52 59 WM-20CST-53 59 WM-20CST-54 59 WM-20CST-55 59 WM-20CST-60 59 WM-20CST-63 59 WM-20CST-64 59 WM-20CST-67 59 vii On-Line Ordering There 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